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Operating Instructions UVD 170S/340S 

 

 

21

6.3.2  Flow Cell Removal 

• 

If the 

UVD 170S/340S 

is still connected to the data system, first terminate communication 

using the Disconnect command in CHROMELEON

TM

 (

 CHROMELEON

TM

 manual). 

• 

Switch off the detector. Disconnect the power cord. 

• 

Open and remove the side panel. Do not bend the Teflon capillary. 

• 

Undo the 4 retaining screws and remove the flow cell cover. 

• 

Undo the knurled flow cell retaining screw and carefully draw out the flow cell assembly. 

 

  

Warning:

 

During operation, the lamp becomes extremely hot and remains so for 
some time after the unit is switched off. Therefore, to avoid possible 
injury, always allow sufficient time for lamp cooling before attempting 
any maintenance. 

6.3.3  Flow Cell Replacement 

  Important:

 

The flow cells of the detectors 

UVD 170S/340S

 and  

UVD 160S/320S

 

are 

not

 interchangeable. 

 

• 

Insert the new/cleaned flow cell, aligning the notch with the alignment pin of the mounting. 

No

 further alignment is necessary. 

• 

Replace the flow cell cover. 

• 

Replace the side panel. 

• 

The detector may now be switched on and communication with CHROMELEON

TM

 

restored using the Connect command. 

6.3.4  Flow Cell Cleaning 

 

  Important:

  In contrast to the other flow cell versions,

 

it is 

not possible

 to 

disassemble the micro flow cell for cleaning. Clean the micro flow cell 
by flushing with 0.2M nitric acid, followed by water and methanol. 

 

To clean the flow cell (except the micro flow cell), proceed as described below. The numbers 
in parentheses refer to the corresponding parts as illustrated in fig. 7: 

• 

Undo and remove screws (1) and remove the heat exchanger (2). 

• 

Undo and remove screws (5) and carefully remove the lens-retaining plates (6 and 9) and 
lenses (7). 

• 

To avoid scratching the lenses, these should be placed on a clean, lint-free cloth or tissue. 

• 

Clean the lenses using a soft, lint-free cloth or tissue and an optical cleaning solution. 

• 

Scratched or damaged lenses must be replaced. 

 

  Important:

 

Do not

 attempt to remove the flow cell body (8) from its housing (10)! 

 

• 

Cleaning of the flow cell body together with its housing may be carried out by rinsing with 
water, iso-propanol or methanol or by placing the entire assembly into an ultrasonic bath. 

 

Содержание UVD 170S

Страница 1: ...UV VIS Detector UVD 170S 340S Operating Instructions Version 3 01 Date July 14 2000 Dionex Softron 2000 Doc UVD170SUVD340_OI_E_V301 doc...

Страница 2: ...ric emissions standard Part 1 Residential commercial and light industry EN 50082 1 1992 Electromagnetic Compatibility EMC Generic immunity standard Part 1 Residential commercial and light industry EN...

Страница 3: ...n the Front Panel 8 4 3 Installation and Operation within CHROMELEONTM 9 4 3 1 Communication Port 9 4 3 2 Required CHROMELEONTM Modules 9 4 3 3 Installation with the CHROMELEONTM Installation Tool 9 4...

Страница 4: ...and labour ex works Please note that wear parts i e needle needle seat syringe and valve seals cannot be covered by the warranty The warranty period for the deuterium lamp is six months from delivery...

Страница 5: ...accompanying information may result in damage to the instrument Warning Indicates that failure to take note of the accompanying information may result in personal injury 1 4 Intended Use of This Instr...

Страница 6: ...The alteration procedure is as follows Switch off the unit and disconnect the power cable Draw out the fuse cartridge using a small screwdriver fig 1 Using small pliers tweezers to pull out the small...

Страница 7: ...using a small screwdriver fig 1 replace fuses as appropriate Important Only use fuses as indicated in fig 1 min voltage 250 V or those listed in the original parts list If using US type fuses follow t...

Страница 8: ...hnical Specifications page 23 For the standard flow cell the pressure rating is 100 bar 10 000kPa Important The flow cell is primed with 2 propanol 2 4 Rear Panel Connections The UVD 170S 340S is cont...

Страница 9: ...installation Warning Ensure that the PC is off and the power cable disconnected before attempting installation Important The interface board must be protected against static charge at all times If di...

Страница 10: ...bined with extremely low noise electronics enable highest sensitivity Simultaneous detection on 4 wavelengths recording of 3D data fields and the comprehensive data analysis capabilities within the CH...

Страница 11: ...and allow 5 minutes before switching the deuterium lamp on again Otherwise the lamp becomes too hot and could be damaged message Lamp too hot In the event that the PC is switched off or the connection...

Страница 12: ...d then the CHROMELEONTM Installation Tool Server Configuration Select the timebase to which you want to assign the detector UVD170S 340S Via the Edit menu or the menu of the right mouse button choose...

Страница 13: ...ge to view the following signal parameters Signal parameter Description Signal Name Signal name Unit Signal unit of the recorded raw data Factor current amplification factor Tab Dialog Box Error Level...

Страница 14: ...signal specific and global commands are available Signal specific commands Signal type Parameters UV channel Step Average Wavelength Bandwidth Ref Wavelength Ref Bandwidth Signal type Parameters 3D Fi...

Страница 15: ...yl acetate Ensure for the calibration that the deuterium lamp is already warm because its spectrum changes much during the first minutes after switching on the lamp If these conditions are not met the...

Страница 16: ...r not switched on Switch on detector Fuse blown Replace fuse Replaced fuse blows immediately Call Dionex service Connecting cable between UVD 170S 340S and PC not correctly installed Connectors on the...

Страница 17: ...voir on the same level as flow cell Wrong wavelength Select suitable wavelength Connecting cable between UVD 170S 340S and PC not correctly installed Connectors on the detector and the PC must be inse...

Страница 18: ...in the original packing If no original packing is available this can be acquired from Dionex or your local Dionex representative Please note The warranty coverage shall become invalid in any case ide...

Страница 19: ...Operating Instructions UVD 170S 340S 16 Fig 6 Side view UVD 170S 340S side panel open...

Страница 20: ...2 5mm Allen key and carefully remove the lamp The Allen key is contained in the Accessories Warning During operation the lamp becomes extremely hot and remains so for some time after the unit is swit...

Страница 21: ...glass capillary flow cell order no 5065 1800M Standard Flow Cell Order no 5065 1810 The standard flow cell of the UVD 170S 340S has a volume of 10 l and a path length of 9mm The flow cell body is com...

Страница 22: ...lens 1343 0511 9 Lens retaining plate2 5065 1812 11 Single part hand tight fitting included in 5065 1815 12 Capillary tube 1 58x0 25 ID included in 5065 1815 13 PEEK double ferrule 2261 0122 Order No...

Страница 23: ...he UVD 170S 340S has a volume of 6 l and a path length of 2mm The cell body is composed of PEEK and is thus 100 biocompatible The maximum pressure rating of the flow cell is 100bar 10 000kPa Important...

Страница 24: ...low cell cover Replace the side panel The detector may now be switched on and communication with CHROMELEONTM restored using the Connect command 6 3 4 Flow Cell Cleaning Important In contrast to the o...

Страница 25: ...ts as this may lead to irreparable damage Replace the lenses onto either side of the flow cell body so that the flat faces are on the inside Replace the retaining plates 6 and 9 taking care to tighten...

Страница 26: ...l 9mm path Preparative flow cell 6 l 2mm path Micro capillary flow cell 0 14 l 8mm path Flow cell pressure rating Standard flow cell 100bar 10 000kPa Standard flow cell PEEK cap 100bar 10 000kPa Prep...

Страница 27: ...1051 Spanner x 5 16 1 2146 2625 Allen key 2 5mm 1 2261 0121 PEEK fitting screw 1 16 15 mm 2 2261 0122 PEEK double ferrule 2 2309 1100 Accessories container 1 6007 9100 Silicon tubing 2 8 x 1 3 3m 1 8...

Страница 28: ...M3x23 DIN 965 3 pcs Quartz lens 2 pcs Lens retaining plate1 1 pc Lens retaining plate2 1 pc 6065 9001 UVD 340S 170S Repair Kit Quartz lenses 2 pcs PEEK capillary tubing 1 16 0 50 mm 2 m PEEK fitting...

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