Montageanleitung
Mounting instruction
Instruction de montage
Инструкция по монтажу
20000005212
RV 10_1_2_10_20_042016
Betriebsanleitung
DE
Operating instructions
EN
Mode d’emploi
FR
Инструкция по монтажу RU
00/0000/0
IKA
®
- Werke GmbH & Co.KG
Janke & Kunkel-Str. 10
D-79219 Staufen
Tel. +49 7633 831-0
Fax +49 7633 831-98
[email protected]
www.ika.com
EN
•
Read the mounting instruction in full before starting up and follow the safety instructions.
• Refer also to the safety instructions of operating instructions for the manual of the rotary evaporator.
• Keep the operating instructions in a place where they can be accessed by everyone.
• Ensure that only trained staff work with the appliance.
• Follow the safety instructions, guidelines, occupational health and safety and accident prevention regulations.
When working under a vacuum in particular!
• Wear your personal protective equipment in accordance with the hazard category of the medium to be processed. Otherwise there is a risk of:
- splashing liquids,
- body parts, hair, clothing and jewellery getting caught,
- injury as a result of glass breakage.
• Ensure that there is sufficient space above the device as the glass assembly may exceed the height of the device.
• Prior to each use, always check the device, accessories and especially the glass parts for damage. Do not use damaged components.
• Ensure that the glass assembly is tension-free! Danger of cracking as a result of:
- stress due to incorrect assembly,
- external mechanical hazards,
- local temperature peaks.
• Operation with excess pressure is not permitted (cooling water pressure 0.5 bar, minimum cooling water flow rate 30 l/h, maximum cooling water flow rate 100 l/h).
• The glass equipment must always be ventilated when working under normal pressure (e.g. open outlet at cooler) in order to prevent a pressure build-up.
• Evacuated glass vessels must not be heated on one side; the evaporating flask must rotate during the heating phase.
• The glassware is designed for operation under a vacuum of up to 1 mbar. The equipment must be evacuated prior to heating (see manual rotation drive,
chapter ”Commissioning”). The equipment must only be aired again after cooling. When carrying out vacuum distillation, uncondensed vapours must
be condensed out or safely dissipated. If there is a risk that the distillation residue could disintegrate in the presence of oxygen, only inert gas must be
admitted for stress relief.
•
Danger of burning!
The heating bath, tempering medium, evaporator piston and glass assembly can become hot during operation and remain so
for a long time afterwards! Let the components cool off before continuing work with the device.
• A vacuum may form inside the glassware in case of power outage of the rotation drive.
• Imbalance may result in uncontrolled resonance behaviour of the rotation drive or the assembly. Glass apparatus may be damaged or destroyed. In the
event of unbalance or unusual noises, switch off the rotation drive immediately or reduce the speed.
•
Caution!
The surface of the evaporating flask is slippery when silicone oil is used as a tempering medium in the heating bath!
The glassware is made of borosilicate glass 3.3.
The coating of the glassware vertical coated is made out of the material SURLYN.
The glassware vertical coated by SURLYN are suitable for the use in a temperature range from -30 upto +60 °C.
Item
Designation
Quantity glassware diagonal
Quantity glassware vertical
1
Receiving flask
1
1
2
Clamp NS 29, stainless steel
1
1
4
Stopcock
1
1
5
Tube
-
1
6
Condenser
1 Diagonal condenser
1 Vertical condenser
7
Connection
1 Introduction sleeve
1 Vacuum connection
8
Clamp NS 29, plastic
1
1
10
Evaporator piston 1000 ml
1
1
11
Ball joint clamp RV 05.10
1
1
12
Screw joint cap
4
4
13
Hose connection
4
4
18
Washer
-
1
Safety instructions
Product information
Delivery scope
Mounting vacuum seal (illustrations zoomed in see manual rotary evaporator)
Inserting vacuum seal
Place the vacuum seal in the condenser
receptacle and fit the glassware to the
device according to the assembly inst-
ructions (Fig. 11 a, b and c).
Note: The vacuum seal has to be intro-
duced completely into the the condenser
receptacle. Pay attention to the correct
positon of the vacuum seal.
First use
Insert steam tube (1).
Insert the vacuum seal (2). Pay attention to
the correct positon of the vacuum seal!
Loosen the union nut and the annular spring
from the drive head of the rotation evapora-
tor and slide these parts over the condenser
flange (Fig. 11d). The annular spring engages
in the flange slot, so the union nut is secured.
Mount the small parts onto the condenser.
Secure the vertical condenser by the Velcro
®
band to the support rod.
Hinweis: See operating instructions for the rotary
evaporator!
1
2
3a
3b
Fig. 11a
Fig. 11b
Fig. 11c
Fig. 11d
The seal on the glass condenser should be checked at regular intervals and replaced if necessary.
For cleaning disconnect the main plug.
To clean the glassware use only water with a detergent that contains tensides, or use isopropylalcohol for stubborn soiling.
Cleaning
Source language: German
Glassatz vertikal /
Glassware vertical /
Verrerie verticale /
Вертикальная стеклянная посуда
RV 10.1
RV 10.700
RV 10.900
RV 10.6000
Glassatz vertikal beschichtet /
Glassware vertical, coated /
Verrerie verticale, avec revêtement /
Вертикальная стеклянная посуда
с покрытием
RV 10.10
RV 10.710
RV 10.910
RV 10.6010
Glassatz diagonal /
Glassware diagonal /
Verrerie diagonale /
Диагональная стеклянная посуда
RV 10.2
RV 10.800
RV 10.1000
RV 10.7000
Glassatz diagonal beschichtet /
Glassware diagonal, coated /
Verrerie diagonale, avec revêtement/ /
Диагональная стеклянная посуда
с покрытием
RV 10.20
RV 10.810
RV 10.1010
RV 10.7010
7
8
13 (4x)
12 (4x)
6
18
5
4
1
11
10
2
Rotationsantrieb
Rotation drive
Entraînement de rotation
Привод
7
8
13 (4x)
12 (4x)
6
18
5
4
1
11
10
2
Mounting the washer (illustrations zoomed in see manual rotary evaporator)
Fig. 18a
Drainage
washer
Fig. 18b
Note:
Pay attention to the correct positon of the washer.
The PTFE tube (5) with the washer (18) can be mounted optionally on the
vertical glass sets.
It serves for filling the evaporator flask when there is a vacuum in the glass
set.
Solvent can be sucked through the PTFE tube into the evaporator flask by
opening the stopcock (4).
3991500d
