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• Ultra pure water, 500 mL
1.
Put on the personal protective equipment identified in the safety data sheet (MSDS/SDS).
2.
Rinse the volumetric flask with ultra pure water three times.
3.
Add approximately 21.25 g of NaNO
3
to the volumetric flask.
4.
Add 100 mL of ultra pure water to the volumetric flask.
5.
Shake the volumetric flask until the powder is fully dissolved.
6.
Add ultra pure water to the 500-mL mark.
7.
Shake the volumetric flask to fully mix the solution.
Note: The approximate shelf life of the prepared solution is 3 months.
3.7.3 Rinse and fill the calibration standard bottle
Add a small quantity of calibration standard to the calibration standard bottle. Swirl the bottle to rinse
the bottle, then discard the calibration standard. Fill the calibration standard bottle with 10-mg/L (10-
ppm) Sodium Chloride (NaCl) standard.
Note: Not all analyzers have a calibration bottle. The calibration standard bottle has a label with a yellow stripe. A
yellow "CAL" label is attached to the tubing for the calibration standard bottle.
If prepared solution
is
available, go to the next section.
If prepared solution
is not
available, prepare 10-mg/L NaCl standard as follows. All volumes and
quantities used to prepare the calibration standard must be precise.
Items supplied by the user:
• Volumetric flask (2x), 500 mL, Class A
• NaCl, 1.272 g
• Ultra pure water, 500 mL
• 1–10 mL TenSette pipet and tips
1.
Prepare 500 mL of 1-g/L NaCl standard as follows:
a.
Rinse the volumetric flask with ultra pure water three times.
b.
Add 1.272 g NaCl to the volumetric flask.
c.
Add 100 mL of ultra pure water to the volumetric flask.
d.
Shake the volumetric flask until the powder is fully dissolved.
e.
Add ultra pure water to the 500-mL mark.
f.
Shake the volumetric flask to fully mix the solution.
2.
Prepare 500 mL of 10-mg/L NaCl standard as follows:
a.
Rinse the other volumetric flask with ultra pure water three times.
b.
Use a pipet to add 5 mL of the 1-g/L calibration standard to the volumetric flask. Put the pipet
in the flask to add the solution.
c.
Add ultra pure water to the 500-mL mark.
d.
Shake the volumetric flask to fully mix the solution.
Note: The approximate shelf life of the prepared solution is 3 months.
Section 4 Preparation for use
Install the analyzer bottles and stir bar. Refer to the operations manual for the startup procedure.
Section A Appendix
A.1 Prepare KCl electrolyte
To prepare 500 mL of 3M KCl electrolyte, do the steps that follow:
36
English
Содержание NA5600 sc Na+
Страница 17: ...English 17 ...
Страница 34: ...Figure 20 DIPA bottle installation Analyzer without enclosure 34 English ...
Страница 52: ...3 5 1 Abnehmen der Stromabdeckplatte Berücksichtigen Sie dabei die folgenden bebilderten Schritte 52 Deutsch ...
Страница 54: ...54 Deutsch ...
Страница 62: ...Abbildung 10 Führen des Kabels durch einen internen Anschlussstecker 62 Deutsch ...
Страница 72: ...Abbildung 20 Installation der DIPA Flasche Analysator ohne Gehäuse 72 Deutsch ...
Страница 92: ...92 Italiano ...
Страница 100: ...Figura 10 Far passare il cavo attraverso il tappo di una porta interna 100 Italiano ...
Страница 110: ...Figura 20 Installazione del flacone di DIPA Analizzatore senza alloggiamento 110 Italiano ...
Страница 128: ...3 5 1 Dépose du couvercle d accès électrique Reportez vous aux étapes illustrées suivantes 128 Français ...
Страница 130: ...130 Français ...
Страница 138: ...Figure 10 Acheminement du câble par un connecteur de port interne 138 Français ...
Страница 148: ...Figure 20 Installation du flacon de DIPA Analyseur sans boîtier 148 Français ...
Страница 167: ...Español 167 ...
Страница 175: ...Figura 10 Pasar el cable a través de un tapón de puerto interno Español 175 ...
Страница 185: ...Figura 20 Instalación de una botella de DIPA en un analizador sin carcasa Español 185 ...
Страница 202: ...3 5 1 Remover a tampa de acesso eléctrico Consulte os passos ilustrados abaixo 202 Português ...
Страница 204: ...204 Português ...
Страница 212: ...Figura 10 Passar o cabo através de uma tampa de porta interna 212 Português ...
Страница 222: ...Figura 20 Instalação do frasco de DIPA Analisador sem estrutura 222 Português ...
Страница 239: ...3 5 1 De afdekkap voor elektronica verwijderen Raadpleeg de volgende afgebeelde stappen Nederlands 239 ...
Страница 241: ...Nederlands 241 ...
Страница 249: ...Afbeelding 10 Steek de kabel door de tule van een interne poort Nederlands 249 ...
Страница 259: ...Afbeelding 20 DIPA fles plaatsen Analyser zonder behuizing Nederlands 259 ...
Страница 277: ...3 5 1 Zdejmowanie pokrywy dostępu elektrycznego Sprawdzić listę kolejnych czynności na rysunku Polski 277 ...
Страница 279: ...Polski 279 ...
Страница 287: ...Rysunek 10 Poprowadzenie przewodu przez zatyczkę portu wewnętrznego Polski 287 ...
Страница 297: ...Rysunek 20 Instalacja butelki z DIPA analizator bez obudowy Polski 297 ...
Страница 314: ...3 5 1 Ta bort el åtkomstskyddet Se de illustrerade stegen som följer 314 Svenska ...
Страница 316: ...316 Svenska ...
Страница 333: ...Figur 20 Installation av DIPA flaska analysator utan kapsling Svenska 333 ...
Страница 351: ...Suomi 351 ...
Страница 368: ...Kuva 20 DIPA pullon asennus analysaattori jossa ei ole koteloa 368 Suomi ...
Страница 385: ...3 5 1 Az elektromos szerelőfedél leszerelése Lásd az alábbi képeken bemutatott lépéseket Magyar 385 ...
Страница 387: ...Magyar 387 ...
Страница 395: ...10 ábra Vezesse át a kábelt az egyik belső csatlakozó dugóján Magyar 395 ...
Страница 405: ...20 ábra DIPA palack beszerelése ház nélküli analizátor Magyar 405 ...
Страница 423: ...3 5 1 Снимите крышку доступа к электрооборудованию Следуйте инструкциям на представленных ниже рисунках Русский 423 ...
Страница 425: ...Русский 425 ...
Страница 433: ...Рисунок 10 Пропустите кабель через заглушку внутреннего порта Русский 433 ...
Страница 443: ...Рисунок 20 Установка бутылки DIPA Анализатор без корпуса Русский 443 ...
Страница 461: ...Türkçe 461 ...
Страница 478: ...Şekil 20 DIPA şişesinin takılması Muhafazasız analiz cihazı 478 Türkçe ...
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Страница 483: ......