24
Manual filling:
You can fill the evaporation flask manually
prior to creating the vacuum. The evaporation flask should
not be filled more than half its volume.
Automatic filling:
Prior to filling the evaporation flask, a
vacuum controller is used to regulate the glass apparatus
to the target pressure.
• Now fill the evaporation flask using the back feed line.
Adjust the drive height
Adjust the lower end stop
To adjust the drive height, grasp the height adjusting
handle and hold the trigger (
1
).
The lift is unlocked and you can move the drive up and
down. Release the trigger, the lift is locked in the adjusted
height.
Depending on the size of the
evaporation flask, the setting angle
of the rotary drive and the position
of the heating bath and lift, the
evaporation flask can be in contact
with the bottom of the heating
bath.
Glass may break!
Limit the lower lift position with the variable end stop.
Turn the knob (
1
) anticlockwise to unlock the stopper, and
then you may adjust the lower end stop by moving it up
and down.
Turn the knob clockwise, the stopper is locked in the
adjusted lower end stop.
Refer to the operating instructions
of the heating bath!
• Move the drive to the bottom position and check the
position of the heating bath in relation to the evaporation
flask. When using larger evaporation flasks or depending
on the angle of the rotary drive, you can move the heating
bath to the right.
• Fill the heating bath with the tempering medium until the
evaporation flask is surrounded by tempering medium to
2/3 of its volume.
CAUTION
CAUTION
CAUTION
CAUTION
CAUTION
Fill the evaporation flask
Set up the heating bath
• Switch on the rotary drive and slowly increase the speed.
Avoid creating waves.
• Switch on the heating bath using the power switch.
Avoid stress on the glass due to
different evaporation flask and
heating bath temperatures when
lowering the evaporation flask into
the heating bath!
• Due to the vacuum present, the solvent is suctioned into
the evaporation flask. This enables you to keep solvent
loss due to suctioning to a minimum.
The maximum allowed load (eva-
poration flask and contents) is 3 kg.
CAUTION
1
1
The scale from 1 to 10 corresponds to a speed range of 20
to 300 rpm under nominal load.
NOTICE
Make sure that the speed adjusting
knob is in the “
0
” position when
switching on the power switch,
otherwise a warning sound will be
given.
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