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Maintenance
195
Etching the Cyclonic Spray Chamber
The cyclonic spray chamber can be etched in order to improve drainage using the
following procedure. However, if you will be using the cyclonic spray chamber in
determinations of silicon, this procedure should
not
be used.
1. Prepare a 0.5% solution of hydrofluoric acid (HF), observing the precautions
listed above.
2. Ignite the plasma.
3. Aspirate the HF solution for between 1 and a maximum of 2 minutes.
4. At first, you will see beads of water inside the cyclonic spray chamber, then after
approximately 30 seconds, the beads will begin to disappear.
5. Aspirate a rinse solution for several minutes.
Hydrofluoric acid — toxic and corrosive.
Hydrofluoric acid (HF) is toxic,
extremely
corrosive, and can cause
severe burns.
Hydrofluoric acid will readily burn skin, and if the
fumes are inhaled, lung tissue. Burns may not be immediately painful
or visible. Contact with eyes could result in blindness.
•
When using hydrofluoric acid, always wear suitable protective
clothing including a face mask, work in a fume hood, and observe the
manufacturer’s instructions and your local safety regulations.
Avertissement: L'acide fluorhydrique - toxique et corrosif.
L'acide fluorhydrique (HF) est toxique, extrêmement corrosif et peut
causer des brûlures graves.
L'acide fluorhydrique sera facilement
brûler la peau, et si les vapeurs sont inhalées, les tissus pulmonaires.
Les brûlures peuvent ne pas être immédiatement douloureuses ou
visibles. Contact avec les yeux peut entraîner la cécité
.
•
Lors de l'utilisation de l'acide fluorhydrique, toujours porter des
vêtements de protection appropriés, y compris un masque, le travail
dans une hotte, et observer les instructions du fabricant et vos règles
de sécurité locales.
!
Warning
!
Warning
Summary of Contents for AVIO 200
Page 1: ...AVIO 200 SPECTROMETER Hardware Guide ICP OPTICAL EMISSION ...
Page 2: ......
Page 3: ...AvioTM 200 Spectrometer Customer Hardware and Service Guide ...
Page 12: ...Contents 10 ...
Page 30: ...28 ...
Page 31: ...Safety Practices 1 ...
Page 32: ...30 Safety Practices ...
Page 56: ...54 Safety Practices ...
Page 57: ...Preparing Your Laboratory 2 ...
Page 58: ...Preparing Your Laboratory 56 ...
Page 70: ...Preparing Your Laboratory 68 ...
Page 71: ...System Description 3 ...
Page 72: ......
Page 97: ...Installation 4 ...
Page 98: ......
Page 119: ...Installation 117 Figure 4 8 Replacing the torch 1 3 4 6 8 2 9 10 5 7 ...
Page 121: ...Installation 119 1 2 7 9 8 10 3 4 5 6 ...
Page 164: ...Installation 162 ...
Page 165: ...Maintenance 5 ...
Page 166: ......
Page 184: ...Maintenance 182 1 2 7 9 8 10 3 4 5 6 ...
Page 188: ...Maintenance 186 Figure 5 8 Replacing the Torch 1 3 4 6 8 2 9 10 5 7 ...
Page 272: ...Maintenance 270 ...
Page 273: ...Troubleshooting 6 ...
Page 274: ......
Page 293: ...Troubleshooting 291 Figure 6 1 Normal Plasma Conditions at 0 torch position ...
Page 294: ...Troubleshooting 292 Figure 6 2 Normal Plasma at 3mm position ...
Page 297: ...Troubleshooting 295 Figure 6 5 Injector too far forward ...
Page 298: ...Troubleshooting 296 Figure 6 6 No Aux Gas Torch may be glowing ...
Page 299: ...Troubleshooting 297 Figure 6 7 Air Leak or Spray Chamber Temperature too high ...
Page 300: ...Troubleshooting 298 Figure 6 8 Thin Plasma due to leak in Plasma Gas Line ...
Page 308: ......