Buchi Lyovapor L-300, Руководство по эксплуатации

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Büchi Labortechnik AG Table of contents
Operation Manual Lyovapor™ L-300/L-300 Pro v
7 Operating Pro control panel ............................................................................................. 52
7.1 Layout of Pro control panel.................................................................................................. 52
7.2 Function bar......................................................................................................................... 52
7.3 Other symbols on the control panel..................................................................................... 54
7.4 Menu bar ............................................................................................................................. 54
7.4.1
Start menu .............................................................................................................. 54
7.4.2 Favourites menu..................................................................................................... 55
7.4.3 Method menu.......................................................................................................... 55
7.4.4 Configuration menu ................................................................................................ 55
7.4.5 Messages menu ..................................................................................................... 61
7.5 Status bar ............................................................................................................................ 62
7.6 Editing a method.................................................................................................................. 64
7.6.1
Creating a new method .......................................................................................... 64
7.6.2 Changing the name of a method ............................................................................ 64
7.6.3 Setting the sample collapse temperature ............................................................... 65
7.6.4 Setting the gas type................................................................................................ 65
7.6.5 Setting the shelf loading temperature..................................................................... 65
7.6.6 Setting the steps of a method................................................................................. 66
7.6.7 Setting the phases of a method.............................................................................. 67
7.7 Deleting a method ............................................................................................................... 69
7.8 Setting end point definitions ................................................................................................ 69
7.8.1
Pressure difference test.......................................................................................... 70
7.8.2 Temperature difference test ................................................................................... 71
7.8.3 Pressure rise test.................................................................................................... 72
7.9 Performing freeze-drying using a method [Pro control panel] ............................................. 74
7.9.1
Preparing the instrument ........................................................................................ 74
7.9.2 Selecting a method................................................................................................. 74
7.9.3 Starting freeze-drying ............................................................................................. 75
7.9.4 Changing parameters while the process is running................................................ 76
7.9.5 Ending freeze-drying .............................................................................................. 76
7.9.6 Shutting down the instrument ................................................................................. 76
7.9.7 Switching off the instrument ................................................................................... 77
7.10 Performing freeze-drying manually [Pro control panel] ....................................................... 77
7.10.1 Preparing the instrument ........................................................................................ 77
7.10.2 Starting freeze-drying ............................................................................................. 77
7.10.3 Editing parameters while the process is running .................................................... 78
7.10.4 End point definition ................................................................................................. 78
7.10.5 Ending freeze-drying .............................................................................................. 79
7.10.6 Shutting down the instrument ................................................................................. 79
7.10.7 Switching off the instrument ................................................................................... 80
8 Operating top-mount drying racks .................................................................................. 81
8.1 Operating stoppering acrylic drying chamber ...................................................................... 81
8.2 Operating manifold acrylic drying chamber (heatable shelves)........................................... 84
8.3 Operating manifold acrylic drying chamber (non-heatable shelf) ........................................ 87
8.4 Operating acrylic drying chamber (heatable shelf) .............................................................. 90
8.5 Operating acrylic drying chamber (non-heatable shelf)....................................................... 92
8.6 Operating manifold drying rack............................................................................................ 94
8.7 Determining the number of flasks........................................................................................ 96
8.8 Operating manifold valves ................................................................................................... 96