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KV4000 Kinematic Viscosity Bath
Operation and Technical Manual
KV4000-Manual
-
14 -
difference obtained in the previous step.
This is the offset value.
c. Press the Program Key. The lower
green display will flash. Use the up or
down keys to adjust to the new
calibration offset value on the upper red
display calculated in the previous step.
When the value has been entered, the
controller will automatically store the
value. The lower green display will stop
flashing. If further adjustments are
necessary, press the Program Key
again. Resume regular operations by
pressing the Exit / Function key two
times. Verify if the new calibration is
correct by observing the upper red
display and comparing the value with
the calibrated reference device.
Auto Tune.
This routine allows the digital
temperature control to learn the heating
parameters needed for any particular set
point temperature. This operation should be
done when installing a new unit, after
replacing or changing the bath medium type,
or utilizing a different temperature set point
20% different from the previously used set
point temperature.
a. Set the operating temperature to the
desired setting.
b. Press the up and down arrow buttons
simultaneously for about 5 seconds.
When Auto Tune is active, the lower
green LED display will blink
TUNE
. Auto
Tune will automatically toggle off when
the set point temperature is reached.
Auto tune can be terminated by pressing
the up & down buttons simultaneously
again.
5 Operation
This unit is designed for performing kinematic
viscosity tests using glass capillary viscometers.
Please be sure to read the safety and hazard
warnings, the installation procedure, and any of
the standard test methods before operating this
instrument.
5.1 Bath
Fill the
bath with the appropriate heat transfer
fluid based upon the testing temperature. Fill the
bath with the medium from the top through one
of the seven port openings using a wide neck
funnel with a 500mL griffin beaker adding about
½ L at a time to 2" (5 cm) from the top of the
bath to allow room for fluid expansion. This will
provide the proper depth for immersing the
viscometers and allow for thermal expansion.
NOTE:
Do not attempt moving the bath
when filled with fluid medium. Drain all fluid
before moving or relocating the instrument. See
section 7.2 of this document. Sudden starting
and stopping could result in hot bath fluid being
forcefully ejected from the bath. It could also
result in overbalancing and tipping over the
instrument.
NOTE:
Do not drain the bath until the fluid is at
ambient temperature.
Testing
Temperature
Recommended Fluid
15 - 50°C*
Distilled water will be suitable.
50 - 95°C
Koehler
supplies
highly
refined white technical oil
(part # 355-001-001) that
contains an oxidation inhibitor
to limit clouding at higher
temperatures.
CAS# 8042-47-5
Minimum Flash Point: 120°C
(248°F)
Fire Point: 202°C (395°F)
95 - 150°C
Koehler supplies a clear
silicone heat transfer fluid
(part # 355-001-002) with high
oxidation resistance and low
volatility. CAS # 63148-62-9.
Minimum Flash Point: 200°C
(392°F).
NOTE:
Do not use bath fluids that will
decompose or volatilize producing flammable
vapors below the maximum instrument operating
tempe25°C.
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