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12 | Help with faults

BÜCHI Labortechnik AG

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Operation Manual FatExtractor E-500

Problem

Possible cause

Action

Loss of solvent

Seals wrong, deformed or
damaged

Exchange the seals.

Incorrect positioning of the
beaker/ glassware and seals

Move each condenser a
small distance forward and
backward.

Check that the sealings
are correctly installed.

Contact BUCHI Costumer
Service.

Not sufficient cooling

Make sure that the cooling
fits the requirements. See
Chapter 3.5 "Technical
data", page 22

Incorrect installed solvent col-
lector circuit

Make sure that the solvent
collector circuit is correctly
installed. See Chapter 5.7
"Connecting the coolant
tubes to the condenser
tank bottle", page 30 and
Chapter 5.6 "Connecting
the solvent tubes to the
condenser tank bottle",
page 29

Incorrect installed extraction
glass chamber

Make sure that the extrac-
tion glass chamber is cor-
rectly installed. See Chap-
ter 5.9.2 "Preparing the ex-
traction glass chamber
Soxhlet", page 31

Boiling retardation

Incorrect positioning of the
beaker

Make sure that the beakers
are correctly installed in
the beaker brackets and
on the heating plate.

Too long waiting time between
preparation of the instrument
and start

Start the instrument quickly
after solvent was added

Boiling surface of the beaker
is dirty

Clean the beaker

Boiling surface of the beaker
is worn

Replace the beaker

Содержание FatExtractor E-500

Страница 1: ...FatExtractor E 500 Operation Manual 11593950 B en...

Страница 2: ...ight to make changes to the manual as deemed necessary in the light of experi ence especially with respect to structure illustrations and technical details This manual is copyrighted Information from...

Страница 3: ...leakages during extraction process 12 2 6 9 Incorrect function of the Analyte Protection Sensors 13 2 6 10 Traces of dark extracts or residuals of extract foam 13 2 7 Personal protective equipment 13...

Страница 4: ...nomic Continuous Extraction 34 5 11 2 Preparing the extraction glass chamber for an Economic Continuous Extraction 34 5 11 3 Installing the extraction glass chamber Economic Continuous Extraction 34 5...

Страница 5: ...Performing a Soxhlet Extraction 63 9 3 1 Adjusting the optical sensor on the extraction glass chamber Soxhlet 63 9 3 2 Preparing the instrument for a Soxhlet Extraction 63 9 3 3 Selecting a method 63...

Страница 6: ...ith faults 77 12 1 Troubleshooting 77 12 2 Draining solvent from Extraction glass chamber Soxhlet only 79 13 Taking out of service and disposal 80 13 1 Taking out of service 80 13 2 Disposal 80 13 3 R...

Страница 7: ...chi com contact 1 1 Warning notices in this document Warning notices warn you of dangers that can occur when handling the device There are four danger levels each identifiable by the signal word used...

Страница 8: ...the result of a correctly carried out instruction Mark up Explanation Window Software Windows are marked up like this Tab Tabs are marked up like this Dialog Dialogs are marked up like this Button Bu...

Страница 9: ...ion safe apparatus Processing samples which could be caused to explode or ignite by impact friction heat or sparks e g explosives Use of the instrument with samples that react with solvent Use of the...

Страница 10: ...these operating instructions The staff must comply with the local applicable requirements and regulations for safe and hazard conscious working practices Safety related incidents that occur while usin...

Страница 11: ...s or else wear suitable protective gloves 2 6 2 Empty beakers on heating plates Empty beakers on active heating plates lead to very hot surfaces and can damage the instrument and the beakers u Remove...

Страница 12: ...s the ambient 2 6 6 Overfilled extraction beakers Overfilled extraction beakers can cause spills and lead to instrument damage or fire u Do not fill more than 175 mL in the extraction beakers u Do not...

Страница 13: ...oning of the analyte protection sensor 2 7 Personal protective equipment Depending on the application hazards due to heat and or corrosive chemicals may arise u Always wear appropriate personal protec...

Страница 14: ...beaker contains the solvent The solvent is heated vapor rises up to the condenser con denses and drops into the extraction chamber with the sample The magnetic valve is closed the solvent is collected...

Страница 15: ...or rises up to the condenser con denses and flows into tank The analyte remains in the beaker 3 1 3 Economic Continuous Extraction Step 1 Extraction The sample is located in the extraction chamber The...

Страница 16: ...X X Dry step X X with SmartDrying See Chapter 8 11 Setting SmartDrying Soxhlet and Economic Continuous Extraction only page 58 3 2 Configuration 3 2 1 Front view 4 5 11 10 1 2 3 6 7 8 9 Fig 2 Front vi...

Страница 17: ...Chapter 3 2 3 Upper connec tions on the rear side page 17 2 Lower connections See Chapter 3 2 4 Lower connec tions on the rear side page 18 3 2 3 Upper connections on the rear side 1 2 3 4 Fig 4 Conn...

Страница 18: ...onnections on the buttom 1 Coolant water solvent tank in marked IN 2 Solvent in marked TANK IN 3 Fuse 4 Power supply connection 5 Fuse 6 Inert gas connection option marked INERT 7 Coolant water out ma...

Страница 19: ...Condenser rack Soxhlet Extraction 3 For UniversalExtractor E 800 4 Chamber rack Soxhlet Extraction 5 Condenser rack Economic Continu ous Extraction 6 Condenser rack Hot Extraction 7 Chamber rack Econ...

Страница 20: ...3 Product description B CHI Labortechnik AG 20 88 Operation Manual FatExtractor E 500 3 2 6 Interface 1 2 3 4 Fig 7 Interface 1 Stop button 2 Screen 3 Function buttons 4 Navigation control...

Страница 21: ...on Manual FatExtractor E 500 21 88 3 2 7 Pro Interface 1 2 3 Fig 8 Interface Pro 1 Stop button 2 Touch screen display 3 Navigation control 3 3 Type plate The type plate identifies the instrument The t...

Страница 22: ...nd address 3 4 Scope of delivery NOTE The scope of delivery depends of the configuration of the purchase order Accessories are delivered as per the purchase order order confirmation and deliv ery note...

Страница 23: ...dium below boiling point solvent Number of extraction positions 6 Solvent tank volume 2 L Max working volumes Extraction glass chamber Soxhlet 120 mL Max working volumes Extraction glass chamber Soxhl...

Страница 24: ...sing linearly to 50 relative hu midity at 40 C Storage temperature max 45 C 3 5 3 Materials Component Materials of construction Housing Steel 1 4301 304 with powder coating Exhaust Aluminium PE UHMW 1...

Страница 25: ...he carrier u Keep packaging for future transportation 4 2 Storage u Make sure that the ambient conditions are complied with see Chapter 3 5 Tech nical data page 22 u Wherever possible store the device...

Страница 26: ...B CHI Labortechnik AG 26 88 Operation Manual FatExtractor E 500 Fig 10 Lifting the instrument u Lift the instrument this requires two persons each lifting at the points indicated on the left and right...

Страница 27: ...ument to any external thermal loads such as direct solar radiation or other ignition source Do not place any flammable devices or substances close to the instrument as they could ignite due to the hea...

Страница 28: ...upply cables make sure that they match the specifica tions on the type plate u Make sure that all connected devices are grounded u Make sure that the power plug is freely accessible at all times u Ins...

Страница 29: ...lace with a hose clip 5 6 Connecting the solvent tubes to the condenser tank bottle Precondition R Make sure that the instrument is not con nected to the power supply u Attach the inlet tube onto the...

Страница 30: ...drain tube onto the connection marked CW TANK IN u Attach the drain tube in place with a hose clip u Attach the inlet tube onto the connection marked CW IN u Attach the drain tube onto the connection...

Страница 31: ...32 u Install the protection shields See Chapter 5 12 1 Installing two protec tion shields Soxhlet only page 35 u Select the Soxhlet method on the interface See Chapter 5 14 Selecting a configuration...

Страница 32: ...led extraction glass chamber can cause glass breakage u Install the extraction glass chamber according to following instructions u Prepare the extraction glass chamber Soxhlet See Chapter 5 9 2 Prepar...

Страница 33: ...tion board u Push the chamber rack in the instrument 5 10 Preparing the instrument for Hot Extraction 5 10 1 Installations for Hot Extraction u Prepare the condenser See Chapter 5 13 Preparing the con...

Страница 34: ...ee Chapter 5 12 2 Installing one protec tion shield Hot and Economic Continuous Extraction only page 36 u Select the Economic Continuous Extraction method on the interface See Chapter 5 14 Selecting a...

Страница 35: ...instrument 5 12 Installing the protection shields 5 12 1 Installing two protection shields Soxhlet only u Make sure that both protections shields fit to gether u Hold both protection shields on both s...

Страница 36: ...inuous Extraction only u Hold the protection shield on both sides at the point indicated NOTICE An incorrectly installed protection shield causes an error message on the inter face u Put the protectio...

Страница 37: ...r E 500 37 88 u Put the sealing on the bottom of the con denser u Attach the solvent connection nut with the seal to the condenser u Connect the solvent collector tube NOTICE Do not use force to carry...

Страница 38: ...actor E 500 u Secure the condenser with the flange lock u Turn the condenser u Connect the solvent collector tube to the in stallation board u Attach the tubes with the attachment clip to the installa...

Страница 39: ...to the Settings submenu via the navigation path u Tap the action Select configuration The display shows a dialog with the selectable configurations u Tap the configuration according to the installed...

Страница 40: ...settings on the internet gate way TCP HTTPS traffics through remote port 443 u In order to use the BUCHI Cloud a DNS server must be configured on the instru ment NOTE If there is no DNS server availa...

Страница 41: ...B CHI Labortechnik AG Installation 5 Operation Manual FatExtractor E 500 41 88 Navigation path Settings Network u Navigate to the action Network u Enable the function DHCP The instrument is prepared...

Страница 42: ...ettings submenus or actions depending on current operation 4 Function bar Shows functions that can be performed ac cording to the current operation 5 Function buttons Pressing a function button perfor...

Страница 43: ...The lift moves down UP Up The lift moves up COPY Copy Copies the selected method SKIP Skip Skips the actual extraction step VIEW View Shows the parameters of the run ning extraction ABORT Abort Aborts...

Страница 44: ...hoice of display lan guage on the interface The following languages are avail able English German French Italian Spanish Japanese Chinese Russian Polish Beeper Off On Setting for audible signal in re...

Страница 45: ...s Subnet mask Gateway Delete app con nection Confirmation question Resets external connections to the instrument Demo Mode On Off Simulate an extraction Submenu Service WARNING Incorrect use of the ac...

Страница 46: ...r On Off Chiller On Off option Submenu System information The submenu System information contains details of the connected devices and in formation on network connection diagnosis Action Option Explan...

Страница 47: ...with the instrument Time of extraction View Shows the time the instrument per formed extractions 6 3 4 Solvent menu The solvent menu contains the available solvents for the extraction methods The solv...

Страница 48: ...atus bar Shows the currently used solvent and extrac tion method 2 Menu bar Shows symbols representing the menus 3 Content area Shows current settings submenus or actions depending on the current oper...

Страница 49: ...tion con trol START Start Starts the extraction process STOP Stop Aborts extraction on all extraction positions QR Code QR Code The display shows a QR Code which contains the data of all extraction pa...

Страница 50: ...3 Status 4 Extraction cycles Soxhlet Extraction only 5 Extraction position 6 Extraction time and heating level 7 Rinse time and heating level 8 Drying time and heating level 9 Control buttons On the h...

Страница 51: ...ontrols Display brightness Enter setting Display brightness level in 0 100 Configuration Choice of extraction method The following configurations are available SOX Soxhlet Extraction HE Hot Extraction...

Страница 52: ...shield Valves Lift current Line voltage Line frequency Actors Change settings The following settings can be changed Valves Soxhlet valves See Chapter 11 4 Draining solvent from Extraction glass chamb...

Страница 53: ...Submenu History QR code Shows the history list of the data export QR codes to export data SeeChapter 9 6 Exporting extraction parameters page 70 Submenu Data use Action Option Explanation Number of ex...

Страница 54: ...the view Method u Tap the function Save on the function bar The method is saved 8 2 Changing the name of a method Navigation path u Navigate to the Method menu via the navigation path u Tap the name o...

Страница 55: ...path u Tap the name of the method that you wish to edit The display shows the view Method u Tap the function Edit on the function bar u Select the action Extraction time with the navigation control u...

Страница 56: ...g levels u Adjust the heating level to compensate the ambient conditions Navigation path u Navigate to the Method menu via the navigation path u Tap the name of the method that you wish to edit The di...

Страница 57: ...he function OK on the function bar u Tap the function Save on the function bar The Soxhlet valve open time is saved 8 8 Setting the rinse time of a method Soxhlet and Hot Extraction only Enter the dur...

Страница 58: ...heating level is saved 8 10 Setting the number of drains for a method Hot Extraction only During each drain 3 4 mL of solvent is drained into the solvent tank The level in the beaker is lowered to fin...

Страница 59: ...t drying step settings can damage the analyte and the beaker u Changing the default settings is at your own risk The duration of the drying time of a method depends on the solvent volume Navigation pa...

Страница 60: ...the ambient conditions Navigation path u Navigate to the Method menu via the navigation path u Tap the name of the method that you wish to edit The display shows the view Method u Tap the function Ed...

Страница 61: ...age 62 Adding solvent through the condenser with a dispenser CAUTION Not correctly installed condenser A not correctly installed condenser can cause skin burns or a building fire u A beaker is placed...

Страница 62: ...s placed under the position u An extraction glass chamber is installed at the position Soxhlet and Economic Continuous Extraction only u The lift is in the lower position u Put a funnel on the condens...

Страница 63: ...econdition R All commissioning operations have been completed See Chapter 5 Installation page 27 R Make sure that the configuration Soxhlet Extraction is selected See Chapter 5 14 Selecting a configur...

Страница 64: ...5 Starting a Soxhlet Extraction NOTE Boiling retardation 4 The beakers contain an integrated boiling surface No boiling aids are needed NOTE As an alternative fill the solvent at the beginning of an e...

Страница 65: ...raction WARNING Risk of dangerous vapors hot parts and hot glassware A hot instrument can cause building fire skin burns or death u Wait 15 min before opening the lift u Do not touch hot parts or surf...

Страница 66: ...lecting a method Navigation path u Navigate to the Home menu via the navigation path u Tap the method The display shows a dialog with the selectable methods u Select the method you wish to use u Tap t...

Страница 67: ...on path u Tap the function Down on the function bar The lift moves down u Wait until the lift is in the lower position u Make sure that all components of the glass setup are aligned Testing procedure...

Страница 68: ...for an Economic Continuous Extraction Precondition R All commissioning operations have been completed See Chapter 5 Installation page 27 R Make sure that the configuration Economic Continuous Extract...

Страница 69: ...are needed NOTE As an alternative fill the solvent at the beginning of an extraction through the con denser See Chapter 9 1 1 Adding solvent through the condenser page 61 Navigation path Precondition...

Страница 70: ...e menu is showing the status Finished R The instrument temperature is less than 150 C u Tap the function Up on the function bar The lift moves up u Open the protection shield u Remove the beaker for f...

Страница 71: ...a QR code u Scan the QR code on the display with the camera function of the App 9 6 2 Exporting extraction parameters with cloud connection Precondition R The App is installed on a mobile device R An...

Страница 72: ...ion path u Tap the submenu Create own The new solvent is created 10 2 Changing the name of a solvent own created solvents only Navigation path u Navigate to the Solvent menu via the navigation path u...

Страница 73: ...eets the requirements of the safety data sheets for the chemicals used 4 Make sure that the cleaning agent is compatible with the materials used See Chapter 3 5 Technical data page 22 4 If you have an...

Страница 74: ...ymbols on the instrument are legible u If they are dirty clean them Weekly Protection shields NOTICE Do not use Acetone u Wipe down the protection shields with a damp cloth u Make sure that they click...

Страница 75: ...Chapter 11 3 3 Switch of the pump page 76 11 3 1 Switch on the pump Navigation path Service Actors Precondition R A tank bottle is installed See Chapter 5 8 Preparing the tank bottle page 30 u Naviga...

Страница 76: ...lass chamber Soxhlet only Navigation path Service Actors Valves Precondition R Solvent remains in the extraction glass chamber R The lift is in the lower position R The instrument has ambient temperat...

Страница 77: ...Make sure that the power supply is connected and switched on Method cannot be started Solvent tank is full u Empty the solvent tank Protection shield is open u Close the protection shield Method stops...

Страница 78: ...rcuit is correctly installed See Chapter 5 7 Connecting the coolant tubes to the condenser tank bottle page 30 and Chapter 5 6 Connecting the solvent tubes to the condenser tank bottle page 29 Incorre...

Страница 79: ...nic solvent for extraction u Stick to the standard appli cation parameters Sand Celite layers mixed up u Clean the extraction cham bers 12 2 Draining solvent from Extraction glass chamber Soxhlet only...

Страница 80: ...tubing and communication cables from the device 13 2 Disposal The operator is responsible for proper disposal of the instrument u When disposing of equipment observe the local regulations and statuto...

Страница 81: ...ics 14 1 1 Condenser circuit Condenser Condenser Condenser Condenser Condenser Condenser Connection CW IN Connection CW OUT Flow meter inside instrument Connection CW Tank OUT Connection CW Tank IN Co...

Страница 82: ...ank IN Condenser solvent tank IN solvent Condenser solvent tank OUT Fig 17 Solvent circuit 14 2 Spare parts and accessories Use only genuine BUCHI consumables and spare parts in order to ensure correc...

Страница 83: ...063 Condenser flange E 500 11067817 Condenser tank bottle 11065966 Tank adapter PTFE 11064590 Tank bottle 2 L GL 45 11065983 Set of gliding elements including magnets 10 pcs 11067827 Soxhlet assembly...

Страница 84: ...r brackets HE 2 x 11067829 set of draining tubes for HE 11067480 beaker carrier cover for HE 11068487 Conversion kit from Soxhlet Universal to ECE Includes 6 Extraction glass chamber ECE 11062499 set...

Страница 85: ...bes PTFE 11067220 Holder for extraction thimbles diameter 25 43 mm 11068443 Extraction beaker carrier Allows to carry 6 beakers 11067474 11067042 Extraction beaker HE carrier Allows to carry 6 beakers...

Страница 86: ...or extraction thimbles Order no Set of holders for glass sample tubes with frit PTFE 3 pcs 11067485 Set of holders for LSV glass sample tubes PTFE 3 pcs 11067486 Holders for thimbles d25 PTFE 3 pcs 11...

Страница 87: ...for FatExtractor E 500 Installation Operation qualification for the FatExtractor E 500 incl binder with documents IQ OQ inspection and basic tag English 11068557 Repeating OQ for FatExtractor E 500 Re...

Страница 88: ...n zh India BUCHI India Private Ltd IN Mumbai 400 055 T 91 22 667 75400 F 91 22 667 18986 india buchi com www buchi com in en Indonesia PT BUCHI Indonesia ID Tangerang 15321 T 62 21 537 62 16 F 62 21 5...

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