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< 7. Calibration >
7-8
IM 12E01B30-02EN
1st Edition : Mar. 08, 2023-00
(5) Stop supplying the sample and drain all the sample in the detector. (Turn ON [Maint.] on the
main menu. Switch On [SV4] from [SV].
(6) Drain several times while supplying the zero water and remove all the contaminants left in
the head tank or the detector. After the cleaning, stop the zero water and drain all the water
left in the detector or the head tank.
(7) Connect the standard-solution tank to the sample inlet and feed the standard solution at
a rate of 2 L/min using a pump. Supply the standard solution agitating it with a magnetic
stirrer.
(8) When the standard solution begins to overflow the Flow cell, stop supplying the standard
solution by turning off the pump, and drain it off by opening the drain value. Then close the
drain valve and again supply the standard solution.
(9) Allow the standard solution to flow for 4 minutes or more and after the reading stabilizes,
carry out span calibration.
(10) Confirm the reading is stable. Press [check stability].
(11) After the message pops saying the reading is stable, enter the calibration value. Then press
[Next].
(12) Check the result of calibration and press [Accept] to update the Slope of the calibration
parameter.
(13) Drain the standard solution and clean the Flow cell with zero turbidity water. If you finish the
calibration, run the sample and turn off the maintenance mode after the reading becomes
stable.
7.8
Auto zero calibration
Automatic cleaning and Automatic zero calibration run one time. Execute this operation in a
measurement mode. Maintenance mode cannot carry out this operation. This operation does not
affect any automatic sequence schedule.
If Auto zero calibration cannot be selected, check the following two points.
• Activate the Wash box. (See “4.2.4 Wash/Cal. box”)
• Activate the Automatic cleaning/Automatic zero calibration function. (See
cleaning/Automatic zero calibration setting”)
7.9
Zero shift correction
Perform this calibration when you need to adjust the Zero value after both Zero and Slope
calibration are conducted correctly.
(1) Turn on the maintenance mode.
(2) Press on Main screen and go to the calibration menu.
(3) On the calibration menu, select [Zero shift correction] in the menu list of Calibration others.
(4) Run or feed from top of the detector a sample to use the Zero shift correction
(5) Confirm the reading is stable. Press [check stability].
(6) After the message pops saying the reading is stable, enter the value in [Cal.point]. Then
press [Next].
(7) Check the result of calibration and press [Accept] to update the Zero shift value of the
calibration parameter.
(8) Place the clear cover and the top cover on top of the detector. If you finish the calibration,
run the sample and turn off the maintenance mode.
Summary of Contents for TB830D
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