8
Run the System
Run the Experiment
2D-LC User Guide
214
Run the Checkout Familiarization Procedure for
Comprehensive (LCxLC)
To run the checkout, various hardware configurations are possible, see
on page 56. Not all options can be shown. As example the
is used here.
To achieve optimal sensitivity, in comprehensive mode, especially for LC/MS
applications, the LC flow is often split prior to the mass spectrometer.
The following parameters have been optimized for this standard configuration.
Parameters can deviate slightly for your system. Run the experiment and
subsequently edit or optimize the method for your setup.
Table 24
Example for a MS passive splitter setup (ratio 1:2)
Description (PN)
Usage
TEE, ST, 1/16 inch, Low Dead Volume
(0100-0969)
T-piece
DAD Heat Exchanger Capillary 310 mm, 0.12 mm
i.d. (G1315-87339)
2D detector connected to T-piece
Capillary ST 0.075 mm x 500 mm, long socket
(5500-1205)
Inlet of the LCMS source connected to the other
end of the T-piece
Capillary ST 0.075 mm x 250 mm, long socket
(5500-1206)
Remaining connection to the T-piece is used as
waste capillary
Содержание 1290 Infinity II 2D-LC Solution
Страница 122: ...5 2D LC Data Acquisition in MassHunter Workstation 11 Instrument Details 2D LC User Guide 122 3 Click Screen 4 Click OK...
Страница 263: ...2D LC User Guide 263 9 Data Analysis GC Image Basic Information 3 Import parameters...
Страница 264: ...9 Data Analysis GC Image Basic Information 2D LC User Guide 264 4 Fit view...
Страница 267: ...2D LC User Guide 267 9 Data Analysis GC Image Basic Information 11 View single 2D chromatograms 12 Select blobs...
