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Operating Manual

SPECORD S 600
UV/Vis Spectrophotometer

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Содержание SPECORD S600

Страница 1: ...Operating Manual SPECORD S 600 UV Vis Spectrophotometer...

Страница 2: ...Jena GmbH Konrad Zuse Str 1 07745 Jena Deutschland Telefon 49 3641 77 7407 Fax 49 3641 77 7449 E Mail service analytik jena com http www analytik jena com 211 502 23 A 08 2021 Analytik Jena GmbH Copyr...

Страница 3: ...t 15 5 2 Installation conditions 15 6 Installation and start up 16 6 1 Connectors and display elements 16 6 2 Connecting the SPECORD S600 17 6 3 Start up 17 6 4 Switching off the SPECORD S600 19 7 Acc...

Страница 4: ...Contents 4...

Страница 5: ...sample throughput but also provides solutions for special applications if used in combination with the diverse accessories available 1 2 Notes on the User s Manual In this manual the following symbols...

Страница 6: ...anual the manual uses the following system Chapters and illustrations are numbered consecutively Every illustration has its own caption Steps of operation are numbered Cross references are marked by a...

Страница 7: ...ff the SPECORD S600 at the power switch and discon nect the power cable from the power outlet 2 2 General safety regulations For your personal safety and for a trouble free operation carefully read th...

Страница 8: ...Electric shocks The SPECORD S600 is electrically powered At several parts inside the system extre mely hazardous electrical voltages are accessible To ensure Protection Class I protective earth connec...

Страница 9: ...the radiation properties of the lamps Especially protect the beam exit window of the deuterium lamp Make sure to remove the protective cap from the halogen bulb after having inserted it to avoid any...

Страница 10: ...h holmium oxide filter 0 5 nm Wavelength accuracy D2E peaks at 486 0 nm and 656 1 nm 0 3 nm Wavelength reproducibility with holmium oxide filter 0 02 nm Photometric accuracy VIS at 546nm with Hellma F...

Страница 11: ...ption 140 VA Fuses Line fuses 230 VAC T 3 15 AH 250V Type 19181 Wick mann 115 VAC T 3 15 AH 250V Type 19181 Wick mann Radio noise suppression EN 61326 Class B Noise immunity EN 61326 Protection Type I...

Страница 12: ...at is open to three sides and the poly chromator section on the left side 1 Lamp compartment 2 Sample compartment with carrier rails for holding accessories 3 Polychromator Fig 1 Mechanical design of...

Страница 13: ...by the holographic grating The produced spectrum is imaged onto the diode array The measured values of the individual photodiodes thus repre sent the value of intensity I over a small spectral region...

Страница 14: ...that may enter the polychromator through the open sample compartment including the currents on the diode array caused by electronics The intensity of the dark current must be subtracted from the inten...

Страница 15: ...ressive vapors e g strongly corrosive acid or caustic vapors away from the vicinity of the device The installation site of the SPECORD S600 must meet the following requirements The place should be fre...

Страница 16: ...d 2 D2E lamp ON LED yellow 3 Line power ON LED green Fig 3 Display elements on front panel The LED s light when the SPECORD S600 has been switched on and the lamps are on The power input connector wit...

Страница 17: ...s Manual 3 Connect the SPECORD S600 see Connectors and display elements p 16 to the PC free COM port or USB port using the supplied connecting cable Note When you use the autosampler you must connect...

Страница 18: ...elements on front panel p 16 3 In WinASPECT software select the SPECORD S600 PC port used Activate the Measurement Set Parameters menu function to open the window of the SPECORD S600 device driver Fig...

Страница 19: ...eriod is over 6 4 Switching off the SPECORD S600 1 Exit the WinASPECT session using the File Exit menu command 2 The shut down the computer 3 Finally switch off the SPECORD S600 at the power switch No...

Страница 20: ...1 1 Universal holder 1 Mount for cell holders or solid sample holders 2 Clamping lever Fig 7 Universal holder Fig 8 Installing and clamping the universal holder 1 Put the universal holder with its ho...

Страница 21: ...the beam This setup provides an optimized signal to noise ratio 7 1 2 Cell holder The cell holder is suitable for holding standard cells of an external width of 12 5 mm and a pathlength of between 1 a...

Страница 22: ...Further accessories Optionally the following accessories are available for the SPECORD S600 Thermostatted cell holder water cooled Adjustable cell holder for micro submicro or HPLC cells Peltier cont...

Страница 23: ...ples 11 60 variable angle reflectance accessory Absolute reflectance accessory Sipper system XYZ sampler Fiber coupling with measuring probes and SMA connectors 75 mm Integrating Sphere for transmissi...

Страница 24: ...ce Department For the address refer to the inside cover page 8 2 Cleaning Wipe off spilt samples in the sample compartment or on accessory units instantly with cleaning tissue Wipe off contamination o...

Страница 25: ...ff This particularly applies to the deuterium lamp because of the relatively high ignition voltage required The following rule applies as criterion for the service life of the deuterium lamp With one...

Страница 26: ...In the open lamp compartment you can see the deuterium lamp and the halogen lamp 1 Deuterium lamp 2 Knurled screws for fastening the deuterium lamp 3 Plug and socket connection 4 Operating hour meter...

Страница 27: ...connect its power cable 2 Open the flap of the lamp compartment and allow the lamps to cool down suffi ciently 3 Loosen the three pole plug and socket connection Fig 13 3 by compressing the lateral st...

Страница 28: ...5 Remove the new halogen lamp from its packaging 6 Insert the new halogen lamp taking care to ensure that the notch at its base en closes the pin in the bottom part of the holder 7 Fasten the halogen...

Страница 29: ...the defective line fuses Make sure to use only the following fuse types T 2 AH 4 Close the fuse holder again 5 Reconnect the power cable to the power input connector of the SPECORD S600 and the power...

Страница 30: ...ispose of the waste ma terial samples cropping up in the analyses in accordance with the relevant legal and local regulations When the service life of the device is over dispose of the device with its...

Страница 31: ...s on back panel 16 Fig 5 WinASPECT program icon 18 Fig 6 Dialog box of SPECORD S600 device driver 18 Fig 7 Universal holder 20 Fig 8 Installing and clamping the universal holder 20 Fig 9 Cell holder 2...

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