Sigma 100008 Manual Download

Page: 1 / 113

Translation of the original operating manual

sb
11/2017
Rev. 1.7.1 of 08/12/2022
Sigma 4-5KRL;Refrigerated Centrifuge for Robot Use;Sigma 4-5KRL IVD; ;

Refrigerated Centrifuge for Robot Use

Sigma 4-5KRL

Sigma 4-5KRL IVD

from serial no. 165039

Refrigerated Centrifuge
for Robot Use

Operating Manual

part no. 0703302

Summary of Contents for 100008

Page 1: ...17 Rev 1 7 1 of 08 12 2022 Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD Refrigerated Centrifuge for Robot Use Sigma 4 5KRL Sigma 4 5KRL IVD from serial no 165039 Refrigerated Centrifuge for Robot Use Operating Manual part no 0703302 ...

Page 2: ...Refrigerated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 2 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual ...

Page 3: ...RL IVD Version 11 2017 Rev 1 7 1 of 08 12 2022 sb 3 113 Translation of the original operating manual Copyright by Sigma Laborzentrifugen GmbH An der Unteren Söse 50 37520 Osterode am Harz Germany Tel 49 0 5522 5007 0 Fax 49 0 5522 5007 12 Web www sigma zentrifugen de E mail info sigma zentrifugen de ...

Page 4: ...Refrigerated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 4 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual ...

Page 5: ...17 3 1 Marking of the unit 17 3 2 Explanation of the symbols and notes 18 3 3 Responsibility of the operator 19 3 4 Requirements concerning the personnel 20 3 5 Informal safety instructions 21 3 6 Safety instructions 22 3 6 1 Electrical safety 22 3 6 2 Mechanical safety 22 3 6 3 Safety Instructions for robot controlled centrifuges 23 3 6 4 Fire prevention 23 3 6 5 Chemical and biological safety 24...

Page 6: ...2 2 1 Installation of the rotor 34 6 2 2 2 Installation of accessories 34 6 2 2 3 Adapters 36 6 2 2 4 Vessels 36 6 3 Control system Spincontrol L 37 6 3 1 User interface 37 6 3 2 Manual mode 38 6 3 2 1 Starting a centrifugation run 38 6 3 2 2 Interrupting a centrifugation run 38 6 3 2 3 Interrupting a deceleration process 38 6 3 2 4 Selection display and modification of data 38 6 3 2 5 Speed relat...

Page 7: ...arriers 57 8 1 4 Load bearing bolts 58 8 1 5 Glass breakage 59 8 2 Sterilisation and disinfection of the rotor chamber and accessories 59 8 2 1 Autoclaving 60 8 3 Service 61 8 4 Return of defective centrifuges or parts 62 9 Disposal 64 9 1 Disposal of the centrifuge 64 9 2 Disposal of the packaging 64 10 Technical data 65 10 1 Ambient conditions 66 10 2 Technical documentation 66 11 Appendix 67 11...

Page 8: ...ated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD Table of contents 8 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual ...

Page 9: ...hat is marked with IVD is intended for human biological samples including donated blood and tissue in conjunction with diagnostic in vitro applications This means that it is a medical product in accordance with Regulation EU 2017 746 on in vitro diagnostica Only trained specialised personnel are authorised to use the centrifuge in closed laboratories The intended use also includes observation of a...

Page 10: ...r way Non compliance may be prosecuted under criminal law 1 5 Standards and regulations These operating instructions have been created in accordance with the relevant European standards and regulations see chapter 11 7 EC declaration of conformity 1 6 Scope of supply The centrifuge comprises 1 rotor wrench size 13 Part no 930 102 1 hexagon socket wrench size 5 Part no 930 051 1 tube of silicone gr...

Page 11: ... 12 2022 sb 11 113 Translation of the original operating manual 2 Layout and mode of operation 2 1 Layout of the centrifuge 2 1 1 Functional and operating elements 1 Centrifuge lid 2 User interface see chapter 6 3 1 User interface 3 Slide cover 4 Mains switch Fig 1 Total view of the centrifuge 5 Name plate see chapter 2 1 2 Name plate Fig 2 Rear view of the centrifuge ...

Page 12: ...4 5KRL IVD 2 Layout and mode of operation 12 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual 6 Serial interface see chapter 2 1 3 Serial interface pin assignment 7 Equipotential bonding screw 8 Fuse 9 Mains power input Fig 3 Detailed view A connections ...

Page 13: ...perating manual 2 1 2 Name plate 1 Manufacturer 2 Power consumption 3 Max speed 4 Max kinetic energy 5 Serial number 6 Part number 7 Nominal voltage 8 Type 9 Consult operating manual 10 Symbol for special disposal see chapter 9 Disposal 11 IVD mark if applicable 12 Date of manufacture 13 CE mark in compliance with the directive 2006 42 EC 14 Max permissible density 15 Refrigerant data Fig 4 Exampl...

Page 14: ...n assignment There is a floating normally closed contact between pin 1 and pin 4 When the centrifuge is started the contact opens thereby signalling that the centrifuge is ready for operation The switching capacity is 48 VDC 1 A maximum 1 floating normally closed contact with pin 4 2 TxD transmit 3 RxD receive 4 floating normally closed contact with pin 1 5 GND ground 6 not used 7 not used 8 not u...

Page 15: ...and quadratically as a function of the angular velocity The bigger the radius in the rotor chamber is and the higher the speed is the higher the centripetal acceleration is However the forces acting on the rotor also increase Das 2 2 2 Area of application Depending on the area of application of the centrifuge and also on the particle size solids content and volume throughput of the mixture of subs...

Page 16: ...mined by way of the stated formula If afterwards the speed or the radius is changed the resulting relative centrifugal force will be recalculated automatically by the control unit If the RCF is changed the speed will be adapted while the specified radius is maintained The speed gravitational field diagram provides an overview of the relationship between speed radius and RCF see chapter 11 2 Speed ...

Page 17: ...r Warning against hand injuries Name plate see chapter 2 1 2 Name plate CE mark in compliance with the directive 2006 42 EC Do not dispose as part of domestic waste Consult operating manual Medical product in accordance with the regulation EU 2017 746 NRTL mark only for the USA and Canada RCM mark only for Australia China RoHS 2 mark only for China California Proposition 65 mark only for the USA U...

Page 18: ...symbols causes serious health problems up to life endangering injuries DANGER This symbol stands for a direct hazard to the life and health of persons due to electrical voltage Non observance of these symbols causes serious health problems up to life endangering injuries WARNING This symbol stands for a potential hazard to the life and health of persons Non observance of these symbols can cause se...

Page 19: ...k the operator is obliged to take measures in order to prevent danger to life or health during work ensure that the centrifuges are used properly and entirely as intended see chapter 1 2 Intended use take protective measures against fire and explosion when working with hazardous substances take measures for the safe opening of the centrifuges The operator must perform a risk assessment concerning ...

Page 20: ...persons are present in the danger zone or work area This manual uses the following personnel qualifications for various areas of activity Qualified electrician Due to their special training knowledge experience and familiarity with the relevant standards and regulations qualified electricians are in the position to perform work on electrical systems and to autonomously identify and prevent possibl...

Page 21: ...f a patient user or other person c a serious risk to public health 3 5 Informal safety instructions This operating manual is a part of the product The operating manual must be kept at the location of use of the centrifuge Ensure that it is accessible at all times The operating manual must be handed over to any subsequent owner or operator of the centrifuge Any changes additions or updates received...

Page 22: ... which the housing needs to be removed Inspect the electrical equipment of the unit regularly Defects such as loose or burnt cables must be eliminated immediately Following the completion of any type of repair or service the qualified and specialised personnel must perform final inspection and testing in compliance with the relevant standards 3 6 2 Mechanical safety In order to ensure the safe ope...

Page 23: ... rotor and accessories for signs of damage that can be discerned from the outside Special attention must be paid to all of the rubber parts e g motor cover lid seal and adapters in terms of visible structural changes Defective parts must be replaced immediately Open the centrifuge when it is not in use so that moisture can evaporate 3 6 3 Safety Instructions for robot controlled centrifuges This c...

Page 24: ...owever require special safety measures e g centrifugation of infectious toxic radioactive or pathogenic substances 3 6 6 Safety instructions for centrifugation For safe operation observe the following before starting the centrifuge WARNING Ensure that the centrifuge was set up properly see chapter 5 Set up and connection Maintain a safety distance of at least 30 cm 12 inches around the centrifuge ...

Page 25: ...ons Pay special attention to changes such as corrosion cracks material abrasion etc After 10 years they must be inspected by the manufacturer After 50 000 cycles the rotor must be scrapped for reasons of safety If other data concerning the service life are engraved on the rotor or bucket these data shall apply accordingly For example a bucket with the engraving max cycles 10 000 has a service life...

Page 26: ... a limited service life WARNING Perform regular checks at least once per month for safety reasons Pay special attention to changes such as corrosion cracks material abrasion etc The rotors and accessories must be put out of service after 10 years Any use after this period may be permissible in individual cases after an inspection performed by the manufacturer After 50 000 cycles the rotor must be ...

Page 27: ...rms a self check and identifies malfunctions Error messages are displayed as Error followed by a code number see chapter 7 2 Table of error codes 3 7 4 Earth conductor check For the earth conductor check there is an equipotential bonding screw on the rear panel of the centrifuge see chapter 2 1 1 Functional and operating elements An earth conductor check can be carried out by authorized and specia...

Page 28: ...mergency doctor 3 9 Remaining hazards The centrifuge was built in accordance with the state of the art and in compliance with the generally recognized safety rules However danger to life and limb of the operator or of third parties or impairments of the unit or other material assets cannot be completely excluded when the unit is being used Use the unit only for the purpose that it was originally i...

Page 29: ...in its original packaging for up to a year Store the centrifuge only in dry rooms The permissible storage temperature is between 20 C and 60 C If you would like to store it for more than one year or if you intend to ship it overseas please contact the manufacturer 4 3 Notes on transport Install the transport safety device see chapter 4 5 Transport safety device Always lift the centrifuge with a li...

Page 30: ...or any possible future transport of the centrifuge 4 5 Transport safety device The transport safety device consists of two hexagon socket screws which are located at the bottom panel CAUTION The transport safety device must be removed prior to start up because the screws lock the motor bearings Removal Lift the centrifuge upwards at the front side Always reach under from the side Put a suitable ob...

Page 31: ...ing it near heat generators Avoid direct sunlight UV radiation The table must be stable and have a solid even surface Attention During transport from cold to warmer places condensational water will collect inside the centrifuge It is important to allow sufficient time for drying min 24 h before the centrifuge can be used again 5 2 Power supply 5 2 1 Type of connection DANGER The operating voltage ...

Page 32: ...mal circuit breaker Switch the unit off by actuating the mains power switch If it has tripped let the circuit breaker cool for approximately 2 minutes Switch the unit on The centrifuge is now ready for operation 5 2 2 Customer provided fuses Typically the centrifuge must be protected with 16 Amp B fuses that are to be provided by the customer NOTE To ensure safe disconnection in the event of a fau...

Page 33: ... start key remains inactive and can only be activated via the connected PC or by entering a code Entering the code Press and hold the stop key while entering the code Turn the function knob 1 notch to the left and then 3 nothes to the right Release the stop key The start key will be illuminated the centrifuge is ready for operation 6 2 1 Opening and closing the lid The lid can be opened if the cen...

Page 34: ...7060 In doing so hold the rotor at its outer rim Follow the safety instructions and hazard warnings see chapter 3 Safety CAUTION When using rotors for microtiter plate formats Ensure that the plate holders are inserted together with the plates into the buckets NOTE The lid screw serves for the fastening of the lid onto the rotor only not for the fastening of the rotor onto the motor shaft Removal ...

Page 35: ...ssible In this case however it is very important that the rotationally symmetrical inserts are identical see figure correct incorrect Fig 9 Permissible and impermissible loading of a swing out rotor with vessels of various sizes example illustration Centrifugation with low capacity Install the sample vessels in a rotationally symmetrical manner so that the buckets and their suspensions are loaded ...

Page 36: ...venly Loading the edges of a bucket only is not permissible 6 2 2 4 Vessels Load the vessels outside of the centrifuge Liquids in the buckets or multiple carriers cause corrosion Fill the vessels carefully and arrange them according to their weight Imbalances result in the excessive wear of the bearings Always fill the tubes up to their useful volume the volume that is stated for the tube When usi...

Page 37: ...emitting diodes and one function knob The display is divided into several different fields The various functions of the system can be called up by pressing and turning the function knob 1 Start key 2 Function knob 3 Display 4 Stop key 5 Lid key Fig 11 User interface of the Spincontrol L control system Display The centrifuge display has the following display fields 1 Speed RCF field 2 Several displ...

Page 38: ...d before a new centrifugation run can be started A quick stop can also be triggered during a normal deceleration e g in order to speed up the deceleration When a quick stop is triggered fast will be displayed in the lower right hand corner of the display 6 3 2 3 Interrupting a deceleration process Press the start key during a deceleration process in order to interrupt it and to restart the centrif...

Page 39: ...peed RCF values depend on the rotor that is used The parameters speed and RCF can be changed during the centrifugation Fig 13 Setting the speed value or the RCF value 6 3 2 6 Runtime The set runtime is displayed in the upper section of this field with the remaining runtime shown below The runtime is counted down from the set value starting with the start of the centrifuge and ending with the start...

Page 40: ...function In this case the symbol disappears but the bar continues to flash Press the function knob in order to activate the desired setting The bar remains visible as long as the cursor is placed on the symbol Fig 15 The function Runtime as of the set speed is activated Continuous run During the continuous run the runtime of the centrifuge is unlimited and must be stopped manually The centrifuge a...

Page 41: ...ored and displayed Fig 17 Indication Short during a short run 6 3 2 7 Temperature The set value is displayed in the upper area of the field and the actual sample temperature is displayed in the lower area Temperatures between 10 C and 40 C can be preselected NOTE The centrifuge is not equipped with an active heater This is why temperatures above room temperature depend on the air friction of the t...

Page 42: ... to start the rapid cooling process During the rapid cooling process the set temperature can be modified within the range below the actual temperature The Rapid Temp program will be stopped under the following conditions The set value is reached The program will stop with a sound signal if this function is activated The stop button is pressed The program will be stopped prematurely A parameter is ...

Page 43: ...ible buckets the various combinations will be displayed one after the other Confirm the input The selected rotor or rotor bucket combination will be adopted Fig 20 Preselection of a rotor or a rotor bucket combination Automatic rotor identification system If the centrifuge is equipped with an automatic rotor identification system the input mode will be activated automatically if the system detects...

Page 44: ...keless deceleration Fig 21 Preselection of a curve here preselection of an acceleration curve 6 3 2 10 Program lock ProgLock When the program lock is active it is impossible to save any new programs In this case the function save program is disabled In order to activate the program lock Select the ProgLock symbol with the cursor and confirm the selection The symbol and the bar under the symbol sta...

Page 45: ...y Fig 23 Cycle display for rotor 11650 and bucket 13421 Reaching the maximum number of cycles When the maximum number of cycles is reached for a rotor or bucket a corresponding warning signal will be displayed every time that the centrifuge is started the start key lid key and entire display will flash Fig 24 Display when the maximum number of cycles is reached flashing When the start key is press...

Page 46: ... flashes The input lock is activated Proceed in the same manner in order to deactivate the permanent input lock Fig 25 Padlock symbol indicating an activated input lock NOTE If the centrifuge is robot controlled via the computer the display can only be used for display purposes Only the stop key is active at all times and can be used to switch the centrifuge off in an emergency situation 6 3 3 Pro...

Page 47: ...ated status Select a random storage location from the program selection list Free storage locations are indicated by a flashing display Any storage locations that are already occupied will be overwritten during the saving process Save the program in the desired location The program is now saved NOTE The functions Auto Open Buzzer ProgLock and Cycles cannot be entered as part of a program Fig 26 Sa...

Page 48: ... centrifuge can now be controlled via the computer NOTE If the centrifuge is controlled via the computer the display can only be used for display purposes Only the stop key is active at all times and can be used to switch the centrifuge off in an emergency situation 6 4 2 Rotors Robot controlled centrifuges require special rotors that are equipped with magnets on the bottom surface see fig They ar...

Page 49: ...centrifuge is loaded and unloaded by way of a robot special rotors are used see chapter 6 4 2 Rotors These rotors are positioned via an input command The command setpos n moves the rotor automatically to the desired position where it is then locked During the positioning process the message Posi will be displayed in the upper area of the speed RCF field while a dynamic progress bar below this area...

Page 50: ...ma 4 5KRL IVD 6 Using the centrifuge 50 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual 6 5 Switching the centrifuge off Open the centrifuge when it is not in use so moisture can evaporate Switch the centrifuge off by pressing the mains power switch ...

Page 51: ...nactive Activate the start key see chapter 6 2 Switching the centrifuge on If the error occurs again contact service Centrifuge cannot be started lid key LED flashes The lid lock is not closed correctly Open and close the lid If the error occurs again contact service Centrifuge decelerates during operation Brief mains power failure Press start key in order to restart the centrifuge System error Po...

Page 52: ...itch and disconnect the power cord from the socket Remove the stopper see figure item 1 from the opening on the right side panel e g with a screwdriver Fig 31 Position of the opening for the emergency lid release The stopper is connected with a string Pull the string in order to release the lid Then reinsert the stopper into the opening WARNING Do not unlock or open the lid unless the rotor is at ...

Page 53: ...n Power off Allow to cool down Provide better ventilation only air cooled centrifuges Provide sufficient water throughput only water cooled centrifuges 46 49 Imbalance error only for centrifuges with imbalance monitoring system Allow to slow down Power off Eliminate the imbalance 50 59 Lid error Press lid key Close lid Remove foreign matter from the opening of the lid lock device With error 50 and...

Page 54: ...tact In the event of queries malfunctions or spare part enquiries From Germany Contact Sigma Laborzentrifugen GmbH An der Unteren Söse 50 37520 Osterode Germany Tel 49 0 55 22 50 07 44 44 E mail support lab sigma zentrifugen de Outside Germany Contact our agency in your country All agencies are listed at www sigma zentrifugen de Sales Partners NOTE If you would like to utilise our service please s...

Page 55: ...osive and aggressive substances Do not use solvents Do not use agents with abrasive particles Do not expose the centrifuge and rotors to intensive UV radiation or thermal stress e g by heat generators 8 1 Maintenance 8 1 1 Centrifuge Unplug the mains power plug before cleaning Carefully remove all liquids including water and particularly all the solvents acids and alkaline solutions from the rotor...

Page 56: ...he care of the accessories special safety measures must be considered as these are measures that will ensure operational safety at the same time Immediately rinse off the rotor buckets or accessories under running water if they have come into contact with any liquids that may cause corrosion Use a brush for test tubes in order to clean the bores of angle rotors Turn the rotor upside down and allow...

Page 57: ...ecision in order to withstand the permanent high stress from high gravitational fields Chemical reactions as well as stress corrosion combination of oscillating pressure and chemical reaction can affect or destroy the metals Barely detectable cracks on the surface can expand and weaken the material without any visible signs Check the material regularly at least once a month for cracks visible dama...

Page 58: ...th operation of the centrifuge Load bearing bolts that are insufficiently greased may cause the centrifuge to stop due to an imbalance Clean the load bearing bolts and bucket groove in order to remove the old grease Apply a small amount of heavy duty grease for load bearing bolts ref no 71401 see the following picture to both load bearing bolts of a bucket Fig 32 Sufficient quantity of grease for ...

Page 59: ...s rotors and rotor chamber In order to completely remove the glass particles and metal dust from the rotor chamber Grease the upper third of the rotor chamber with e g Vaseline Then let the rotor rotate for a few minutes at a moderate speed approx 2000 rpm The glass and metal particles will now collect at the greased part Remove the grease with the glass and metal particles with a cloth If necessa...

Page 60: ...in time min Max time min Max cycles Aluminium buckets 134 138 3 5 Aluminium rotors 134 138 3 5 Glass tubes 134 138 3 40 Polyallomer polycarbonate rectangular carriers 115 118 30 40 Polyallomer polycarbonate round carriers 115 118 30 40 Polyamide buckets 115 118 30 40 10 Polycarbonate polyallomer lids for angle rotors 115 118 30 40 20 Polycarbonate tubes 115 118 30 40 20 Polyphenylsulfone PPSU caps...

Page 61: ... stress high quality components were used during the production of the centrifuge Nevertheless wear cannot be excluded and it may not be visible from the outside Especially the rubber parts that are among other things part of the motor suspension are subject to ageing This is why we recommend having the centrifuge checked by the manufacturer during an inspection once per year in the operating stat...

Page 62: ...ods For this purpose we require a declaration of decontamination The form must be filled in completely and signed by authorised and specialised personnel only Affix the original form in a clearly visible manner to the outside of the packaging NOTE We will return the part unit if no declaration of decontamination is provided 2 Form for the return of defective parts This form is for the product rela...

Page 63: ... of the original operating manual NOTE The defective part unit must be packaged in a transport safe manner Please use the original packaging for the unit if at all possible If the product is dispatched to us in unsuitable packaging you will be charged the cost for returning it to you in new packaging The forms can be downloaded online from www sigma zentrifugen de Service Overhaul and repair ...

Page 64: ... symbol means that it is not permissible to dispose of the unit among household waste You can return these centrifuges free of cost to Sigma Laborzentrifugen GmbH Ensure that the unit is decontaminated Fill in a declaration of decontamination see chapter 8 4 Return of defective centrifuges or parts Comply with any other applicable local rules and regulations 9 2 Disposal of the packaging Use the p...

Page 65: ...e I 20 Power consumption kW Input fuse AT Series fuse at the transformer AT 1 5 12 0 temperature fuse 16 0 temperature fuse 1 phase Performance data Max speed rpm Max capacity ml Max gravitational field x g Max kinetic energy Nm 4 700 840 4 470 20 078 Other parameters Time range Temperature range Storage locations 10 sec 99 h 59 min 59 sec short run continuous run 10 C to 40 C 50 Physical data Hei...

Page 66: ...ture NOTE At a nominal voltage of 100V or 200V a tolerance of 10 5 applies For indoor use only Allowable ambient temperature 5 C to 35 C Max allowable relative humidity of air 80 from 5 C up to 31 C with a linear decrease to 67 relative humidity of air at 35 C Maximum altitude 2 000 m above sea level 10 2 Technical documentation For environmental reasons the comprehensive technical documentation o...

Page 67: ...H An der Unteren Söse 50 37520 Osterode Germany Tel 49 0 55 22 50 07 82 13 Fax 49 0 55 22 50 07 92 13 E mail info sigma zentrifugen de DANGER Rotors and accessories of the standard centrifuge 4 5L must not be used in a robot controlled centrifuge without consultation with the manufacturer 11 1 1 Rotor radii The information in the accessories table concerning the radius refers to the values of the ...

Page 68: ... 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix 68 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual 11 2 Speed gravitational field diagram Fig 34 Speed gravitational field diagram ...

Page 69: ... It decelerates brakeless spin out In general the runtime until the set speed is reached depends on the moment of inertia of the rotor Linear curves The slope of the fixed acceleration curves defines the time that is required to accelerate the rotor by 1 000 rpm Curve 9 is a special case compared to the other curves The centrifuge accelerates with maximum power The runtime until the set speed is r...

Page 70: ...6KS 4 16KHS 6 16S 6 16HS 6 16KS 6 16KHS 9366 15 000 4 5KL 4 16S 4 16KS 4 16KHS 6 16S 6 16HS 6 16KS 6 16KHS 11805 10 years 8KS 8KBS 11806 10 years 8KS 8KBS 12082 7 years 1 14 1 14K 12083 7 years 1 14 1 14K 12084 7 years 1 14 1 14K 12085 7 years 1 14 1 14K 12092 5 years 20x 1 14 1 14K 12093 5 years 20x 1 14 1 14K 12094 5 years 20x 1 14 1 14K 12096 5 years 20x 1 14 1 14K 12097 5 years 20x 1 14 1 14K ...

Page 71: ...lonitrile C3H3N 100 1 1 4 3 3 4 4 4 1 4 1 Allyl alcohol C3H6O 96 1 3 3 2 2 2 2 4 1 1 1 Aluminium chloride AlCl3 saturated 1 3 2 4 1 1 1 1 4 Aluminium sulfate Al2 SO4 3 10 1 1 1 3 1 1 1 1 1 1 1 Ammonium chloride NH4 Cl aqueous 1 1 1 2 1 1 1 1 1 1 3 Ammonium hydroxide NH3 H2O 30 1 3 4 1 1 2 1 1 1 Aniline C6H7N 100 1 3 4 1 2 4 4 4 1 4 1 Anisole C7H8O 100 3 4 4 1 4 4 2 1 4 1 Antimony trichloride SbCl3...

Page 72: ...00 1 2 1 3 1 2 1 Diaminoethane C2H8N2 100 1 1 3 1 1 3 4 1 1 1 Diesel fuel 100 1 1 3 1 1 1 3 1 1 1 Dimethyl formamide DMF C3D7NO 100 1 1 4 1 1 4 3 1 3 1 Dimethyl sulfoxide DMSO C2H6SO 100 1 2 4 1 1 4 4 1 1 Dimethylaniline C8H11N 100 3 4 2 4 1 1 Dioxane C4H8O2 100 2 1 4 1 3 2 3 4 1 3 1 Dipropylene glycol mono methyl ether C4H10O 100 3 1 4 1 4 4 4 4 1 1 Ethyl acetate C4H8O2 100 1 1 4 1 1 4 4 4 1 4 1 ...

Page 73: ...lcohol CH4O 100 1 2 4 1 1 3 1 3 1 2 1 Methyl benzene C7H8 100 3 1 4 1 3 4 4 4 1 4 1 Methyl ethyl ketone MEK C4H8O 100 1 1 4 1 1 4 4 4 1 4 1 Methylene chloride CH2Cl2 100 4 3 4 3 3 4 4 4 1 1 Mineral oil 100 1 1 1 1 1 1 1 1 1 1 Nitric acid HNO3 10 1 4 1 4 1 1 1 1 4 3 Nitric acid HNO3 100 4 4 4 4 4 4 1 4 1 Nitrobenzene C6H5NO2 100 3 4 4 3 2 4 4 4 1 4 1 Oleic acid C18H34O2 100 1 1 1 2 1 1 1 3 1 Oxalic...

Page 74: ...ide NaCl 30 1 1 1 1 1 1 1 1 1 1 3 Sodium hydroxide NaOH 30 1 1 4 1 1 1 1 1 1 2 4 Sodium hydroxide NaOH 50 1 1 4 1 1 1 1 1 2 4 Sodium sulfate Na2SO4 10 1 1 1 1 1 1 1 1 1 1 1 Spirits C2H6O 96 1 1 1 1 1 1 1 3 1 1 Styrene C8H8 100 4 1 4 1 3 4 4 1 4 1 Sulphuric acid H2SO4 6 1 4 1 4 1 1 1 1 2 3 Sulphuric acid H2SO4 fuming 4 4 4 4 4 4 4 4 1 4 3 Tallow 100 1 1 1 1 1 1 1 1 1 1 Tetrahydrofuran THF C4H8O 100...

Page 75: ... Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix Version 11 2017 Rev 1 7 1 of 08 12 2022 sb 75 113 Translation of the original operating manual 11 6 Serial Control Interface Specification ...

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Page 97: ...gerated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix Version 11 2017 Rev 1 7 1 of 08 12 2022 sb 97 113 Translation of the original operating manual ...

Page 98: ...gerated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix 98 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual ...

Page 99: ...gerated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix Version 11 2017 Rev 1 7 1 of 08 12 2022 sb 99 113 Translation of the original operating manual ...

Page 100: ...erated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix 100 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual ...

Page 101: ...or Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix Version 11 2017 Rev 1 7 1 of 08 12 2022 sb 101 113 Translation of the original operating manual Lars 11 7 EC declaration of conformity ...

Page 102: ...erated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix 102 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual ...

Page 103: ...erated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix Version 11 2017 Rev 1 7 1 of 08 12 2022 sb 103 113 Translation of the original operating manual ...

Page 104: ...erated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix 104 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual ...

Page 105: ...Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix Version 11 2017 Rev 1 7 1 of 08 12 2022 sb 105 113 Translation of the original operating manual 11 8 Declaration of conformity China RoHS 2 ...

Page 106: ...erated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix 106 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual ...

Page 107: ...for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix Version 11 2017 Rev 1 7 1 of 08 12 2022 sb 107 113 Translation of the original operating manual 11 9 UKCA declaration of conformity ...

Page 108: ...erated Centrifuge for Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD 11 Appendix 108 113 Version 11 2017 Rev 1 7 1 of 08 12 2022 sb Translation of the original operating manual ...

Page 109: ...elerates during operation 51 Centrifuge is inclined 51 Centrifuge lid 11 Centrifuge was moved during run 51 Centrifuge cleaning and care 55 Centrifuge service life 26 Changes in colour 60 Changes in structure 60 Check commands 49 Chemical and biological safety 24 Chemical resistance of plastic 57 China RoHS 2 Declaration of conformity105 Cleaning agents 59 Cleaning the bores of angle rotors 56 Cle...

Page 110: ...articles 59 Global warming potential GWP 65 Gravitational field 65 Grease for load bearing bolts 10 55 58 H Hard running noise during the centrifugation 51 Hazard warnings 9 34 36 Heavy duty grease for load bearing bolts 10 58 Hexagon socket wrench 10 Highly corrosive substances 23 I Imbalance 34 36 Imbalance error 53 Imbalance monitoring system 27 Importance of the operating manual 9 Important in...

Page 111: ...rd to the life and health 18 Potentially hazardous situation 18 Power consumption 13 65 Power cord is not plugged in 51 Power failure 52 Power supply 31 Preselection of a curve 44 Pressure refrigerant 65 Pressure marks 57 Prevention of accidents 9 Problem description 62 Process error 53 Process values 49 ProgLock program lock 44 Program Rapid Temp 42 Program lock ProgLock 44 Protection class 31 65...

Page 112: ...ed personnel 20 Speed 13 16 39 65 Speed gravitational field diagram 68 Speedometer error 53 Standards and regulations 10 Standstill monitoring system 27 Starting a centrifugation run 38 Status of the centrifuge 49 Sterilisation of the rotor chamber and accessories 59 Stopping of the centrifuge due to an imbalance 58 Storage and transport 29 Storage conditions 29 Storage locations 65 Stress corrosi...

Page 113: ...or Robot Use Sigma 4 5KRL Refrigerated Centrifuge for Robot Use Sigma 4 5KRL IVD Index Version 11 2017 Rev 1 7 1 of 08 12 2022 sb 113 113 Translation of the original operating manual W Warranty and liability 9 Wear 61 Weight 29 ...

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