Buchi SpeedDigester K-439, Руководство по эксплуатации

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4 Description of function
18
K-439
Operation Manual, Version B
4 Description of function
This chapter explains the basic working principle of the SpeedDigester K-439. It also shows how the
instrument is structured and provides a general functional description of its assemblies.
4 .1 Functional principle
The SpeedDigester K-439 is a special heating device to digest samples. It can generate max. tempera-
tures of 580 °C. This allows e.g. acid digestion of organic sample components in a concentrated
sulfuric acid / catalyst mixture, known as 'Kjeldahl digestion'. During the processing the sample
material can reach peak temperatures of up to 370 °C at the bottom area of the sample tubes. The
maximum temperature of the sample highly depends on its composition i.e. the ratio of catalyst to
acid and can change during the digestion process.
Digestion process overview
3
2
1
4
Environmental
air inlet
dangerous vapors are drawn away
Condensation
zone
Infrared heating
Boiling / digesting
sample
Insulation plate
(fireclay insertion)
Acid vapor
outlet to
suction unit
(e.g. Scrubber)
(
≈
5 cm)
Safety
zone
Processing steps:
• The infrared heating
1
generates high temperatures in the sample.
• Inside the sample tubes the digestion process takes place
2
while the acid is constantly boiling.
• Hot acid fumes rise into the condensing zone
3
. After reflux, the acid flows back down to the
sample material, establishing a constant cycle.
• Residual fumes which escapes the condensation zone is highly corrosive (!) and hazardous to life
forms. It must be withdrawn by a suction unit that deliveres sufficient flow (i.e. with a Scrubber
B-414 or a water jet pump)
4
.
Note
The condensation should not take place inside the safety zone in order to prevent digestion of the
sealing rings. In case the condensation is too close to the suction module (e.g. due to very high
temperature settings) the digestion fumes may escape and the sample can dry out!