3-8
Changing the Mode of Operation
4. Using tubing equal to 0.004-inch ID, connect port S of the selector valve
to the IonSABRE II probe.
Recommendation:
To reduce peak broadening, use 0.004-inch ID tubing
for sample flow rates
1.2 mL/min; use 0.005-inch ID tubing for sample
flow rates
1.2 mL/min.
Requirements:
•
If you are replacing the tubing between the selector valve and the
probe, minimize the length to reduce peak broadening.
•
When cutting the tubing to length, cut it squarely (that is,
perpendicular to its horizontal axis).
5. Install the corona pin (see
).
Removing the IonSABRE II probe
Required material
Chemical-resistant, powder-free gloves
To remove the IonSABRE II probe:
1. Prepare the instrument for working on the source (see
2. Remove the corona pin (see
3. Disconnect the selector valve tubing from the IonSABRE II probe.
Warning:
To avoid electric shock, do not use stainless steel tubing
or stainless steel finger-tight screws to connect the selector valve
to the IonSABRE II probe; use the PEEK tubing and natural
(beige) colored PEEK finger-tight screws supplied with the
instrument.
Warning:
The LC system connections, IonSABRE II probe, and
source can be contaminated with biohazardous and/or toxic
materials. Always wear chemical-resistant, powder-free gloves
while performing this procedure.
Warning:
To avoid electric shock, ensure that the instrument is
prepared for working on the source before commencing this procedure.
Summary of Contents for Xevo TQD
Page 12: ...xii...
Page 20: ...xx Table of Contents...
Page 23: ...Uses and compatibility 1 3 Xevo TQD TP03406...
Page 24: ...1 4 Specifications and Operating Modes Xevo TQD with visor up TP03407...
Page 42: ...1 22 Specifications and Operating Modes...
Page 52: ...2 10 Preparing for Operation...
Page 76: ...3 24 Changing the Mode of Operation...
Page 194: ...4 118 Maintenance Procedures...
Page 208: ...A 14 Safety Advisories...
Page 234: ...B 26 External Connections...
Page 238: ...C 4 Materials of Construction and Compliant Solvents...
Page 250: ...Index 8...