Buchi B-820, Руководство пользователя

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32
BÜCHI Fat Determination B-820/B-821
Version: 3.00af Gas supply on?
User: C.Heiter Press <ENTER> to cont.
C13 : 285 C20 : 1095
C16 : 516 C22 : 1408
C18 : 768 C24 : 1687
S W I T Z E R L A N D
Preheating p H2 55kPa
Sample weight/Mode p air 50kPa
Determination T oven 130°C
Data manager T inj. 220°C
Setup T FID 260°C
Sample no: 5 p H2 55kPa
Vial no: 5 p air 50kPa
Switch off: yes T oven 140°C
Start after 62s T inj. 220°C
Main menu T FID 260°C
gen.corr.
Name: coconut oil
Manual sample weight
Automatic sample weight
Factors
Main menu
Stop p H2 55kPa
Main menu p air 50kPa
T oven 260°C
T inj. 220°C
T FID 260°C
Remaining time 1215s
Time: 2400s p H2 55kPa
Start preheating p air 50kPa
Main menu T oven 130°C
T inj. 220°C
T FID 260°C
Determination with autosampler
Determination without autosampler
Sample no: 5 p H2 55kPa
Next number p air: p air 50kPa
T oven 130°C
T inj. 220°C
Main menu T FID 260°C
Ready injection 2 gen.corr.
Name: coconut oil
5 Operation
Manual sample weight
Automatic sample weight
Factors
Calibration
Main menu
Determination "Fatty Acids"
Determination "Total fat"
No Mode Weihgt Weight Weight Conc.
[g] C13[g] C5[g] [%]
1 fact.gen. 0.7055 0.2115 99.8
Name: Factor
2 fact.b.a. 0.055 0.054 99.5
Name: Factor C4
3 but. acid 0.8550 0.2134 0.056
Name: butter
4 gen.corr. 4.3575 0.1245
Name: wheat
5 spec.corr
.
2.3654 0.2056
Name: cheese
"Table of factors"
Factor Fat: 0.953
Factor butyric acid: 1.123
CF: 28.570
Blank value but.acid 0.0031g
Main menu
No Mode Weight Weight Conc.
[g] C13[g] [%]
1 FA-calib.
Name: Calibration
2 FA-factor 0.7133 0.2078 99.7
Name: Factor
3 FA-det. 2.1351 0.2132
Name: milk powder
Factor fatty acids: 1.053
Main menu