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User Manual ECC-Opto-Std – Release 2.62

9 Components ECC-Opto-Std

Socket screw

DIN-912 M4x10

Lid

ECC1-00-0127-A

Glass window 22 x 0.3 mm

LAB0018

Current collector mesh (Al)

ECC1-00-0328-B

Current collector mesh (Cu)

ECC1-00-0328-A

Stand ECC-Opto-Std

ECC1-00-0151-A

Feed wire

ECC1-00-0010-F

Compression spring (Au)

FED9015

Touch screw

ECC1-00-0128-A

Glass fiber separator

with tongue 10 x 1.0 mm

ECC1-01-0012-J

O-Ring 16 x 1.8 mm

DIC9012

Cell base

ECC1-00-0124-A

O-Ring 6.75 x 1.78 mm

DIC9013

Reference electrode pin

ECC1-00-0010-G

Plug

ECC1-00-0130-B

Piston

ECC1-00-0126-A

Содержание ECC-Opto-Std

Страница 1: ...2016 EL CELL GmbH User Manual Release 2 62 Electrochemical Test Cell ECC Opto Std November 2016...

Страница 2: ...ies EL CELL GmbH maintains the right to make changes without further notice to products described in this manual to improve reliability function or design EL CELL GmbH does not assume any liability ar...

Страница 3: ...Description 4 2 Features 6 3 Safety Precautions 7 4 Unpacking 7 5 Assembly and Connection 9 6 Disassembly and Cleaning 12 7 X Ray Experiments 13 8 Further Kits 15 9 Components ECC Opto Std 16 10 Spar...

Страница 4: ...nt collector is placed right below the optical window This WE is sandwiched from below with a glass fiber separator and an appropriate counter electrode CE This way the optical instrument looks from t...

Страница 5: ...window Current collector mesh Aluminium or Copper 16 mm Spring loaded piston Working electrode material WE placed on the current collector mesh Glass fiber separator Counter electrode CE Inspection ar...

Страница 6: ...pphire Beryllium and Kapton windows are available on request Working electrodes can be single crystals or grains powder samples and free standing electrodes applied onto current collector mesh Maximum...

Страница 7: ...ly toxic and can cause cancer Take proper precautions when handling the Beryllium window Avoid direct contact with skin Carefully collect and dispose properly any Beryllium fragments when accidentally...

Страница 8: ...eed wire assy ECC1 00 0010 F 4 Current collector mesh copper 5 pieces ECC1 00 0328 A V 5 Current collector mesh aluminium 5 pieces ECC1 00 0328 B V 6 Filling tube with syringe 5 ml for vacuum filling...

Страница 9: ...ctrode max 10 mm in diameter max 1 mm thick 4 Put the provided glass fiber separator on top 5 Place the working electrode on top of the separator with the active layer pointing UPWARDS The working ele...

Страница 10: ...rds Then release the piston so that the electrolyte is sucked into the cell by the previously applied vacuum NOTE Never pressurize the cell during the filling procedure Repeat the two previous steps t...

Страница 11: ...11 of 19 User Manual ECC Opto Std Release 2 62 13 Connect your potentiostat to the 2 mm sockets 1 of the cell cable grey REF red WE blue CE Adapters 2 are provided for connection to 4 mm banana plugs...

Страница 12: ...slightly depends on the thickness of the cell stack 6 Disassembly and Cleaning Right after use disassemble the cell in the reverse order of assembly All chemicals used have to be disposed properly Al...

Страница 13: ...kit comprises a Beryllium window ECC1 00 0222 A and a modified cell lid ECC1 00 0127 C The lid features a 10 mm inspection hole and a 10 mm wide groove that allows for a viewing angle onto the sample...

Страница 14: ...small piece of polyethylene foil 15 mm in diameter 10 m thick in between the holed current collector and the Beryllium window Beryllium is highly toxic and can cause cancer Take proper precautions wh...

Страница 15: ...w 22 x 0 3 mm ECC1 00 0149 A 2 Lid Sapphire ECC1 00 0127 B Components Zinc Selenide Kit ECC1 00 0156 D 1 Zinc Selenide window 22 x 0 3 mm ECC1 00 0250 B s 2 Lid Zinc Selenide ECC1 00 0127 E Components...

Страница 16: ...328 B Current collector mesh Cu ECC1 00 0328 A Stand ECC Opto Std ECC1 00 0151 A Feed wire ECC1 00 0010 F Compression spring Au FED9015 Touch screw ECC1 00 0128 A WE Glass fiber separator with tongue...

Страница 17: ...10 N Au standard 5 pieces FED9015 V Spring forces see page 12 Compression spring 20 N Au 5 pieces FED9020 V Spring forces see page 12 Compression spring 30 N Au 5 pieces FED9021 V Spring forces see pa...

Страница 18: ...Kit ECC1 00 0306 A Glass window 5 pieces LAB0018 V Glass fiber separator 5 pieces ECC1 01 0012 J V Current collector mesh copper 5 pieces ECC1 00 0328 A V Current collector mesh aluminium 5 pieces EC...

Страница 19: ...ted Warranty does not cover defects damage or nonconformity resulting from abuse misuse neglect lack of reasonable care modification or the attachment of improper devices to the goods This Limited War...

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