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Serinus 51 

SO

2

/H

2

S Analyzer 

 
 

User Manual 

Version: 1.0 

July 2011 

 
 
 
 
 
 
 

Tel:

 (+61) 1300 364 946.  

Fax:

 (+61) 1300 668 763. 

E-mail:

 [email protected] 

Spare Parts 

[email protected] 

Address: 

Australia - Head Office  

1492 Ferntree Gully rd Knoxfield  Victoria, 3180, Australia 

Содержание Serinus 51

Страница 1: ...r User Manual Version 1 0 July 2011 Tel 61 1300 364 946 Fax 61 1300 668 763 E mail ecotech ecotech com au Spare Parts parts ecotech com au Address Australia Head Office 1492 Ferntree Gully rd Knoxfiel...

Страница 2: ......

Страница 3: ...in the References section of this manual If after reading this manual you have any questions or you are still unsure or unclear on any part of the Serinus 51 then please do not hesitate to contact Eco...

Страница 4: ...tened in place Safety requirements To reduce the risk of personal injury caused by electrical shock follow all safety notices and warnings in this documentation If the equipment is used for purposes n...

Страница 5: ...actory repairs and returned goods efficiently and expeditiously we need your help Before you ship any equipment to our factory please call your local Ecotech service response centre or distributor to...

Страница 6: ...RF immunity IEC 61000 4 4 Electrical fast transient burst immunity IEC 61000 4 5 Surge immunity IEC 61000 4 6 Conducted RF Immunity IEC 61000 4 11 Voltage dips and interruption immunity Electromagneti...

Страница 7: ...y of packing list d Photographs of damaged equipment and container e Contact you freight forwarder for insurance claims You may want to keep a copy of these documents for your records also Refer to th...

Страница 8: ...use IEC 60417 5016 Earth ground terminal IEC 60417 5017 Protective conductor terminal IEC 60417 5017 Equipotentiality IEC 60417 5021 Alternating current IEC 60417 5032 Caution hot surface IEC 60417 50...

Страница 9: ...Serinus 51 User manual 1 0 Front Matter vii...

Страница 10: ...elevant information on theory specifications installation operation maintenance calibration communication and troubleshooting Any information that cannot be found within this manual can be found by co...

Страница 11: ...ZERO AIR SCRUBBER 6 1 5 4 REACTION CELL 7 1 5 5 MAIN CONTROLLER PCB 7 1 5 6 REFERENCE DETECTOR PREAMPLIFIER 7 1 5 7 PMT HIGH VOLTAGE SUPPLY AND PREAMPLIFICATION 7 1 5 8 LAMP DRIVER PCB 8 1 5 9 PRESSUR...

Страница 12: ...S DOWNLOADER PROGRAM 48 5 5 1 SETTINGS 48 5 5 2 DATA 50 5 5 3 REMOTE SCREEN 51 5 5 4 REMOTE TERMINAL 52 6 SERVICE 53 6 1 PNEUMATIC DIAGRAM 53 6 2 MAINTENANCE TOOLS 53 6 3 MAINTENANCE SCHEDULE 54 6 4 M...

Страница 13: ...71 8 3 2 ADDITIONAL COMPONENTS 71 8 3 3 REMOVED COMPONENTS 71 8 3 4 MENUS 71 8 3 5 FLOW CALIBRATION 71 8 3 6 PRESSURE CALIBRATION 71 8 4 HIGH PRESSURE ZERO SPAN VALVE 71 8 4 1 SINGLE PRESSURIZED CALIB...

Страница 14: ...e 18 Serinus Downloader Remote Screen tab 51 Figure 19 Serinus downloader Remote Terminal tab 52 Figure 17 Pneumatic diagram 53 Figure 18 Removing plunger 55 Figure 19 Removing fan filter 55 Figure 20...

Страница 15: ...tly with a bypass taking the sample around the SO2 scrubber and thermal converter All measurements are automatically corrected for gas temperature and pressure changes and referenced to 0 C 20 C or 25...

Страница 16: ...lectable current output of 0 20 mA 2 20mA or 4 20 mA or Voltage output of 0 to 5 V with menu selectable zero offset of 0 5 or 10 Range 0 full scale from 0 0 05 ppm to 0 20 ppm with 0 5 and 10 offset R...

Страница 17: ...automatic zero performs a zero check at a specified time through a 24 hour cycle which adjusts the lower limit of the analyzers Zero air Purified air in which the combined effect of the concentration...

Страница 18: ...efineries paper mills coke ovens aluminum steel graphite electrical and construction industries and to a smaller extent tannaries Hydrogen sulfide is toxic to many different parts of the human body it...

Страница 19: ...y the Hydrocarbon Kicker and is also used to perform zero background adjustments 1 4 2 Kalman filter theory The Serinus analyzer series use the advanced digital Kalman filter This filter provides the...

Страница 20: ...than 5 m and condensed water vapour that interfere with sample measurement 1 5 2 Hydrocarbon Kicker The Hydrocarbon kicker removes interfering hydrocarbons from sample air This is achieved by using c...

Страница 21: ...e SO2 reactions UV Reference Detector The UV reference detector monitors the intensity of UV radiation entering the measurement cell This measurement is used to compensate for variations in UV lamp ou...

Страница 22: ...input voltage of 115 or 230VAC 50 60 Hz and an output voltage of 12 VDC power for distribution within the analyzer Note Input voltage can be manually changed by sliding the red switch left 230 for 22...

Страница 23: ...ss and real time access to instruments when a network is available to connect with External I O port The Analog Digital port sends and receives analog digital signals to other devices These signals ar...

Страница 24: ...that may be installed in either the front or rear panel then either slide the lid backwards bench top Check that all pneumatic and electrical connectors are connected if not reconnect Check for any vi...

Страница 25: ...g moisture condensation in sample Do not pressurize sample line under any circumstances Sample should be drawn through instrument from the atmosphere This should be done either by and internal pump if...

Страница 26: ...is recommended that a gas calibrator be used with SO2 source to deliver precise concentrations of SO2 Exhaust port The exhaust port is where the measured sample is expelled from the analyzer The exhau...

Страница 27: ...logger TCP IP optional Plug in network cord this cord should be attached to network Use Remote data download program to access instrument and download data supplied on utilities CD Analog Digital Thi...

Страница 28: ...s Remove instrument from rack Replace red plugs into pneumatic connections Place instrument back in plastic bag with desiccant packs and seal bag Ideally the bag it was delivered in Place back in foam...

Страница 29: ...mA for a stable reference voltage signal output 10 15 minutes Ref stabilize Adjusts the detector to set its maximum voltage output and create a stable output signal After this warm up has completed th...

Страница 30: ...rner these lights indicate the status of the instrument as a whole a A red light indicated that the instrument has a major failure and is not functioning b A yellow light indicates there is a minor pr...

Страница 31: ...s all information and fields available to users and is generally only used during initial setup Time and Date 6 The Time and Date are displayed in between the menu buttons at the bottom of the screen...

Страница 32: ...s is running through the measurement cell When this is happening activate the span calibrate field a window will open with editable numbers change the numbers to match the concentration that the instr...

Страница 33: ...moving the USB memory to safely remove the USB stick also occurs in the service menu 3 5 6 Failure to do this may cause corruption to the data on the memory stick Gain A multiplication factor used to...

Страница 34: ...wer failure occurred or power was disconnected from analyzer 3 5 2 1 Status The Component status menu contains a list of the main components within the instrument and their status Cell Temp The cell t...

Страница 35: ...e field to allow the user to change the current temperature units of the analyzer Cell Temperature of the reaction cell Converter Temperature of the thermal converter Flow block optional internal pump...

Страница 36: ...the preprocessor proportional to the detected gas signal from the reaction cell This voltage represents the actual measurement of gas Ref Voltage Reference voltage as measured by the preamplifier boar...

Страница 37: ...buttons to change time 24 hour clock Backlight Select how long the instrument backlight will stay on for 30 Secs 1 Min 2 Mins 5 Mins 10 Mins 30 Min 1 Hr Always On Always Off Front Screen This field al...

Страница 38: ...is a microprocessor generated field and cannot be set by the operator Note This reading is only valid if zero air or a steady concentration of span gas has been fed to the analyzer for at least one h...

Страница 39: ...calibration mode selected below Note Timed calibration with span comp enable does not fulfill U S EPA approval Cal Port Select whether the instrument will sample from the external span zero source Ca...

Страница 40: ...me and date Note The units of the repeat interval can be changed by pressing the key minutes hours days Span Cal Level Enter the concentration of span gas used during the timed span calibrations Cycle...

Страница 41: ...en service work is being performed Next service due An editable field where the user can set the date when the next instrument service is required Section 6 3 has a recommended maintenance schedule th...

Страница 42: ...tic which configures the instrument for tests on the optical measurement source Electrical which configures the instrument for testing of the electrical circuits Preamp which configures the instrument...

Страница 43: ...s Span Zero select Shows the action of the valve that determines whether Sample gas or Calibration gas internal zero air is being sampled Open Span Zero Closed Sample gas Cal Port Select Shows the act...

Страница 44: ...rovides a list of calibration values used by the instrument to generate valid data The operator can collect these values and report them on calibration reports as part of their quality assurance Instr...

Страница 45: ...when Over ranging is set to enabled Set to desired over range value This value cannot be set below the RANGE value This is the alternate scale the recorder or DAS indicates when over ranging is active...

Страница 46: ...rop ID The ID address of the analyzer when Multidrop RS232 communications is used Baud RS232 1 Set the Baud rate that the instrument will communicate over 1200 2400 4800 9600 14400 19200 38400 Protoco...

Страница 47: ...Serinus 51 User manual 1 0 Operation 33 3 5 7 5 Digital Outputs Menu Assign the digital outputs 0 7...

Страница 48: ......

Страница 49: ...rt 1 Ensure suitable zero air source is connected to the sample port on the back panel of analyzer see section 2 3 1 2 Let the instrument stabilize 3 Enter the quick menu and select Zero Calibration 4...

Страница 50: ...e H2S efficiency is set to 100 2 Connect a source of H2S span gas to the calibration port 3 Enter Main Menu Measurement Settings menu Gas to Measure and set this field to H2S 4 Allow H2S readings to s...

Страница 51: ...nt to sample for 15 minutes and record measurement 6 The linearity and correlation can be calculated for each point manually or all points calculated within excel 7 Manual Calculations Record the conc...

Страница 52: ...are found The gradient m falls between 0 98 and 1 02 The intercept b lies between 0 3 The correlation R2 is greater than 0 9995 13 Reject the calibration if the above criteria are not met If the cali...

Страница 53: ...w fitting from top of cell anticlockwise remove 1 8 black tubing and screw stainless steel blocker onto fitting 1 in Figure 9 3 Remove tubing connecting to hydrocarbon kicker from cell T piece 2 in Fi...

Страница 54: ...en select the unit of pressure being used torr etc 7 The screen will display two horizontal bars Figure 10 the first Amb is for the ambient pressure sensor the second Cell is for the cell pressure sen...

Страница 55: ......

Страница 56: ...is function is an optional extra and must be purchased from Ecotech RS232 2 RS232 communication is the most reliable way to access data from instrument RS232 port 2 should be connected to a computer d...

Страница 57: ...as seen on the PC This should take a Device Installer If a message box comes up asking you to vie click No Figure 12 Device Installer pop up window When initial search has completed access the XPort...

Страница 58: ...ss this value should be obtained from your network administrator and enter Gateway address c Set the number of Netmask bits e g 24 255 0 0 0 16 255 255 0 0 8 255 255 255 0 d When it asks you to Set pa...

Страница 59: ...mote IP Address 000 000 000 000 Remote Port 0 DisConnMode 00 FlushMode 00 DisConnTime 00 00 SendChar 1 00 SendChar 2 00 Settings available during Channel 1 setup 11 When returned to the Change Setup m...

Страница 60: ...ontrol of the Analyzer such as Zero Span sequences Each input has a terminating resistor which can be either PULL UP or PULL DOWN This is set using the Jumper JP1 on the Back Panel printed circuit boa...

Страница 61: ...e 16 External 25pin I O individual pin descriptions Warning The Analog and Digital Inputs and Outputs are rated to CAT I meaning that they should be less than 12VDC Exceeding these voltages can perman...

Страница 62: ...settings are defined There are two icons in the main header they are Save Settings which saves the current settings as default and Cancel changes Output Output file Enter in the destination folder in...

Страница 63: ...ion Used when the analyzer is being connected via a network IP Address Enter the IP address of the analyzer as described in Ecotech technote TEC 0045 Port Enter the port number of the analyzer as desc...

Страница 64: ...ges and displays on screen along with saving as a text file Save data Saves the data into excel file format Clear Data Deletes data from the screen Rebuild index This function is used when the downloa...

Страница 65: ...e instrument The screen is a screenshot and not an automatically updated feed the refresh button will need to be used when tracking changes in parameters By clicking the green Connect button in the to...

Страница 66: ...r must be clicked The remote terminal tab consists of 3 different sections Advanced Protocol Within this section the user selects the parameter number from within the advanced protocol then clicks the...

Страница 67: ...re the following equipment Toolbox Digital multimeter DMM Computer or remote data terminal and connection cable for RS232 communication Pressure transducer absolute and connection tubing calibrated in...

Страница 68: ...check 40 Monthly Check fan filter clean if necessary 55 Perform span calibration 35 Check date and time is correct 23 6 Monthly Check the zero air scrubber 58 PMT Desiccant packs 59 Perform multi poin...

Страница 69: ...ing place finger on tubing connector and pull to the side Figure 22 Removing plunger 5 Remove old filter wipe down plunger with damp cloth and insert new filter 6 Replace plunger screw cap on and reco...

Страница 70: ...asurement cell T piece 3 Unscrew the T piece form the cell anti clockwise 4 Once the t piece has been removed use the orifice filter removal tool to remove either the orifice and or filter 5 Orifice a...

Страница 71: ...the pressures to stabilize check that the gas flow 0 if this is not the case then there is a leak 5 If the two pressures are within 10 of each other then the leak check has passed 6 If the pressures...

Страница 72: ...location of the leak 6 When the location of the leak has been determined check all tubing and fittings to make sure that they are attached appropriately and have no splits or cracks 6 4 7 Replace Zer...

Страница 73: ...the PMT is extremely sensitive to light it is essential that before opening the PMT assembly to make sure that the analyzer is switched off In addition even when the analyzer is switched off it is ver...

Страница 74: ...DFU and ensure that the flow is in the correct direction arrows points toward tubing 6 4 10 Check UV lamp alignment Required equipment Oscilloscope Proper operation of the UV lamp is essential to the...

Страница 75: ...section 3 5 2 3 3 Compare the Serinus pressure sensor measurement to the current ambient pressure from an external calibrated sensor Ensure that they are reading the same 3 TORR 0 4 kPa 4 If no extern...

Страница 76: ...llic clip holding the battery whilst sliding the old battery out 4 Now place the new battery in with the positive side facing up 5 Close the main PCB and return the screws Close the cover again 6 Turn...

Страница 77: ...0 Heater and thermistor assembly C020074 Power supply optical bench H011211 02 Cooler thermoelectric kit H011211 03 Thermistor assembly kit H011211 04 Serinus 51 User Manual M010040 Lense Biconvex H01...

Страница 78: ...Orifice 14 mil H010043 13 Orifice 20 mil H010043 19 Lamp Assembly UV C020076 External pump repair kit suite 607 pump P031001 Silicone heatsink compound C050013 SO2 Scrubber H040011 01 Molycon Assembly...

Страница 79: ...that the voltage switch is in the proper position Contrast misadjusted Set or adjust the display contrast by simultaneously pressing two keys on the front panel as follows Contrast Press Up arrow for...

Страница 80: ...s Faulty calibration source Ensure calibration gas is plumbed correctly is not contaminated and is a NATA NIST reference gas Zero drift No flow Check sampler flow Charcoal saturated Replace the charco...

Страница 81: ...Serinus 51 User manual 1 0 Troubleshooting 67 7 2 Electronic Zero adjust 7 3 SO2 reaction cell temperature failure...

Страница 82: ......

Страница 83: ...o be affected yet reduces the loading filter and therefore the frequency with which they will need to be changed The dual filter option is shown in the pneumatic diagram red dashed line and requires n...

Страница 84: ...bow adjust bracket and lid bolts until the lid is square and bolts are tight Now carefully insert the instrument into the rack by placing the instrument slides into the lid slides ensure that the rac...

Страница 85: ...tubing between the gas cylinder and the analyzer Auxiliary port inlet Note This connection may need to be retightened during this operation 3 Open the cylinder main valve and adjust the regulator to...

Страница 86: ...ulator with shut off valve 2 Connect a line of 1 8 stainless steel tubing between the appropriate gas cylinder and the analyzer inlet port Note This connection may need to be retightened during this o...

Страница 87: ...ation 1 Set Cal Mode Measure 2 Remove the flow meter on the calibration port and connect a vent line to port 3 Reconnect instrument fittings and place in original set up 4 The instrument is now in nor...

Страница 88: ......

Страница 89: ...T HIGH VOLTAGE Pot High Voltage Controller Pot for PMT S50 S40 17 SO2 Lamp ADJ Pot S50 Lamp Adjust Pot 18 O3 Lamp ADJ Pot S10 Lamp Adjust Pot 19 O3 ZERO Measure Pot Coarse S10 Signal Zero coarse 20 O3...

Страница 90: ...en if applicable eg NOx 52 Calculated Gas Concentration Gas 3 eg NO2 53 Primary Gas Average Average of the readings for Gas1 of the last n minutes where n is the averaging period 54 Secondary Gas Aver...

Страница 91: ...age Offset Current Range Gas2 0 0 or 0 20mA 1 5 or 2 20mA 2 10 or 4 20mA 100 Voltage Offset Current Range Gas3 0 0 or 0 20mA 1 5 or 2 20mA 2 10 or 4 20mA 101 Full Scale Gas 1 5 0 Volt Calibration valu...

Страница 92: ...ion Point 3 PPM 139 Calibration Point 4 PPM 140 Calibration Point 5 PPM 141 Desired Pump Flow SLPM 142 Actual Pump Flow SLPM 143 Set Lamp Current 144 Lamp Current mA 145 Cycle Time Minutes 146 CO Cool...

Страница 93: ...SEC FILTER 2 30 SEC FILTER 3 60 SEC FILTER 4 90 SEC FILTER 5 300 SEC FILTER 6 ADPTIVE FILTER 7 165 NO2 Filter 0 Disabled 1 Enabled 166 Background Interval 0 24 Hrs 1 12 Hrs 2 8 Hrs 3 6 Hrs 4 4 Hrs 5...

Страница 94: ...D intensity controller POT 180 Last Power Failure Time Time Stamp of the Last power fail 4 byte time stamp Bit 31 26 Year 0 99 Bit 25 22 Month 1 12 Bit 21 17 Date 1 31 Bit 16 12 Hour 00 23 Bit 11 06 M...

Страница 95: ...Serinus 51 User manual 1 0 Appendix 81 199 External Analog Input 1 200 External Analog Input 2 201 External Analog Input 3 202 Converter Set Point Converter Set Point Temperature...

Страница 96: ...HV FAIL Bit 5 OUT OF SERVICE Bit 4 instrument is in zero mode Bit 3 instrument is in span mode Bit 2 unused Bit 1 SET PPM selected CLEAR MG M3 Bit 0 reserved LSB DSPAN Function Commands the unit under...

Страница 97: ...manual 1 0 Appendix 83 Device response ACK if the unit under test is able to perform the command NAK if not RESET Function Reboots the instrument software reset Format RESET DEVICE I D TERMINATOR Devi...

Страница 98: ...t shown by the following table Character Hex Value Binary Block Check STX 02 0000 0010 0000 0010 D 44 0100 0100 0100 0110 A 41 0100 0001 0000 0111 0 30 0011 0000 0011 0111 9 39 0011 1001 0000 1110 7 3...

Страница 99: ...Serinus 51 User manual 1 0 Appendix 85...

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