1
Basic Operations
Installing a Column into the GC/MS System
4
DSQ II Hardware Manual
Thermo Scientific
Installing a Column into the GC/MS System
To install a column, you will need:
• Capillary column, 5MS, 15 m, 0.25 mm i.d., 0.25 μm
• Column Measuring Tool
• Gloves, clean, lint- and powder-free
• Injector ferrule, for 0.25 mm column
• Magnifying glass
• Methanol or other suitable solvent
• Scoring wafer (or sapphire scribe) to cut capillary column
• Leak detector (Thermo Scientific GLD Pro PN 66002-001 or equivalent)
• Flowmeter (Thermo Scientific GFM Pro flowmeter PN 66002-010 or equivalent)
• Tissue, lint-free
• Transfer line ferrule, 0.4 mm i.d.
• Wrench, open-ended, 5/16-in.
• Wrench, open-ended, 6 mm
• Wrenches (two), open-ended, 7/16-in.
For information about setting up the TRACE GC Ultra or FOCUS GC, refer to the
documentation supplied with the instrument.
1. Connect the column to the injector that is inside the TRACE GC Ultra.
Figure 1.
GC Injector (Front)
WARNING - BURN HAZARD:
The injector, oven, and transfer line may be hot. Allow
them to cool to room temperature before touching them.
1
Injector
4
Column
2
Injector Ferrule
5
Column Outlet
3
Injector Nut
6
Transfer Line
1
4
3
4
2
6
5
Summary of Contents for DSQ II
Page 1: ...DSQ II Hardware Manual 120299 0002 Revision C December 1 2009 ...
Page 4: ......
Page 8: ......
Page 36: ...1 Basic Operations Shutting Down the GC MS System 20 DSQ II Hardware Manual Thermo Scientific ...
Page 198: ...5 Ion Source and Inlet Valve Inlet Valve Upgrade 182 DSQ II Hardware Manual Thermo Scientific ...
Page 202: ...6 Prefilter and Quadrupole 186 DSQ II Hardware Manual Thermo Scientific ...
Page 206: ...7 Ion Detector Electron Multiplier 190 DSQ II Hardware Manual Thermo Scientific ...
Page 242: ...226 DSQ II Hardware Manual Thermo Scientific Index ...