NanoFlow source
3-23
and three times the diameter of the cone aperture. Typically this distance is
approximately 2 mm.
Capillary tip position:
For tuning instructions, see the MassLynx Xevo TQD online help topic,
“Tuning manually for NanoFlow operation”.
Restarting a stalled borosilicate glass capillary electrospray
Should the spray stop, you can restart it. To do so, in the Tune window, set
Capillary to 0 kV. Then adjust the three-axis manipulator so that, viewed
under magnification, the capillary tip touches the sample cone, and a small
piece of the borosilicate glass capillary shears off.
If necessary, you can also apply some NanoFlow gas pressure, to force a drop
of liquid from the capillary. Apply as much as 1.4 bar (20 psi). Doing so
induces the drop’s appearance unless the capillary is blocked.
d
2d
3d
Cone aperture diameter
Summary of Contents for Xevo TQD
Page 12: ...xii...
Page 20: ...xx Table of Contents...
Page 23: ...Uses and compatibility 1 3 Xevo TQD TP03406...
Page 24: ...1 4 Specifications and Operating Modes Xevo TQD with visor up TP03407...
Page 42: ...1 22 Specifications and Operating Modes...
Page 52: ...2 10 Preparing for Operation...
Page 76: ...3 24 Changing the Mode of Operation...
Page 194: ...4 118 Maintenance Procedures...
Page 208: ...A 14 Safety Advisories...
Page 234: ...B 26 External Connections...
Page 238: ...C 4 Materials of Construction and Compliant Solvents...
Page 250: ...Index 8...