
Chapter 7
Column
Installation
144
a.
Make sure that your packed column has been correctly prepared as
described in the
Preparing a Metal Packed Column
b. Insert the column end to the metal adapter paying attention that the
column end touches the bottom
c.
Finger-tighten the column end retaining nut until they start to grip the
column.
d. Tighten the column retaining nut.
CAUTION
Overtightening the compression ferrule does not necessarily produce a stronger,
leak-free joint. In fact, very often the reverse is true. Overtightening can cause a leak
in the joint and make it very difficult to reseal that particular joint when changing
columns.
Connecting a Packed Column to the TCD Detector
Materials required:
•
metric/imperial retaining nut
•
metric/imperial ferrules
•
10 mm or 1/4 inch wrench
•
adapter for detector
1. Insert the appropriate adapter into the bottom of the detector base, then push
up the adapter into the detector base as far as possible.
2. Slide the ferrule up to detector base then finger-tighten the adapter retaining
nut until it starts to grip the adapter.
3. Use the wrench to tighten the retaining nut. Use no more pressure than is
necessary to obtain a good seal (1/4 to 1/2 turn).
4. Insert the detector end of the column to the adapter base as far as possible.
5. Slide the ferrule up to adapter base then finger-tighten the column retaining
nut until it starts to grip the column.
Summary of Contents for FOCUS GC
Page 4: ...iv InstructionManual ...
Page 70: ...Chapter 2 The FOCUS GC User Interface Info Diagnostics 70 Instruction Manual ...
Page 92: ...Chapter 4 Column Oven Oven Parameters 92 Instruction Manual ...
Page 124: ...Chapter 6 Purged Packed Column Injector PPKD PPKD Injector Menu 124 Instruction Manual ...
Page 170: ...Chapter 8 Flame Ionization Detector FID Detector Signal Parameters 170 Instruction Manual ...
Page 186: ...Chapter 9 Thermal Conductivity Detector TCD Detector Signal Parameters 186 Instruction Manual ...
Page 242: ...Chapter 13 SOP number P0473 04 E 02 May 2007 242 Instruction Manual ...
Page 336: ...Chapter 16 LAN Option Set up Set Up 336 Instruction Manual ...
Page 344: ...Glossary 344 Instruction Manual C min 1 instead of C min g L 1 instead of g L ...
Page 350: ...Index 350 Instruction Manual ...