22
BÜCHI
Rotavapor
R-220
5 Operation
5.4
Table of Solvents
Solvent
Formula Molar Mass
Evaporation
Boiling Point
Spec.Gravity
Vacuum in mbar for a
in g/mol
Energy in J/g
at 1013 mbar
in g/cm
3
Boiling Point at 40°C
Acetic acid
C
2
H
4
O
2
60.0
695
118
1.049
44
Acetone
C
3
H
6
O
58.1
553
56
0.790
556
n-Amyl alcohol, n-Pentanol
C
5
H
12
O
88.1
595
37
0.814
11
Benzene
C
6
H
6
78.1
548
80
0.877
236
n-Butanol, tert. Butanol
C
4
H
10
O
74.1
620
118
0.810
25
(2-Methyl-2-Propanol)
C
4
H
10
O
74.1
590
82
0.789
130
Carbon tetrachloride
CCI
4
153.8
226
77
1.594
271
Chlorobenzene
C
6
H
5
CI
112.6
377
132
1.106
36
Chloroform
CHCI
3
119.4
264
62
1.483
474
Cyclohexane
C
6
H
12
84.0
389
81
0.779
235
Diethyl ether
C
4
H
10
O
74.0
389
35
0.714
850
1,2,-Dichlorethane
C
2
H
4
CI
2
99.0
335
84
1.235
210
1,2,-Dichlorethylene (cis)
C
2
H
2
CI
2
97.0
322
60
1.284
479
1,2,-Dichlorethylene (trans)
C
2
H
2
CI
2
97.0
314
48
1.257
751
Diisopropyl ether
C
6
H
14
O
102.0
318
68
0.724
375
Dioxane
C
4
H
8
O
2
88.1
406
101
1.034
107
DMF (Dimethylformamide)
C
3
H
7
NO
73.1
153
0.949
11
Ethanol
C
2
H
6
O
46.0
879
79
0.789
175
Ethyl acetate
C
4
H
8
O
2
88.1
394
77
0.900
240
Heptane
C
7
H
16
100.2
373
98
0.684
120
Hexane
C
6
H
14
86.2
368
69
0.660
335
Isoamyl alcohol, 3-Methyl-1-Butanol
C
5
H
12
O
88.1
595
129
0.809
14
Isopropyl alcohol
C
3
H
8
O
60.1
699
82
0.786
137
Methanol
CH
4
O
32.0
1227
65
0.791
337
Methylene chloride, Dichloromethane CH
2
CI
2
84.9
373
40
1.327
850
Methylethylketon
C
4
H
8
O
72.1
473
80
0.805
243
Pentachlorethane
C
2
HCI
5
202.3
201
162
1.680
13
Pentane
C
5
H
12
72.1
381
36
0.626
850
n-Propyl alcohol
C
3
H
8
O
60.1
787
97
0.804
67
1,1,2,2,-Tetrachloroethane
C
2
H
2
CI
4
167.9
247
146
1.595
35
Tetrachloroethylene
C
2
CI
4
165.8
234
121
1.623
53
THF (Tetrahydrofurane)
C
4
H
8
O
72.1
67
0.889
357
Toluol
C
7
H
8
92.2
427
111
0.867
77
1,1,1,-Trichlorethane
C
2
H
3
CI
3
133.4
251
74
1.339
300
Trichlorethylene
C
2
HCI
3
131.3
264
87
1.464
183
Water
H
2
O
18.0
2261
100
1.000
72
Xylol (Mixture)
C
8
H
10
106.2
389
25
(o)
144
0.880
(m)
139
0.864
(p)
138
0.861
Table 3: Table of Solvents (CRC Handbook, 65th Ed)
Содержание Rotavapor R-220
Страница 46: ...46 B CHI Rotavapor R 220 9 Appendix...