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Appendix B: Measuring Special Samples

118

C76IB003EN-E

B.2

Special Filling Techniques

Bubbling samples

If the sample to be measured tends to form gas bubbles, degas it before the

measurement (see Appendix B.1).

If this is not possible, introduce the sample at a temperature higher than the

measuring temperature.

You can also put the density meter at a slight angle by means of proper spacers

below the right side of the DMA M to allow the bubbles to escape due to buoyancy.

Suspensions and emulsions

Suspensions or emulsions may tend to separate in the measuring cells, giving

incorrect results. Leave such samples in the measuring cell as briefly as possible.

Prethermostat them before filling.

It may help to put spacers below the left legs of DMA M, thus putting it at an angle

to counterbalance the separation force generated by the oscillation of the

measuring cell.

Highly viscous samples

Highly viscous samples can be heated up to lower the viscosity. Always heat the

sample to a temperature that is approx. 15 °C higher than the measuring

temperature, which can be 90 °C maximum.

Pastes

Paste-like materials like toothpaste or tomato ketchup can be filled by syringe.

Inject these kinds of samples into the measuring cell by pushing the plunger very

slowly and continuously.

If the samples have a very high viscosity, you can fill them into the syringe by

pulling the plunger completely out of the syringe, filling it from the back using a

spoon and then mounting the plunger again.

Liquids in aerosol cans

For the quality control of aerosol cans, you can use the Anton Paar Aerosol

Adapter (Mat. No. 74650) to fill the liquid safely and conveniently into your

DMA M. For details, see the Aerosol Adapter instruction manual.

Gases

It is possible to measure gases with the DMA M. For details, contact your local

Anton Paar representative and ask for the respective application report and the

necessary accessories.

Содержание DMA 4100 M

Страница 1: ... EASURE WHAT IS MEASURABLE AND MAKE MEASURABLE THAT WHICH IS NOT ALILEO ALILEI Instruction Manual DMA 4100 M DMA 4500 M DMA 5000 M Firmware Version V2 21 ...

Страница 2: ......

Страница 3: ...Instruction Manual DMA 4100 M DMA 4500 M DMA 5000 M Firmware Version V2 21 ...

Страница 4: ...d changed copied or distributed by means of electronic systems in any form print photocopy microfilm or any other process without prior written permission by Anton Paar GmbH Trademarks registered trademarks trade names etc may be used in this manual without being marked as such They are the property of their respective owner Published by Anton Paar Printed Anton Paar Austria Copyright 2012 Anton P...

Страница 5: ...g the Instrument On Off 27 7 6 Instrument Settings and First Checks 27 8 Operating the Instrument 28 8 1 Input Alternatives 28 8 2 Using the External Keyboard 28 8 3 Using the Touch Screen 29 8 4 Calibrating the Touch Screen 33 8 5 Setting the Screen Saver 33 8 6 Activating Deactivating the Feedback Beeps 34 8 7 Logging On Off 34 8 8 Using Favorites 35 9 Installing Optional Input Output Devices 37...

Страница 6: ...Data 53 11 3 Adjustments 54 11 3 1 Performing an Air Water Adjustment 54 11 3 2 Performing a Temperature Range Adjustment 55 11 3 3 Performing a High Density High Viscosity Adjustment DMA 5000 M only 56 11 3 4 Performing an Atmospheric Pressure Adjustment 56 11 3 5 Performing Special Adjustments 57 11 3 5 1 Special Adjustments 57 11 3 5 2 Special Adjustment for the Canadian Excise Alcohol Table 59...

Страница 7: ... 5 Viewing Statistics 87 15 6 Printing and Exporting Results and Other Data 88 15 7 Deleting Results 89 16 Using Special Functions 90 16 1 System Security 90 16 1 1 Security Level 90 16 1 2 Auto Logoff and Password Expiry 91 16 1 3 Increased Security 91 16 1 4 Audit Trail 92 16 1 5 Electronic Signature 94 16 2 User Functions Constants Formulas Polynomials and Tables 96 16 3 Calculator 101 16 4 Gro...

Страница 8: ... Measuring at Low High Temperatures 121 C 3 Measuring at High Pressures 122 C 4 Measuring in Harsh Environments 122 Appendix D Adjusting the Camera Settings 124 D 1 Adjusting the Camera Position 124 D 2 Setting the Camera Illumination 124 Appendix E Trouble Shooting 125 Appendix F List of Output Quantities 128 Appendix G List of Quick Settings Parameters 134 Appendix H Bar Codes for Assigning Meth...

Страница 9: ...or revisions to this instruction manual from Anton Paar GmbH these must be treated as part of the instruction manual Conventions for safety messages The following conventions for safety messages are used in this instruction manual TIP Tip gives extra information about the situation at hand DANGER Danger indicates a hazardous situation which if not avoided will result in death or serious injury WAR...

Страница 10: ...he proper functioning of DMA 4100 4500 5000 M if no adjustments have been made to the mechanics electronics and firmware Only use DMA 4100 4500 5000 M for the purpose described in this instruction manual Anton Paar GmbH is not liable for damages caused by incorrect use of DMA 4100 4500 5000 M The results delivered by DMA 4100 4500 5000 M not only depend on the correct functioning of the instrument...

Страница 11: ... Make sure that all hoses and the measuring cell are empty before you move or lift DMA 4100 4500 5000 M To move or lift DMA 4100 4500 5000 M place one hand at the back and grip the ledge at the top Place the other hand at the front under the display There is a hollow for your fingers When carrying the system keep it close to your body Handling of chemicals Observe all safety regulations regarding ...

Страница 12: ...eir containers uncovered Immediately remove spilled sample cleaning agents Make sure that the setup location is sufficiently ventilated The environment of DMA 4100 4500 5000 M must be kept free of flammable gases and vapors Connect DMA 4100 4500 5000 M to the mains via a safety switch located at a safe distance from the instrument In an emergency turn off the power using this switch instead of the...

Страница 13: ...U tube and the reference oscillator Concentration measurement In binary mixtures the density of the mixture is a function of its composition Thus by using density concentration tables the density value of a binary mixture can be used to calculate its composition This is also possible with so called quasi binary mixtures These are mixtures containing two major components and some additional compone...

Страница 14: ...res and Benefits Accuracy Your DMA M series instrument is equipped with the world s most advanced digital density measurement technology The period of oscillation of the U tube is measured by optical pickups Two integrated Pt 100 platinum thermometers together with Peltier elements provide an extremely precise thermostatting of the sample ThermoBalanceTM An additional reference oscillator provides...

Страница 15: ...sity values are automatically converted into concentration values for a large number of factory programmed substances You can also program special substances as required Under harsh industrial conditions operate the DMA M with the set of robust softkeys instead of the touch screen You can operate the DMA M via external keyboard computer mouse or bar code reader You can connect an external terminal...

Страница 16: ...transport 1 Keep the packaging material box foam piece transport protection for possible returns and further questions from the transport and insurance company 2 Check the delivery for completion by comparing the supplied parts to those noted in Table 5 1 3 If a part is missing contact your Anton Paar representative 4 If a part is damaged contact the transport company and your Anton Paar represent...

Страница 17: ...ertificate 96044 1 Accessory kit 70248 2 m Hose 3 x 5 mm silicone transparent 50814 7 Syringe 2 mL Luer 51974 2 Injection adapter Luer 12225 2 Male Luer plug PTFE 63865 2 Adapter Luer cone 63863 1 Screwdriver 75030 1 Waste vessel 6210 Table 5 1 Standard parts Symbol Pcs Article Description Mat No ...

Страница 18: ...sing unit Xsample 352 81338 Sample handling unit Xsample 52 81339 Heated sample changer Xsample 452 H 84806 Heated filling and rinsing unit Xsample 352 H 84808 Protection Protecting cover for keyboard 13350 Protection cap for USB interfaces 81168 Protection foils for touch screen 3 pcs 81402 Protective cover front 3 pcs 88856 Special funnel protection 82448 Special application accessories Aerosol ...

Страница 19: ...2 Color TFT touch screen 3 Power on LED 4 Inspection window for the measuring cell DMA 4100 M only 5 Xsample slot cover plate 6 Sample inlet and outlet 7 Air pump outlet 6 2 View of the Left Side Fig 6 2 View of the left side 1 Blind covers for inlet and outlet of the optional cooling kit 2 USB interfaces 3 Protection cover for the USB interfaces 1 2 3 4 5 6 7 1 2 3 ...

Страница 20: ... BUS interfaces 3 USB interface 4 VGA interface 5 Ethernet interface 6 CAN interface 7 DRY AIR IN AIR PUMP connector 8 DRY AIR IN BLOCK connector 9 Power switch 10 Fuse holder 11 Power inlet 12 Type plate with serial number 13 UL test mark 14 Fan 15 Carrying ledge 1 2 3 4 5 6 7 8 9 10 11 12 14 15 13 ...

Страница 21: ...defined in the settings of the current method and can be adapted according to your needs The progress bar at the bottom of the content area indicates whether the instrument is currently measuring or whether a measurement was finished Buttons area The buttons in this area have the following functions Menu To open the main menu Favorites To open the favorites list Quick Settings To open the quick se...

Страница 22: ...ve sample list had a filling error With red lightning sign The instrument or system has a major problem that needs to be fixed before you continue with measurements e g sample changer is blocked One or more samples of the current sample list could not be measured e g measuring cell is partly empty so that it cannot oscillate To reset the diagnosis button to the green check confirm all error messag...

Страница 23: ...o unfreeze the screen tap the button 6 5 Operating Elements of the Menu Screen To access the menu tap Menu in the main screen Fig 6 5 Menu screen example Header On the left side of the header you find the navigation path to your current position in the menu You can go back to any menu position in your current path by directly tapping on the respective box of the navigation path Content area In the...

Страница 24: ...y box 2 Pull out the black transport plastic plugs from the tip of the injection adapters WARNING Using hazardous or flammable chemicals as samples or cleaning liquids could destroy the instrument and cause serious injuries when not taking special precautions into account See the section Special precautions for flammable chemicals in Chapter 2 for information about a suitable installation place NO...

Страница 25: ...felt 7 3 Checking for Leak Tightness 1 Close one adapter tightly with a male Luer plug 2 Fill air under moderate pressure through the other adapter using a plastic syringe from the accessory box and wait for a few seconds 3 Release the plunger of the syringe If the connections are tight the plunger of the syringe will be slowly pushed back by the pressure in the measuring cell CAUTION If the screw...

Страница 26: ...ose into the hole of the closed waste vessel cap Fig 7 2 Connecting the waste hose To connect the silicone hose at the air pump outlet 1 Cut a piece of approx 250 mm 10 in length from the silicone hose contained in the accessory box 2 Attach the silicone hose to the air pump outlet 3 Attach an adapter Luer cone from the accessory box to the other end of the silicone hose WARNING Liquids leaking fr...

Страница 27: ...ir check and a water check The instrument has a factory adjustment over the whole temperature and viscosity range However during transport the density adjustment can be influenced To perform first checks 1 Wait at least 15 minutes after a reboot for the temperature to stabilize WARNING High voltage at parts of the instrument can cause serious injuries or death Only connect the instruments to the m...

Страница 28: ...m an air water adjustment see Chapter 11 3 1 8 Operating the Instrument 8 1 Input Alternatives You can Tap the elements on the touch screen Use a computer mouse and click on the elements on the touch screen Use an external keyboard to enter characters Use a bar code reader Use the softkeys below the touch screen 8 2 Using the External Keyboard To use buttons When an external keyboard is connected ...

Страница 29: ...rnal keyboard To navigate to the next wizard step press on your external keyboard 8 3 Using the Touch Screen In the following parts of this manual the operation of the instrument is described only for the input option touch screen To use buttons Use the buttons by directly tapping on them The buttons at the bottom of the screen can also be activated with the softkeys below them To highlight items ...

Страница 30: ...p down list 2 Tap OK to select the entry and close the list Fig 8 2 Example Drop down box and check box in the Edit Printer wizard menu Setup Control Panel Printer Management To use check boxes Tap on the check box to activate or deactivate the desired function see Fig 8 2 To use radio buttons Choose one of the radio buttons to activate one of the available functions Drop down box Check box ...

Страница 31: ...surement System Settings Camera To enter characters into an input box or list field 1 There are two ways to open the on screen keyboard Tap on the input box or list field twice to open the on screen keyboard Tap the A symbol within the input box or list field see Fig 8 4 Fig 8 4 Input field of the sample list ...

Страница 32: ...ions to exit a dialog window To get directly to the main screen tap Main Screen and decide whether you want to save or discard changes in the following pop up window To get one menu level higher and save changes tap OK To get one menu level higher without saving changes tap Cancel Deletes the character on the left side of the cursor position Moves the cursor position to the left to the right Chang...

Страница 33: ...ving tap Main Screen and in the following dialog select the option Yes Fig 8 6 Edit Report wizard 8 4 Calibrating the Touch Screen If you have difficulties in hitting the touch screen user elements buttons drop down boxes etc you can calibrate the touch screen The touch screen sensors will then be adapted to the way you tap on the screen 1 Tap Menu and select Setup Control Panel Calibrate Touch Sc...

Страница 34: ...k Beeps If both feedback beep functions are activated the instrument beeps upon every successful touch screen or softkey action mouse click and bar code reader input as well as after the completion of a measurement 1 Tap Menu and select Setup Control Panel Feedback Beeps 2 Activate deactivate the feedback beep option for beeping when a screen item or key is touched 3 Activate deactivate the feedba...

Страница 35: ...nts Chapter 10 4 2 8 8 Using Favorites The favorites function enables you to quickly access your favorite menu dialogs directly from the main screen You can also use the favorites function to activate your favorite menu dialogs without touching the touch screen by using the softkeys below the touch screen The favorites list is the same for all users To add a dialog window to the favorites list 1 O...

Страница 36: ... the position of the list item in the favorites list 3 Proceed so with all other list items whose position you want to change and tap OK To rename a favorites list item 1 Tap Menu and select Setup Favorites Management 2 Highlight the list item and tap Rename 3 Enter the new favorite name and tap OK To delete a favorites list item 1 Tap Menu and select Setup Favorites Management 2 Highlight the lis...

Страница 37: ...es or user defined data fields In the Sample List mode you can also assign methods to samples by reading the respective bar code see Appendix H for bar code examples Tested bar code readers are Symbol DS6707 or Datalogic Firescan D131 To deactivate the on screen keyboard in the sample list If you activate this function the on screen keyboard will not appear when editing the sample list You can con...

Страница 38: ...1 Connect the printer Mat No 44737 or 93362 to the RS 232 interface COM of the instrument using the cable that is supplied together with the printer 2 If you use an RS 232 printer which is not supplied by Anton Paar set the communication settings on the printer properly see Appendix A 3 To connect an office printer not supplied by Anton Paar via USB interface Connect the printer to a USB interface...

Страница 39: ...pens 3 For RS 232 printers perform the following settings Activate deactivate the check box Use as default printer Enter a Name for the printer Select the adequate printer Type 4 Tap OK 5 For USB and network printers perform the following settings Activate deactivate the check box Use as default printer Enter a Name for the printer Select the adequate printer Type Select the paper Format 6 Tap Nex...

Страница 40: ...uch Systems and compatibles are supported We recommend the model Elo 1715L 17 LCD Desktop Touchmonitor 1000 Series firmware V1 9 and higher Only order the external touch screen with IntelliTouch Surface Wave Touch Technology Connect the external touch screen to the VGA interface at the rear and to one of the USB interfaces that are located on the left and rear of the instrument TIP Connect the USB...

Страница 41: ...plays Are you sure you want change the regional settings The instrument will reboot to complete this action 3 Tap Yes to install the new settings The instrument reboots If the instrument is operated in a language or font you do not understand proceed as follows 1 Tap the leftmost button in the main screen Menu 2 Select the menu item with the symbol menu Setup 3 Select the second menu item menu Set...

Страница 42: ...are activated and the air density value gets not stable within the period of time that is defined with the second option the air pump stops nevertheless after this period of time 3 Tap OK to save the changes 10 1 5 Saving a Camera Picture DMA 4500 5000 M Only You can define when the instrument automatically saves a picture of the measuring cell 1 Tap Menu and select Setup Measuring System Settings...

Страница 43: ...Defining the Printout Settings You can define the layout of the printer report and if you want an automatic printout To set the output data for each method see Chapter 12 2 3 10 2 1 Creating Editing and Deleting Printer Report Layouts You can set up to 10 different report layouts for e g different methods different sample types or for internal or external use The layouts can be created edited or d...

Страница 44: ...he document layout the logo graphic files have to have the extension jpg or bmp be located in the root directory of the USB flash drive have a maximum size of 400 x 200 px header logo To import logos 1 Tap Menu and select Setup Printout Settings Import Logos 2 Use the drop down list Drive to select the connected USB flash drive 3 Use the drop down list File Name to select the correct file 4 Use th...

Страница 45: ... save the changes Related topics Registering Editing Deleting a Printer Chapter 9 3 2 Defining the Result Output Chapter 12 2 3 Printing and Exporting Results and Other Data Chapter 15 6 10 3 Setting Sample List Options In the Sample List menu you can Select the sample list mode Define automatic sample name additions before and after the sample name These additions will be added to each sample nam...

Страница 46: ... Quick Settings button on the main screen If a sample changer with magazine is connected you can select Simple mode or User defined mode For details see the corresponding Xsample instruction manual 3 Define the Automatic Sample Name Sample Name Prefix and Sample Name Postfix 4 Tap OK to save the changes To set user defined data fields 1 Tap Menu and select Setup Measuring System Settings Sample Li...

Страница 47: ...e written in lower case letters e g administrator is set as the password for the administrator user For the administrator user the auto logon function is activated 10 4 1 User Groups Auto Logon Naming Rules and Password Rules User groups There are three user groups which have different levels of user rights Naming rules User names must have at least one character Allowed are characters from the AS...

Страница 48: ...this user is logged on and the instrument is switched off and on again there is no logon procedure All instrument functions according to user rights of the auto logon user are freely accessible Example The user smith belongs to the user group Operator and the auto logon function is activated for him If he switches off the instrument anyone can switch the instrument on and start measuring without a...

Страница 49: ... dialog and tap OK 5 Tap OK To delete a user account You cannot delete your own account i e the currently active account or an account of a user group that has a higher level of user rights than your own account 1 Tap Menu and select Setup User Management 2 Highlight a user name on the user list and tap Delete To set or change a password If the instrument is operated in increased security mode you...

Страница 50: ...rement properties that encompass the expected measurement results of your samples for a successful adjustment Calibrating Calibrations are checking procedures which are carried out using certified standards By comparing the measured result with the standard reference value you can validate the quality of your measurements 11 2 Checks 11 2 1 Editing the Check Settings You can edit the name method c...

Страница 51: ...nt to open the check administration list 2 Tap New to open the two step Check Edit wizard 3 Perform the following settings Enter a name for the check Select the method to define detailed method settings for the check e g in the method Density Use the check box Must be started every to define if the check is obligatory and enter a time interval in days 4 Tap Next Select the quantity Define the chec...

Страница 52: ...s have to be defined for a certain method and are always performed at the temperature of the selected method with the corresponding predetermination equilibrium type of measurement Air checks and water checks are available for any method When to do water checks and custom checks Use the water check and custom check to verify that the instrument is measuring with satisfactory accuracy We recommend ...

Страница 53: ...he water check failed we recommend taking corrective actions until the check is valid again Take a look at the camera image attached to the result to check if the water was filled bubble free see Chapter 11 2 3 Check the quality of the water Clean the measuring cell thoroughly If the above mentioned actions do not help perform an air water adjustment 11 2 3 Viewing Printing or Exporting Current Ch...

Страница 54: ... is already clean and dry and equilibrated to 20 C The adjustment procedure can be aborted by tapping Cancel To perform an air water adjustment 1 Tap Menu and select Checks Adjustments Air Water Adjustment 2 Rinse the measuring cell TIP If you use undenatured ethanol as the last rinsing liquid only 3 4 minutes drying time are required 3 Tap the Air Pump on button to dry the measuring cell 4 Tap OK...

Страница 55: ... your instrument over the whole temperature range to reach the maximum accuracy for measurements at different temperatures than 20 C During the temperature range adjustment an air adjustment is performed at 40 C and 60 C then a water adjustment at 60 C and 40 C The whole adjustment takes about 30 minutes The adjustment procedure can be aborted by tapping Cancel 1 Tap Menu and select Checks Adjustm...

Страница 56: ... adjustment is performed When the adjustment is finished the following information is displayed Old Value Calculated density of water of the previous adjustment New Value Calculated density of water with the new adjustment constants Deviation Relative and absolute deviation between new and old value 3 Check the recommendation on the screen and select Special if Apply is recommended 4 For filling t...

Страница 57: ...emperatures After a successful adjustment procedure the special adjustment can be used as a standard measuring quantity that is displayed and printed It can also be used as an input parameter for a user function as the API input quantity as the input quantity for the Canadian excise alcohol table Five different special adjustments can be stored For each special adjustment name unit and temperature...

Страница 58: ... The special adjustment routine starts 5 Rinse the measuring cell 6 Press the Air Pump on button to dry the measuring cell 7 Fill the first standard into the measuring cell and tap OK Check that the standard is filled without air bubbles 8 Enter the reference value for the first standard and tap OK 9 Enter the reference value for the second standard and tap OK 10 Rinse the measuring cell 11 Press ...

Страница 59: ...nt Data Density Module and select Density Adjustment Special Adjustment or Temperature Adjustment to open the respective adjustment list 2 Highlight a list item and tap Details to see the detailed adjustment data 3 To perform a printout on paper or to a PDF file or to export the data as an MS Excel or Text file tap Print or Export and follow the instructions on the screen 11 3 7 Viewing Printing o...

Страница 60: ...cell 4 Select a measuring method that is set to 20 C and measurement finished by equilibrium For DMA 5000 M use the setting measurement finished by equilibrium slow 5 Open the bottle with the liquid density standard TIP If your bottle with density standard has a septum we recommend you pierce it carefully with any clean sharp tool and fill a Luer tip syringe with standard liquid by pushing the tip...

Страница 61: ...g Methods 12 1 Measuring Methods Each method contains the following kind of information Instrument settings Xsample settings and measuring module settings if any module is installed Layout of measuring data on the main screen Measuring units Parameter list for printout and data export You can use the factory preset methods as they are or change them to suit your needs see Chapter 12 2 You can also...

Страница 62: ...rrection Brix Concentration Sugar Density Density Temperature Density Condition U ViewTM For measurements of sugar in soft drinks Ethanol w w OIML ITS 90 Ethanol OIML ITS 90 w w Density Density Temperature Density Condition U ViewTM For measurements of alcohol concentration in distillates Ethanol v v OIML ITS 90 Ethanol OIML ITS 90 v v Density Density Temperature Density Condition U ViewTM For mea...

Страница 63: ...ccording to calculations for product group A with temperature correction to 15 C Fuel Oil API API Density 15 C Density API Specific Gravity 15 C Density Temperature API Gravity 15 C Density Condition U ViewTM For measurements of fuel oil according to calculations for product group B with temperature correction to 15 C Lubricants API API Density 15 C Density API Specific Gravity 15 C Density Temper...

Страница 64: ...e If you select Equilibrium the measurement finishes after temperature equilibrium was established DMA 5000 M With this instrument you have the choice between predetermination equilibrium fast equilibrium medium and equilibrium slow The slower the equilibrium the more accurate are the results Measuring temperature Timeout If a measurement is not finished after the specified timeout it will be abor...

Страница 65: ...Highlight a list item and tap OK To define the content of output fields You can directly change the content of output fields in the main screen The changes are automatically saved in the current method 1 Tap on the output field 2 Select the Group Quantity Unit and number of Digits and tap OK TIP Before you use the output quantity Canadian Excise Alcohol Table of the group Ethanol Tables see Append...

Страница 66: ...esult Output 2 Highlight a list item and use the up down arrows in the right column to change the position of the list item 3 Proceed so with all other list items whose position you want to change and tap OK 12 2 4 Defining Limits Limits can be set for any parameter separately e g density concentration sugar etc If any of the selected quantities is out of the limited range you will be warned with ...

Страница 67: ...er formula parameters to define how API parameters shall be determined and to define which special adjustment shall be used for the Canadian excise alcohol table API parameters are usually calculated based on true density the input quantity can be defined as Density not visc corr Density Special Adjustment 1 5 The API Product Group can be set to A crude oil B fuels or D lubes to set up measuring m...

Страница 68: ...arameters are set by default If the No Sample List mode is used Sample name measurement type Type and Density Temperature If the Sample List mode is used Measurement type and Density Temperature Additional parameters can be added to your quick settings for every method User defined data fields see Chapter 10 3 and user functions of the Constant type see Chapter 16 2 will be automatically added to ...

Страница 69: ... and delete methods The maximum number of methods is 50 To create a new method make a copy of the existing method which has the most similar method settings to the one you want to create Then rename the new method and change its method settings to your needs To copy a method 1 Tap Menu and select Methods Method Management to open the method list 2 Highlight a method name and tap Copy A new method ...

Страница 70: ...nd select Methods Method Visibility 2 Highlight a method 3 Enable the check box to set the method visible or disable the check box to set the method invisible 4 Tap OK To change the sequence of the method list 1 Tap Menu and select Methods Method Visibility 2 Highlight a method and use the up and down arrows in the Order column to change the position of the method in the list 3 Proceed so with all...

Страница 71: ...ater Check are predefined If you select MM Multiple Measurements tap the column Unit Settings and enter a value between 2 and 10 If you select TS Temperature Scan tap the column Unit Settings and enter the Start Step and End temperature of the temperature scan Make sure to set the temperature step interval so that the instrument can reach the end temperature by a whole number of steps divide the i...

Страница 72: ...e corresponding input field if needed 3 Define your parameters if needed 4 Tap OK 13 3 Using the Sample List Mode The sample list is a tool that helps you managing samples that you want to measure No results are stored in the sample list but using the Single Sample button in the sample list links you to the data memory and you can view the results of already measured samples in the sample list You...

Страница 73: ...type and measurement settings as desired 5 To exit the sample list and save the changes tap Main Screen To edit or delete a sample in the sample list TIP You cannot edit or delete samples in the sample list that have already been measured To edit a sample highlight the row and change the settings as desired To delete a sample from the list highlight the sample and tap Delete Sample To exit the sam...

Страница 74: ...e List and then OK 3 Choose one of the ten sample lists in the drop down list Sample list templates 4 Tap OK To clear the current sample list 1 Tap Sample List and then List Management 2 Select Clear Sample List After the sample list was cleared the symbol on the diagnosis quick access button may change If the symbol was the yellow alarm signal or the red lightning they will change to the green ch...

Страница 75: ...s may cause serious injuries Before filling any sample or cleaning liquid into your DMA M make sure that all safety instructions concerning the use of chemicals and the use of flammable chemicals are met see Chapter 2 make sure all wetted parts are resistant to the filled in liquid see Appendix A 2 make sure that you have suitable cleaning fluids at hand for cleaning the measuring cell see Chapter...

Страница 76: ...ton in the quick access area to open the live camera view of the measuring cell 2 Tap Zoom In to get a magnified view 3 Attach a USB flash drive and tap Save Picture to save the current picture 4 Tap X to exit the measuring cell view Fig 13 1 Camera window Bubble detection using the inspection window DMA 4100 M You can check the quality of the filling visually by looking through the inspection win...

Страница 77: ...unt another adapter Luer cone and connect it to a waste vessel using a second silicone hose 3 x 5 mm 5 Mount a valve or hose clamp at the outlet silicone hose 6 Close the valve and fill your sample into the funnel 7 Fill the measuring cell by carefully opening the valve and closing it again before the funnel runs empty To fill with a peristaltic pump 1 Mount an adapter Luer cone to the sample inle...

Страница 78: ...ing Measurements To speed up measurements Automatic sample naming See Chapter 10 3 Prethermostatting Prethermostat your samples to the measuring temperature before injection to reduce the time necessary for the temperature equilibration Predetermination option Using this option reduces the measuring time substantially see Chapter 12 2 1 To perform a measurement 1 Before starting a measurement chec...

Страница 79: ...ed and an acoustic signal is given The Density Condition output field shows the message valid The result values are frozen The display can be unfrozen by tapping the button The result values are saved in the data memory and can be viewed printed exported or deleted 5 Measure the next sample or clean and dry the measuring cell Related topics Safety Instructions Chapter 2 Mounting the Hoses Chapter ...

Страница 80: ...iagnosis quick access button changes Instead of the green check mark the yellow alarm sign is displayed Note For complete transparency and traceability of your sample filling and measurement process check the filling visually by means of the built in camera U ViewTM DMA 4500 5000 M or the inspection window DMA 4100 M in addition to the fully automatic FillingCheckTM temp equilibration Appears duri...

Страница 81: ...ts employ a regular and effective cleaning routine and store the instrument under the recommended conditions 14 1 Cleaning and Drying the Measuring Cell Cleaning frequency Clean and dry the measuring cell at least after each working day or working shift Cleaning more frequently can be necessary when you perform adjustments when you measure a sample that is not miscible with the previous sample e g...

Страница 82: ...ning liquid 2 Recommended for petrochemical samples petroleum naphtha cleaning liquid 1 and acetone cleaning liquid 2 If you are not sure if a cleaning liquid is suitable for your sample perform a preliminary test in a test tube to see if any phase separation precipitate or opalescence can be observed To perform a cleaning and drying procedure without Xsample filling equipment 1 Rinse the measurin...

Страница 83: ...ty Checks Chapter 11 2 2 Air Pump Settings Chapter 10 1 4 Measuring at High Humidity Low Temperature Conditions Appendix C 1 14 2 Storing the Instrument Clean and dry the measuring cell see Chapter 14 1 before storing the instrument for more than one day Otherwise algae may grow on the glass surface that are difficult to remove For storage for less than one day the measuring cell can be filled wit...

Страница 84: ...Expert Settings Data Memory Settings and activate the check box Automatically delete old measurement data The oldest 100 measurement results will then be automatically deleted as soon as the number of 900 measuring results has been exceeded in the data memory 15 2 Defining Data Columns for the Data Browser You can define the kind of data which shall be displayed in the data browser You can change ...

Страница 85: ...ultiple sample view you can see a number of results listed in a table In the single sample view you can see a more detailed view of one result at a time In the multiple sample view the output quantities according to the data browser settings are displayed In the single sample view the output quantities according to the result output settings are displayed If no output quantities have been selected...

Страница 86: ... Name Method only available if previously used User defined data fields Print Export Status Sample Error State User only those who performed measurements are available Magazine pos Measuring value Master Condition Quantity Camera image available Electronic Signature Comparators older than newer than equals not equal larger than smaller than containing not containing printed exported not printed ex...

Страница 87: ...e the following settings Filter criterion Date range Comparator equals Value Last Week To delete a filter 1 In the multiple sample view tap Filter to open the Filter dialog 2 Highlight the filter that you want to delete and tap Delete 15 5 Viewing Statistics Statistical numbers are always calculated according to the filter settings of the measured data in the data browser Statistical details will ...

Страница 88: ...elect Print Report Paper PDF File 2 Tap OK to open the Print Report dialog 3 Use the drop down boxes Target Report and Drive and the input box File Name to define the printout settings and tap OK Exported PDF files are password protected To export data 1 Insert a USB flash drive into a USB interface 2 Tap Print or Export and select Export Data Excel File Text File 3 Tap OK to open the File Export ...

Страница 89: ...the Result Output Chapter 12 2 3 15 7 Deleting Results We recommend deleting your result data regularly after a successful data export or printout To delete a single result 1 Tap Menu and select Data Memory Delete Measured Data 2 Highlight a row in the multiple sample view 3 Tap Single Sample and tap Delete Entry To delete several results 1 Tap Menu and select Data Memory Delete Measured Data to o...

Страница 90: ...2 To check your current settings tap Details To set the security level 1 Tap Menu and select Setup System Security Security Level 2 Use the drop down box to select a security level The user defined security level is only visible and can be selected if the user has changed any default security settings Table 16 1 Comparison of security level settings Security Level Low 21 CFR Part 11 Audit Trail Of...

Страница 91: ...ime to a time between 1 and 60 min To set password expiry You can define how long passwords are valid The setting applies to all passwords If a password expires the corresponding user account is deactivated For activating a user account and setting a password see Chapter 10 4 2 1 Tap Menu and select Setup System Security Logon Settings 2 Use the check box to activate the password expiry function 3...

Страница 92: ...e warnings which appear in the diagnosis window are documented in the audit trail Successful or rejected adjustments and passed or failed checks Resetting of adjustments to factory adjustment Exceeding of adjustment intervals and check intervals Changes of methods via settings in the density module Changes in customer functions Table 16 2 Increased security settings On Off No endless data storage ...

Страница 93: ...vate audit trail There are two ways to activate the audit trail function You can set the security level to 21 CFR Part 11 see Chapter 16 1 1 and audit trail will be activated automatically You can activate the audit trail function within your user defined security mode 1 Tap Menu and select Setup System Security Audit Trail to open the Audit Trail Settings dialog 2 Activate deactivate the audit tr...

Страница 94: ...lder select the directory where the log files the md5 file and xls or txt file are saved and click Verify sums 3 In the following dialog select the md5 file that you want to check and click Open The check status and result are displayed If the checksum hash is the same as in the corresponding DMA M audit trail entry the export file has not been manipulated 4 Quit the program by clicking on Close 1...

Страница 95: ...em Security Electronic Signature 2 Use the Electronic Signature check box to activate or deactivate the electronic signature 3 If a password is required during the signing process use the second check box to activate a password inquiry for setting a password see Chapter 10 4 2 4 Tap OK To assign the role for the electronic signature 1 Tap Menu and select Setup User Management 2 Highlight the user ...

Страница 96: ...rement results Examples Calculate the concentration of binary mixtures from the density of the mixture Convert your results into a unit which is not supported in the standard instrument configuration There are six types of user functions constants formulas linear functions polynomials with one input value 1 D polynomials with two input values 2 D and user tables You can program up to 20 user funct...

Страница 97: ... to 50 characters long Use the drop down box Function Type to select Constant Use the drop down box Physical Quantity to select the type of quantity you want to use Use the drop down box Unit to select the output unit 4 Tap Next Activate deactivate the check box Protect function against changes by other users Enter a comment to describe this user function This comment will not be printed exported ...

Страница 98: ...his comment will not be printed exported or displayed anywhere but is only an internal description of your user function 5 Tap Next Enter a Name for the first variable and define the input quantity Do the same for further input quantities if required 6 Tap Next 7 Enter your formula and tap OK TIP Only the operators and constants are allowed To program or edit a linear function 1 Tap Menu and selec...

Страница 99: ...p Menu and select Setup Expert Settings User Function Management to open the user functions list 2 Tap New to program a new polynomial or highlight an existing polynomial and tap Edit to open the four step User Function wizard 3 Perform the following settings Enter a name for the polynomial up to 50 characters long Use the drop down box Function Type to select the polynomial type Use the drop down...

Страница 100: ...hould cover the whole range of values that you want to measure 1 Tap Menu and select Setup Expert Settings User Function Management to open the user functions list 2 Tap New to program a new user table or highlight an existing user table and tap Edit to open the four step User Function wizard 3 Perform the following settings Enter a name for the user table up to 50 characters long Use the drop dow...

Страница 101: ...isplayed options Tap Yes to make a copy of this user function and save your changes under a different name Tap No to open this function in read only mode To delete a user function 1 Tap Menu and select Setup Expert Settings User Function Management to open the user functions list 2 Highlight a list item and tap Delete 16 3 Calculator With the calculator you can simulate any factory predefined func...

Страница 102: ...iable quantity in case more than two quantities are available 5 Enter a Value for the constant input parameter which has not been activated in column Select and tap Next 6 Define the range for the x axis variable input quantity by entering the First Value and the Last Value for the variable quantity The graph is displayed and can be printed out or exported by tapping Print or Export Graphs cannot ...

Страница 103: ...e case that someone changes the settings accidentally Saving the current settings before you perform a firmware upgrade Copying the instrument settings to one or more other M series DMA instruments A backup file contains the following instrument settings and instrument information Global settings in the control panel regional settings keyboard settings network settings Method settings display layo...

Страница 104: ...and the file name using the two drop down boxes The backup file must be stored in the root directory of your USB flash drive 4 Tap Next 5 Select the settings to be restored to your instrument in the column Value and tap OK 6 Tap Yes to restore the settings 7 Follow the instructions on the screen 17 3 Updating the Firmware Generally it is only necessary to update the user interface firmware This se...

Страница 105: ...o update the module firmware TIP A diagnosis message is shown if a too old firmware is installed on one of your modules If the auto logon for a user with administrator rights is activated the firmware update of the module can be started Otherwise the administrator must log on and then start the firmware update menu Service Update Module Firmware 1 Load the latest firmware into the root directory o...

Страница 106: ...if connected Xsample filling equipment and external measuring modules The instrument type serial number and firmware versions are shown in a table In this menu you can also save an instrument log file to a USB flash drive This file contains the last operating steps and may help during trouble shooting To view hardware and firmware configuration 1 Tap Menu and select Service System Information to o...

Страница 107: ... are frozen as well as the quantities on the main screen To unfreeze the values tap the button To view live raw data Tap Menu and select Service Live Raw Data DMA Density Quantities not mentioned in the following table are described in Appendix F e g Density Density Temperature Density not visc corr etc dD Harmonic Value Damping of the first harmonic Delta RHO Value Difference between density calc...

Страница 108: ...rected density valid if the viscosity is greater than 500 mPa s Status Value Status information indicating the temperature status of the cell Air Pump State Status of the air pump 0 or 1 Air Pressure Currently measured air pressure Air Pressure Condition Current status of the measurement Air Pressure State Status of the air pressure measurement Air Pressure Substate Detailed information about the ...

Страница 109: ...s of your instrument in the address field of the browser and press the key Now the system information of your instrument is displayed together with a download link for the PDF file of the instruction manual 18 2 Connecting the Instrument to an External PC via RS 232 If you want to connect the DMA M to a PC AP SoftPrint you have to use a certain cable and a gender changer Please find below the Mat ...

Страница 110: ...efined an RS 232 printer make sure that you do not print anything manually or automatically while using the RS 232 interface for data transfer to a PC Otherwise there will be a conflict with the RS 232 printer and both the printout and data transfer will fail start or Creates a new sample in the sample list and starts a measurement with the active method start method_number or Creates a new sample...

Страница 111: ...s the set temperature of the current method to the given value xx xxx in C This command is only allowed if no measurement is in progress help Returns a list of the available RS 232 interface commands Command Response Description start or start method_number or start method_number magazine_position measurement started The command was accepted and the measurement was started measurement already star...

Страница 112: ... no data available No measurement has yet been finished and so no data is available getdataunit g cm C Example response with the default settings no data available No measurement has yet been finished and so no data is available getdata 0 000892 0 000894 20 001 valid Example response with the default settings no new data available No new measurement has yet been finished and so no new data is avai...

Страница 113: ...ge LIMS Bridge can be used to send remote measurement commands from the LIMS to the instrument and to forward result files from the instrument to the LIMS For more details see the LIMS Bridge instruction manual help commands abort start method number magazine position finished getdatahead getdataunit getdata getrawdata getmethodname getid set temperature xx xxx help List of all available commands ...

Страница 114: ...for the whole temperature range from 0 C to 95 C the temperature accuracy is not constant for the whole range For temperatures above 90 C the temperature accuracy is typically between 0 01 C and 0 05 C b After full temperature equilibrium c Cooling down further than 20 C 68 F below ambient temperature only with external cooling using the cooling kit d For the measuring cell together with the injec...

Страница 115: ...s and cleaning liquids DMA M Standard accessories Material Part Borosilicate glass Measuring cell PTFE Filling adapter Material Part Polyethylene Waste vessel Polypropylene Polyethylene Syringe 2 mL Luer PTFE Injection adapter Luer PTFE Male Luer plug PTFE PTFE Adapter Luer cone Silicone Hose 3 x 5 mm silicone ...

Страница 116: ...de max 3000 m 9800 ft Touch screen 6 4 in TFT 640 x 480 px Memory 512 MB SD card upgrade capability up to 8 GB for internal information logfiles and instrument settings from DCB version 1 000 009 SD card is no longer used 1000 measuring values with without camera pictures Interfaces 4 x USB 2 0 full speed 2 x S Bus 1 x Ethernet 100 Mbit 1 x CAN Bus 1 x RS 232 1 x VGA RS 232 printer settings Interf...

Страница 117: ...ved air 2 Fill a clean glass flask full with the boiled liquid and cover it 3 Wait until the liquid has cooled down to the approx measuring temperature To stir the sample Stir your sample vigorously for 2 to 15 minutes depending on the stirring equipment until no bubbling occurs any more You can also pour the sample through a paper filter after stirring to get an even more efficient degassing effe...

Страница 118: ...e measuring cell Highly viscous samples Highly viscous samples can be heated up to lower the viscosity Always heat the sample to a temperature that is approx 15 C higher than the measuring temperature which can be 90 C maximum Pastes Paste like materials like toothpaste or tomato ketchup can be filled by syringe Inject these kinds of samples into the measuring cell by pushing the plunger very slow...

Страница 119: ...y lead to a failure of the U viewTM function DMA 4500 5000 M The higher the difference between the set measuring temperature and ambient temperature and the higher the air humidity the easier condensation occurs To prevent condensation in the measuring cell To prevent condensation in the measuring cell use a drying cartridge Mat No 65085 and connect it to the DRY AIR IN AIR PUMP connector at the r...

Страница 120: ...rom ISO 8573 1 Max particle size 40 µm Max pressure dew point 10 C below measuring temperature Max oil content 25 mg m3 To regenerate moist ruby gel The drying cartridge contains beaded ruby gel a non toxic drying agent When active the color of the drying agent is red Ruby gel which has absorbed liquid turns orange Moist ruby gel can be regenerated Pour the ruby gel into a glass bowl and blow hot ...

Страница 121: ...ature to 0 C 32 F in the Density Module dialog To measure at high temperatures To prevent bubble formation If you are measuring samples at temperatures significantly higher than ambient temperature the tendency to form gas bubbles in the measuring cell will dramatically increase To ensure precise results you can Degas your samples thoroughly directly before measuring see Appendix B 1 Heat your sam...

Страница 122: ...g to operate the touch screen Use a PC mouse Protection foil Your M series DMA is delivered with a transparent plastic protection foil covering the touch screen Three spare protection foils can be ordered Mat No 81402 If the touch screen has become dirty you can exchange the used protection foil against a new one To exchange the protection foil 1 Remove the used protection foil from the display us...

Страница 123: ... one edge of the display hold the opposite end and bend the foil backwards 4 Peel off the back liner with one hand simultaneously rolling the foil slowly onto the display with the other hand 5 Carefully flatten out the foil with a clean cotton cloth pushing bubbles towards the edges 6 In case of bubbles between foil and display gently push them towards the edges or lift up the foil partly or compl...

Страница 124: ...ra position 3 Use the position buttons to accommodate the position of the camera 4 To save the current camera position tap Save Position 5 Close the camera window by tapping X D 2 Setting the Camera Illumination If the illumination of the camera picture is not suitable for your special environment you can change the corresponding default setting 1 Log on as administrator 2 Tap Menu and select Setu...

Страница 125: ... measuring cell during water adjustment Repeat the filling procedure and use freshly degassed ultra pure bi distilled or deionized water Chapter 11 3 1 Table E 2 Measurement Problem Cause and Correction See I cannot start any measurement 15 minutes or more after booting the instrument Verify whether one or more modules are using older firmware versions than expected from the instrument s firmware ...

Страница 126: ...e filter criteria Change the filter settings Chapter 15 3 I have deleted all results but there are still results visible in the data memory The filter settings in the Delete Measured Data menu are different from the settings in the Data Browser Settings menu Perform corresponding settings in both menus Chapter 15 7 and Chapter 17 Table E 5 Data export Problem Cause and Correction See The export to...

Страница 127: ...efinition of the printer in the Printer Management menu Change the definition Chapter 9 3 No printout on POS printer Printer problems Check the printer See the respective printer instruction manual Wrong or no definition of the printer in the Printer Management menu Change the definition Chapter 9 3 Chinese printer Declare the printer as RS 232 Chinese in the Printer Management menu Chapter 9 3 Th...

Страница 128: ... check Last Check User Name of the user who performed the latest check Master Condition Sum of all available conditions from measuring modules within the system Measurement Type Type of measurement defined in the sample list S Standard C Check TS Temperature scan MM Multiple measurement Method Name of the selected or used method Sample Error State Error messages concerning the sample No error Was ...

Страница 129: ... at around 1 mPa s water Noticeable high readings for samples of higher viscosity Density Temperature Temperature in the measuring cell measured by the Pt 100 measuring sensor Density Condition Current status of the measurement Density Control Temp Temperature in the cell block measured by the Pt 100 control sensor Density Set Temp Set measuring temperature Specific Gravity Density of the sample a...

Страница 130: ...Quotient of the period of oscillation of 1st order of the U tube divided by the period of oscillation of the reference oscillator Group User Functions User functions can be formulas linear functions polynomials 1D or 2D or tables see Chapter 16 2 Group Ethanol Tables Ethanol concentrations in percentage by volume v v or percentage by weight w w according to ethanol concentration tables issued by d...

Страница 131: ...rees at 15 56 C 60 F based on true density at 20 C Ethanol Proof 60 F not visc corr Ethanol Proof 60 F without viscosity correction Group Extract Sugar Tables Concentration of extract sugar sucrose of beverages in different concentration units Number of digits displayed with concentration values DMA 5000 M 3 DMA 4500 M 2 DMA 4100 M 2 Number of digits displayed with Mass Concentration Sugar All 3 m...

Страница 132: ...ium Hydroxide NaOH a w w mol l N Landolt Boernstein based on true density at 20 C range 0 to 50 0 to 9 56 mol l Accuracy approx 0 04 0 01 mol l Sulfuric Acid H2SO4 w w mol l N CRC Handbook of Chemistry and Physics based on true density at 20 C range 0 to 94 0 to 17 6 mol l Accuracy approx 0 05 0 01 mol l a Caution corrodes measuring cell Group API Functions The API functions automatically convert ...

Страница 133: ...lection of the input parameter for API calculations Density Density not visc corr or a Special Adjustment API Product Group Selection of the API product group for calculation of API gravity density and specific gravity API Specific Gravity 15 C Conversion of density at measuring temperature to specific gravity at 15 C API Specific Gravity 20 C Conversion of density at measuring temperature to spec...

Страница 134: ...urement To perform 2 to 10 measurements of a single sample automatically TS Temperature Scan To perform a temperature scan Density Temperature To set the temperature of the density measuring cell Enter a value between 25 and 95 C or 90 C Density Measurement finished by Predetermination default Equilibrium for DMA 5000 M Equilibrium fast Equilibrium medium Equilibrium slow None use method default D...

Страница 135: ...ty Density default Density not visc corr Special Adjustment up to 5 None use method default Density Canadian Excise Alcohol Table Special Adjustment 1 5 default None use method default User defined data fields If set as mandatory in the sample list settings User functions of the Constant type If activated in the method settings Parameter Type Parameter Select Description ...

Страница 136: ...ode tec it com Use the format MethodX with X standing for the position number of the method in the method list To view the position number tap Method The bar codes pictured below are type Code 128 encodes all 128 ASCII characters NOTICE Please check the position number of your method after any changes in the method sequence after deleting or hiding methods and after creating new methods ...

Страница 137: ...317 10 0 001107 0 001131 0 001156 0 001181 0 001205 0 001230 0 001246 0 001291 15 0 001085 0 001110 0 001134 0 001158 0 001182 0 001206 0 001222 0 001267 20 0 001065 0 001088 0 001112 0 001136 0 001160 0 001184 0 001199 0 001243 25 0 001045 0 001068 0 001091 0 001115 0 001138 0 001162 0 001177 0 001220 30 0 001025 0 001048 0 001071 0 001094 0 001117 0 001140 0 001156 0 001198 35 0 001007 0 001029 ...

Страница 138: ...9099 999084 999069 999053 999038 999022 999006 998991 998975 998959 16 998942 998926 998910 998893 998876 998860 998843 998826 998809 998792 17 998774 998757 998739 998722 998704 998686 998668 998650 998632 998613 18 998595 998576 998558 998539 998520 998501 998482 998463 998443 998424 19 998404 998385 998365 998345 998325 998305 998285 998265 998244 998224 20 998203 998182 998162 998141 998120 99...

Страница 139: ... 985640 985591 985543 985494 985446 985397 985348 985299 985250 56 985201 985152 985103 985054 985004 984955 984906 984856 984807 984757 57 984708 984658 984608 984558 984509 984459 984409 984359 984308 984258 58 984208 984158 984107 984057 984007 983956 983905 983855 983804 983753 59 983702 983652 983601 983550 983499 983448 983396 983345 983294 983242 60 983191 983140 983088 983036 982985 982933...

Страница 140: ...66905 966838 966772 966706 88 966640 966574 966507 966441 966374 966308 966241 966175 966108 966042 89 965975 965908 965841 965774 965707 965640 965573 965506 965439 965372 90 965305 965238 965170 965103 965036 964968 964901 964833 964765 964698 91 964630 964562 964495 964427 964359 964291 964223 964155 964087 964019 92 963951 963882 963814 963746 963677 963609 963541 963472 963404 963335 93 96326...

Страница 141: ...e implemented Temperature scan DMA 5000 M only V1 60 19 08 2009 C76IB01D C76IB01E The sequence of items in the data browser favorites list and result output can be changed Screen saver implemented Feedback beep after measurement can be selected Single results can be deleted Audit Trail automatic logoff after 60 minutes without user interaction RS 232 connection with external PC possible Changes of...

Страница 142: ...moved to the quick access area Allowed minimum step size in temperature scans depends now on the equilibrium setting of the density module Keyboard and bar code settings the sample list can be edited with a bar code reader tab key as terminator Redo option after adjustments available New air pump setting Automatic stop when the density value is stable Audit Trail stores more detailed and structure...

Страница 143: ... 95 C Support of CAN bar code readers Hardware redesign SD card is not used anymore Show current method as postfix Standardized output for the RS232 report Prefill of widgets concerning the display layout after switching to another layout Updating UI firmware OS image and firmware modules at once without user confirmation upon every step if all firmware modules are attached during the update Inclu...

Страница 144: ...Appendix K Declaration of Conformity 144 C76IB003EN E Appendix K Declaration of Conformity ...

Страница 145: ...ment Special Adjustments Reset To Factory Adjustment Data Memory Measured Data Statistic Delete Measured Data Audit Trail Check SOP Data Delete Audit Trail Adjustment Data Density Module Density Adjustment Temperature Adjustment Density Adjustment KB Graph Special Adjustment Methods Method Settings Density Current Method Activate Modules Constantsb Density Module Display Layout Result Output Limit...

Страница 146: ... Keyboard and Bar Code Settings Advanced Camera Settingsc User Managementd System Security Security Level Audit Trail Electronic Signature Logon Settings Increased security Printout Settings Automatic Printout Report Management Select Logos Import Logos Name and Address Favorites Management Data Browser Settings Expert Settings User Function Management Calculator Group Calculator Check Management ...

Страница 147: ...ity Calculations DCB Air Pump DMA Density Air Pressure DCB Environment DCB CAN Connector a DMA 5000 M only b Only if a Constant user function was created and or if a module is connected c DMA 4500 M DMA 5000 M only d Users of any user group may change their own password ...

Страница 148: ...tration 62 63 AOAC 130 API density 63 132 133 API functions API parameters 67 API product group 68 output quantities 132 API gravity 132 API specific gravity 133 apparent density 129 apparent specific gravity 129 atmospheric pressure sensor 56 audit 92 audit trail activating deactivating 93 deleting 93 verifying the integrity of exported audit trails 94 viewing printing or exporting 93 audit trail...

Страница 149: ...quick access buttons 22 sample number 21 user indicator 21 drop down box 30 dry air 137 dry air supply 120 drying 81 82 drying cartridge 119 E equilibrium 64 114 error status 22 81 ethanol 62 63 82 83 114 ethanol concentration 130 ethanol tables 130 external keyboard 37 external measuring module 106 116 external PC 109 external touch screen 40 extract 131 extract sugar 114 extract sugar tables 131...

Страница 150: ...129 measurement type 71 measurements performing 78 progress of 79 speeding up 78 trouble shooting 125 measurements using special adjustments 58 measuring at high pressure 122 measuring at high temperatures 121 measuring at low temperatures 121 measuring cell 15 19 22 42 125 129 measuring errors 81 measuring methods copying a method 69 definition 61 deleting a method 70 factory preset methods 61 re...

Страница 151: ...r 14 130 reference temperature 132 regional settings 41 repeatability 114 reproducibility 117 residues 76 82 result data deleting 89 viewing of 85 result output 66 ruby gel 120 S sample amount 76 sample changer 18 sample list clearing 73 74 editing 73 loading 74 saving 73 setting the sample list mode 46 sample list mode No Sample List 46 72 Sample List 46 72 sample list warnings 46 sample name 71 ...

Страница 152: ...ial 99 types 96 user table 100 verifying 101 user groups 47 administrator 47 manager 47 operator 47 user indicator 35 user rights 47 49 user defined data field 45 user defined data fields 46 U tube 14 130 U tube method 13 U ViewTM 15 22 V viscosity 60 118 130 viscosity correction 114 129 voltage 116 W water check 52 wetted parts 115 wizard 33 ...

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