51
Decontamination and Cleaning
Fusion Mixtures
Dissolving a sample by reacting with a fusion-flux mixture is generally chosen
when other techniques for sample dissolution fail. The fusion-flux mixture should
be carefully selected. Knowledge of fusion-flux mixture/crucible compatibility is
essential. Heating the sample-flux mixture may initiate a vigorous or explosive
reaction.
•
Heat the mixture slowly and intermittently until the system is characterized.
•
If you use a muffle furnace rather than a flame for heating, make a trial using
the standard amount of flux but with a smaller amount of sample.
•
Most reacted fusion mixtures are dissolved in acidic solutions. Observe the
precautions described previously for handling acids.
Decontamination and Cleaning
Before using any cleaning or decontamination methods except those specified by
PerkinElmer, users should check with PerkinElmer that the proposed method will
not damage the equipment.
Decontamination
Customers wishing to return instrumentation and/or associated materials to
PerkinElmer for repair, maintenance, warranty or trade-in purposes are
advised that all returned goods must be certified as clean and free from
contamination.
Caution
The fusion matrix will deposit on and dissolve the quartz torch over time.
It is recommended to use the unslotted (0 slots) torch because the
slotted torches will dissolve much faster.
Attention: La matrice de fusion déposera sur et dissoudre le flambeau de
quartz au cours du temps.
Il est recommandé d'utiliser la non fendue (0
fentes) torche parce que les torches fendues vont se dissoudre
beaucoup plus vite.
Summary of Contents for AVIO 200
Page 1: ...AVIO 200 SPECTROMETER Hardware Guide ICP OPTICAL EMISSION ...
Page 2: ......
Page 3: ...AvioTM 200 Spectrometer Customer Hardware and Service Guide ...
Page 12: ...Contents 10 ...
Page 30: ...28 ...
Page 31: ...Safety Practices 1 ...
Page 32: ...30 Safety Practices ...
Page 56: ...54 Safety Practices ...
Page 57: ...Preparing Your Laboratory 2 ...
Page 58: ...Preparing Your Laboratory 56 ...
Page 70: ...Preparing Your Laboratory 68 ...
Page 71: ...System Description 3 ...
Page 72: ......
Page 97: ...Installation 4 ...
Page 98: ......
Page 119: ...Installation 117 Figure 4 8 Replacing the torch 1 3 4 6 8 2 9 10 5 7 ...
Page 121: ...Installation 119 1 2 7 9 8 10 3 4 5 6 ...
Page 164: ...Installation 162 ...
Page 165: ...Maintenance 5 ...
Page 166: ......
Page 184: ...Maintenance 182 1 2 7 9 8 10 3 4 5 6 ...
Page 188: ...Maintenance 186 Figure 5 8 Replacing the Torch 1 3 4 6 8 2 9 10 5 7 ...
Page 272: ...Maintenance 270 ...
Page 273: ...Troubleshooting 6 ...
Page 274: ......
Page 293: ...Troubleshooting 291 Figure 6 1 Normal Plasma Conditions at 0 torch position ...
Page 294: ...Troubleshooting 292 Figure 6 2 Normal Plasma at 3mm position ...
Page 297: ...Troubleshooting 295 Figure 6 5 Injector too far forward ...
Page 298: ...Troubleshooting 296 Figure 6 6 No Aux Gas Torch may be glowing ...
Page 299: ...Troubleshooting 297 Figure 6 7 Air Leak or Spray Chamber Temperature too high ...
Page 300: ...Troubleshooting 298 Figure 6 8 Thin Plasma due to leak in Plasma Gas Line ...
Page 308: ......