34
Rotavapor
R-220 EX
5 Operation
5.6
Table of Solvents
Solvent
Formula
Molar Mass Evaporation Boiling Point Spec.Gravity Vacuum in mbar for a
in g/mol
Energy in J/g at 1013 mbar
in g/cm
3
Boiling Point at 40°C
Acetic acid
C
2
H
4
O
2
60.0
695
118 1.049
44
Acetone C
3
H
6
O 58.1 553
56
0.790
556
n
-Amyl alcohol,
n
-Pentanol C
5
H
12
O 88.1
595
137 0.814
11
Benzene C
6
H
6
78.1 548
80 0.877
236
n
-Butanol, tert. Butanol
C
4
H
10
O 74.1
620
118 0.810
25
(2-Methyl-2-Propanol) C
4
H
10
O 74.1
590
82
0.789
130
Carbon tetrachloride
CCI
4
153.8 226
77 1.594
271
Chlorobenzene C
6
H
5
CI 112.6 377
132
1.106
36
Chloroform CHCI
3
119.4 264
62
1.483
474
Cyclohexane C
6
H
12
84.0 389
81 0.779
235
Diethyl ether
C
4
H
10
O 74.0
389
35
0.714
850
1,2,-Dichlorethane C
2
H
4
CI
2
99.0
335
84
1.235
210
cis
-1,2,-Dichlorethylene C
2
H
2
CI
2
97.0
322
60
1.284
479
trans
-1,2,-Dichlorethylene C
2
H
2
CI
2
97.0
314
48
1.257
751
Diisopropyl ether
C
6
H
14
O 102.0
318
68
0.724
375
Dioxane C
4
H
8
O
2
88.1
406
101 1.034
107
DMF (Dimethylformamide)
C
3
H
7
NO 73.1
153
0.949
11
Ethanol C
2
H
6
O 46.0 879
79
0.789
175
Ethyl acetate
C
4
H
8
O
2
88.1
394
77
0.900
240
Heptane C
7
H
16
100.2 373
98
0.684
120
Hexane C
6
H
14
86.2 368
69 0.660
335
Isoamyl alcohol, 3-Methyl-1-butanol
C
5
H
12
O 88.1
595
129 0.809
14
Isopropyl alcohol
C
3
H
8
O 60.1 699
82
0.786
137
Methanol CH
4
O 32.0 1227
65 0.791
337
Methylene chloride, Dichloromethane
CH
2
CI
2
84.9 373
40
1.327
850
Methylethylketon C
4
H
8
O 72.1 473
80
0.805
243
Pentachlorethane C
2
HCI
5
202.3 201
162
1.680
13
Pentane C
5
H
12
72.1 381
36 0.626
850
n
-Propyl alcohol
C
3
H
8
O 60.1 787
97
0.804
67
1,1,2,2,-Tetrachloroethane C
2
H
2
CI
4
167.9
247
146
1.595
35
Tetrachloroethylene C
2
CI
4
165.8 234
121 1.623
53
THF (Tetrahydrofurane)
C
4
H
8
O 72.1
67
0.889
357
Toluol C
7
H
8
92.2 427 111 0.867
77
1,1,1,-Trichlorethane C
2
H
3
CI
3
133.4
251
74
1.339
300
Trichlorethylene C
2
HCI
3
131.3 264
87
1.464
183
Water H
2
O 18.0 2261 100 1.000
72
Xylol (Mixture)
C
8
H
10
106.2 389
25
(o)
144
0.880
(m)
139
0.864
(p)
138
0.861
Table 5.1: Table of Solvents (CRC Handbook, 65th Ed)