Hach TitraLab KF1000 Series User Manual Download

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DOC022.52.93082

TitraLab

KF1000 series workstations

User Manual

03/2019, Edition 9

Summary of Contents for TitraLab KF1000 Series

Page 1: ...DOC022 52 93082 TitraLab KF1000 series workstations User Manual 03 2019 Edition 9...

Page 2: ......

Page 3: ...the titrant and the reagent 16 3 9 Tidy the work area 17 Section 4 Install accessories 19 4 1 Install a balance 19 4 2 Install the syringe verification kit 19 Section 5 User interface and navigation 2...

Page 4: ...Syringe verification 43 8 7 6 Other maintenance options 44 8 8 Storage and transportation 44 8 8 1 Prepare the instrument for short term storage 44 8 8 2 Prepare the instrument for long term storage...

Page 5: ...C 50 60 Hz Altitude 2 000 m 6 562 ft maximum Operating temperature 15 to 35 C 59 to 95 F Relative humidity 20 to 80 non condensing Storage temperature 5 to 40 C 23 to 104 F Installation category II Po...

Page 6: ...Specifications 4...

Page 7: ...could result in serious injury to the operator or damage to the equipment Make sure that the protection provided by this equipment is not impaired Do not use or install this equipment in any manner o...

Page 8: ...le for compliance could void the user s authority to operate the equipment This equipment has been tested and found to comply with the limits for a Class A digital device pursuant to Part 15 of the FC...

Page 9: ...ts as of the date of sale of the enclosed product Note that some of the component types listed above may or may not be a part of the enclosed product The Environmentally Friendly Use Period EFUP for a...

Page 10: ...t connections Use the USB port on the side of the instrument for the USB applications key supplied with the instrument Use the USB port on the rear of the instrument to connect to a printer mouse keyb...

Page 11: ...box Note For identification the outlet tube from the syringe is fitted with a blue marker 1 Instrument 3 Power cord 2 Sample stopper 4 Power supply Figure 2 Contents of the application box 1 KF standa...

Page 12: ...General information 10...

Page 13: ...uickly in case of emergency Keep the instrument away from temperature extremes including heaters direct sunlight and other heat sources Put the instrument on a stable and level surface in a well venti...

Page 14: ...e any warning messages related to missing applications that show on the display The sensor holder has two positions one over the magnetic stirrer and the second at 180 to the right Move the sensor hol...

Page 15: ...stir bar to the beaker and then attach the beaker to the sensor holder Install the desiccant cartridge and the sample stopper Refer to the illustrated steps that follow 3 5 Prepare the tubes Remove a...

Page 16: ...installed at the optimal positions Do not change the position of the diffusion tip or the tube holder 3 7 Install the sensor 3 7 1 Connect the sensor Use a conical adapter to hold the sensor tightly...

Page 17: ...st be added where there is most turbulence and as far away from the sensor to allow the reagent time to react Check that the titrant tube and the sensor are positioned correctly Refer to Figure 3 wher...

Page 18: ...ridge into the adapter on the titrant and solvent bottle caps Note The molecular sieve in the filled cartridges must be regenerated regularly depending on the humidity of the laboratory Refer to Regen...

Page 19: ...identification 1 Titrant 3 Solvent 2 Waste 3 9 Tidy the work area Attach the tubes to the instrument with the clips on the electrovalve and the sensor holder Refer to the illustrated steps that follow...

Page 20: ...Installation 18...

Page 21: ...ut on a balance The weights are used to calculate the real volume added The real volume is compared with the nominal volume The results are used to calculate the error in the volume added and the syri...

Page 22: ...the tube from the pipette holder to the syringe outlet port 5 Connect the tube from the water bottle to the syringe inlet port 6 On the instrument manually enter the temperature As an alternative conn...

Page 23: ...ect options shown above them in the footer bar The options available are applicable to the current operation e g calibration measurement etc Navigation keys Scrolls through menus and data enter number...

Page 24: ...5 and Table 6 Table 4 Home menu Option Description Cell management Use the pumps to fill or empty the measurement cell Syringe activation Make sure that the syringe is working correctly Data log Manag...

Page 25: ...to the default configuration Options Set the operating parameters Security Set a password and specify which options are password protected Table 6 Maintenance menu Option Description Syringe activati...

Page 26: ...when replacing reagents Maintenance schedule Manage the maintenance tasks Maintenance summary See the number of days remaining on specified devices before maintenance is required Syringe verification...

Page 27: ...Brightness Sets the brightness of the display Sounds Sets the sound options Language Sets the language Network Give a name to the instrument If a printer is connected this name is printed on the hard...

Page 28: ...tically using a regulated addition of the titrant as defined in the application When the cell standby option is active Cell standby starts automatically as soon as an application is selected from the...

Page 29: ...B key and reconnect it 6 3 Prepare the instrument for measurement 1 From the home screen select Purge All attached devices are listed 2 Select All elements to purge all the attached devices or select...

Page 30: ...Startup 28...

Page 31: ...there is no liquid spill Make sure that the initial level is enough so that the sensor is correctly installed in the sample Do not put too much solvent in the beaker 5 From the home screen select Cal...

Page 32: ...that all of the standard is put into the center of the beaker and that none of it spills onto the walls of the beaker 15 Put the sample stopper back into the sensor holder Make sure that the sample s...

Page 33: ...ker with the applicable amount of solvent Refer to the application note and Cell management on page 37 to adapt the volume where applicable Make sure that there is no liquid spill Make sure that the i...

Page 34: ...mple temperature and measurement duration are shown at the bottom of the display The stability bar shows the stability of the signal and ranges in color from red unstable through yellow to green stabl...

Page 35: ...dby operation starts again automatically 24 Push the arrow keys to see the different measurement views or push Next for the options that follow Option Description Replicate sample Use this option to s...

Page 36: ...be used for the measurement If Define blank has been selected before two more sample types are available QC with blank and Sample with blank 8 Make sure that the icon at the bottom of the display is...

Page 37: ...dby operation starts again automatically Push the arrow keys to see the different measurement views 21 Push Next for the options that follow Option Description Replicate sample Use this option to star...

Page 38: ...Use the asterisk character in the name to increment the name using the instrument date and time in YYMMDDHHMMSS format For example where Water is the name of the sample Select Settings Applications E...

Page 39: ...og was the selected option push Preview to see the selected data then push Export or Delete to start the procedure 7 6 Purge Use this procedure to remove air bubbles from the system Refer to Prepare t...

Page 40: ...Standard operations 38...

Page 41: ...asurement cell Refer to Replacement parts and accessories on page 53 for part numbers x Replace syringe electro valve block Refer to Replace the syringe electro valve block on page 40 x Examine the sy...

Page 42: ...the molecular sieve weekly but this will vary depending on the humidity of the laboratory A humidity indicator such as color changing silica gel crystal can be used to show when regeneration is necess...

Page 43: ...nto the titrant bottle Empty to beaker Discards the contents of the syringe into the beaker Make sure that the tube from the outlet port of the syringe is inside the beaker Stop Stops the operation 8...

Page 44: ...elect to discard the contents of the syringe into the titrant bottle or the beaker and then obey the instructions on the display Refer also to Install the syringe on page 12 for the installation Syrin...

Page 45: ...t Make sure to fully rinse the syringe with methanol dry before the test to remove titrant Make sure to fully rinse the syringe with methanol dry after the test to remove water Note A license key is n...

Page 46: ...rification test and save the syringe verification results for fully tested volumes to the data log push Skip 10 When the test is complete Pass or Fail shows Push the left or right arrow to show the re...

Page 47: ...ntenance Syringe activation and empty the contents of the syringe 5 Carefully clean the measurement cell using an applicable organic solvent to dissolve any residue and oil From the home screen select...

Page 48: ...instrument at a temperature 5 to 40 C 23 to 104 F and relative humidity up to 80 4 Make sure that the storage location for the instrument does not have dust condensation or chemical evaporation Maint...

Page 49: ...quivalence point detection value for the application refer to Change application parameters on page 59 Contact technical support Out of range The computed result is outside the accepted limits Refer t...

Page 50: ...ect it again Change the sensor if no measurement is received using the Live Measure option refer to Other maintenance options on page 44 The stirrer does not operate The stirrer does not automatically...

Page 51: ...push the Home key to return to the home screen Remove the USB storage device and make sure the USB icon is no longer seen in the header bar then install the device again and import the new applicatio...

Page 52: ...that name user name is not already used The update to the operator name cannot be done Check that the name is not already used Fail to save the modification of the application The update to the appli...

Page 53: ...or fully and partially automated modes only Make sure that the temperature sensor is installed and connected correctly Incorrect input value The input value is out of range fully and partially automat...

Page 54: ...Troubleshooting 52...

Page 55: ...ed by the manufacturer Note Product and Article numbers may vary for some selling regions Contact the appropriate distributor or refer to the company website for contact information Table 15 Replaceme...

Page 56: ...continued Description Item no Bottle stopper GL45 LZE117 Glass bottle 1L LZE119 Desiccant tube filled with molecular sieve LZE121 Conical adapter LZE183 Stopper 20 mm KF cell LZE123 Tube fitting 2x L...

Page 57: ...d Description Item no Spare pump cassette LZE126 Magnetic stir bar PTFE 20 x 6 mm 5x LZE136 Set of accessories 5 mL syringe LZE140 Power supply without power cable LZE144 Power cable EU YAA080 Power c...

Page 58: ...57 RS 232 adapter cable LZE145 Syringe protection cover LZE156 Electro valve block and connector LZE165 RS 232 cable for balance connection to TitraLab LZE196 Thermo Drucker USB printer LQV161 99 1000...

Page 59: ...cium combined selective LZW9660C 97 002 Legacy adapter LZV662 OPT300 photocolorimetric probe E71T001 PTM450 NP photocolorimetric titration module without power X61T005 pHG311 9 pH electrode pH 0 14 FX...

Page 60: ...Replacement parts and accessories 58...

Page 61: ...e etc is available to change in some parameter groups It specifies if the result is shown on the display Changing this from Yes to No means that the calculated measurement result will not be shown Thi...

Page 62: ...requency of titrant calibration 0 no reminder x x Stirring speed Speed of the stirrer during titrant calibration x x Incremental addition Delay Stirring time before the titration starts x x Injection...

Page 63: ...nd point x Proportional band Proportional band of the PID regulation x Drift threshold Drift value below which the cell is considered as dry x x Max addition speed Maximum speed for titrant addition o...

Page 64: ...Change application parameters 62...

Page 65: ...n on the instrument to purge the syringe of air bubbles refer to Prepare the instrument for measurement on page 27 Why is titrant leaking along the sealing above the electrovalve The tubes have not be...

Page 66: ...Frequently asked questions 64...

Page 67: ......

Page 68: ...h com www hach com HACH LANGE GMBH Willst tterstra e 11 D 40549 D sseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info de hach com www de hach com HACH LANGE S rl 6 route de Compois 1...

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