Lauda PD 12 R Operating Instructions Manual Download Page 1 | Manualshive

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Operating Instructions

Puridest Distillation Apparatus
PD 2 R, PD 4 R, PD 8 R, PD 12 R

DOMINIQUE

DUTSCHER

SAS

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Summary of Contents for PD 12 R

Page 1: ...Operating Instructions Puridest Distillation Apparatus PD 2 R PD 4 R PD 8 R PD 12 R D O M I N I Q U E D U T S C H E R S A S ...

Page 2: ...2 30 Puridest Distillation Apparatus 09 2020 D O M I N I Q U E D U T S C H E R S A S ...

Page 3: ...ational pharmacopeia I II III IV I Main switch II Pilot lamp Clean III Operation pilot lamp IV Distillate withdrawal Before installation please check whether contents of package are in good order and complete Should you note any damages or have any reasons for complaint please contact your supplier or directly LAUDA GFL Gesellschaft für Labortechnik mbH Schulze Delitzsch Str 4 5 30938 Burgwedel De...

Page 4: ...4 30 Puridest Distillation Apparatus 09 2020 D O M I N I Q U E D U T S C H E R S A S ...

Page 5: ...ance Service and Trouble Shooting 12 Descaling 12 9 1 Pilot Lamp Clean 12 9 2 9 2 1 Foam formation caused by polluted water in the boiler 12 9 2 2 Back water in the boiler 13 Re initiation after low water 13 9 3 10 Disposal of Old Units 13 11 Technical Data 14 Distillation Apparatus Puridest models PD 2 R PD 4 R 14 11 1 Distillation Apparatus Puridest models PD 8 R PD 12 R 15 11 2 12 Circuit Diagr...

Page 6: ... of 220 V 3 PE 50 60 Hz 21 13 1 4 PD 8 R for 230 V 1 for a mains supply of 400 V 3 N PE 50 60 Hz 21 13 1 5 PD 8 R and PD 12 R for 220 V 3 for a mains supply of 220 V 3 PE 50 60 Hz 22 13 1 6 PD 8 R and PD 12 R for 220 V 3 for a mains supply of 220 V 3 PE 50 60 Hz 22 13 1 7 PD 8 R and PD 12 R for 400 V 3 for a mains supply of 400 V 3 N PE 50 60 Hz 23 13 1 8 PD 8 R and PD 12 R for 400 V 3 for a mains...

Page 7: ...ating instructions must by all means be read and observed Only then a perfect operation of the Distillation Apparatus can be guaranteed The units may only be installed and operated by persons who have made themselves familiar with these operating instructions Caution The accessible inner parts of the housing that can be reached after lifting the outer lid get strongly heated up during operation Th...

Page 8: ... only suitable for indoor use Table top setting up on solid even and level surfaces only Make sure to place the unit only on a watertight temperature resistant non flammable surface The location must provide sufficient space as well as the necessary carrying capacity for the total weight of the unit unit weight as per technical data chapter 11 of this manual plus weight of the filling For setting ...

Page 9: ...mains must be installed in such a way as to ensure they can be clearly identified and are easily accessible at any time The mains connection cable must not touch any hot surfaces of the unit It may not lead underneath the unit The main switch I of the Distillation Apparatus must be off position O The voltage on the nameplate at the left hand side of the unit must be identical to the mains voltage ...

Page 10: ...lation Apparatus with a temperature of up to 100 C Danger of scaldings Cooling water outlet l 6 3 Connect a temperature resistant hose to the cooling water outlet It may have a maximum length of approx 1 5 m It must be led into an open drain on a lower level and must have a slope on its complete length Make sure the cooling water can drain without back draughts Caution cooling water leaves the Dis...

Page 11: ...lves of the water supply then empty and dry storage tank and boiler in order to avoid germ contamination 8 Functional Description LAUDA GFL Distillation Apparatuses Puridest work automatically After switching on the Distillation Apparatus main switch the green pilot lamp in the main switch I as well as the right hand yellow operation pilot lamp III will light up The built in solenoid valve opens W...

Page 12: ...tainless steel can also be used according to the manufacturer s in structions e g rea calc of M s CHEMOTEC GmbH 63486 Bruchköbel Germany Never use any products con taining hydrochloric acid These will lead to damages to heating element boiler temperature sensor and the ducts of the screw connections Restart the unit as described in chapter 7 Initiation After descalings the first few litres of dist...

Page 13: ...ly then switch the unit back on again The LAUDA GFL Distillation Apparatus Puridest is made of first class material Nevertheless the unit should only be subjected to mechanical strain within sensible limits Make sure that no fluids come into contact with cable connections or the electrical parts inside the unit The powder coated surfaces of the unit can be cleaned with mild detergents if necessary...

Page 14: ...with capil lary tube sensor Switch off temperature 135 C 15 K Electromechanical temperature limiter with capil lary tube sensor Switch off temperature 135 C 15 K Water pressure min max 3 bar 7 bar 43 5 psi 101 5 psi 3 bar 7 bar 43 5 psi 101 5 psi Electrical connection Mains supply 230 V 10 50 60 Hz 1 5 kW shock proof plug 230 V 10 50 60 Hz 3 0 kW shock proof plug Caution Mains voltage deviations e...

Page 15: ... bar 43 5 psi 101 5 psi Electrical connection Mains supply On site fuse 230 V 10 50 60 Hz 6 0 kW Connection box for permanent connection to the mains Netzsicherung on site fuse 35 Amp 220 V 3 PE 10 50 60 Hz 9 0 kW Mains connection cable for permanent connection to the mains on site fuse 3 x 25 Amp 220 V 3 PE 10 50 60 Hz 6 0 kW Mains connection cable for permanent connection to the mains on site fu...

Page 16: ...tion Elektr 1 Electrode cleaning in boiler Elektr 2 Electrode water blocking Elektr 3 Electrode max level storage tank F1 Mains fuse internal Model PD 2 R 10 Amp inert Model PD 4 R 15 Amp inert F2 Mains fuse internal Model PD 2 R 8 Amp inert Model PD 4 R 15 Amp inert F3 Low water cut off thermostat K1 Contactor M Earth housing S1 Main switch Y1 Solenoid valve PD 2 R 12 1 D O M I N I Q U E D U T S ...

Page 17: ...09 2020 Puridest Distillation Apparatus 17 30 PD 4 R 12 2 PD 8 R version 230 V 1 for permanent connection to the mains 12 3 see nameplate D O M I N I Q U E D U T S C H E R S A S ...

Page 18: ...paratus 09 2020 PD 8 R PD 12 R version 220 V 3 for permanent connection to the mains 12 4 see nameplate PD 8 R PD 12 R version 400 V 3 for permanent connection to the mains 12 5 see nameplate D O M I N I Q U E D U T S C H E R S A S ...

Page 19: ... 50 60 Hz ge gr gelb grün PE Protective earth PE Protective earth bl blue N sw black L1 L1 br brown L2 L2 gra grey L3 L3 Distillation Apparatuses can be supplied in different versions for connection to different mains supplies Models PD 2 R and PD 4 R for connection to 230 V see nameplate can be connected to all mains supplies with 220 V or 230 V Models PD 8 R and PD 12 R for connection to 220 V 3...

Page 20: ... fuse on site F4 Mains fuse on site S4 Main switch on site 13 1 1 PD 2 R and PD 4 R for 230 V for a mains supply of 220 V 3 PE 50 60 Hz see nameplate PD 2 R and PD 4 R Mains connection through shock proof plug CEE 7 7 pre assembled all pole separable from the mains 13 1 2 PD 2 R PD 4 R for 230 V for a mains supply of 400 V 3 N PE 50 60 Hz see nameplate PD 2 R and PD 4 R Mains connection through sh...

Page 21: ...ch S4 all pole sepa rable from the mains Connection cable not in scope of supply 13 1 4 PD 8 R for 230 V 1 for a mains supply of 400 V 3 N PE 50 60 Hz see nameplate PD 8 R Mains connection through CEE plug in conformity with IEC standard 60309 2 all pole separable from the mains Con nection cable and CEE plug not in scope of supply D O M I N I Q U E D U T S C H E R S A S ...

Page 22: ...Mains connection through on site switch S4 all pole sepa rable from the mains 13 1 6 PD 8 R and PD 12 R for 220 V 3 for a mains supply of 220 V 3 PE 50 60 Hz see nameplate PD 8 R PD 12 R Mains connection through CEE plug in conformity with IEC standard 60309 2 plug not pre assembled all pole separable from the mains D O M I N I Q U E D U T S C H E R S A S ...

Page 23: ...Mains connection through on site switch S4 all pole sepa rable from the mains 13 1 8 PD 8 R and PD 12 R for 400 V 3 for a mains supply of 400 V 3 N PE 50 60 Hz see nameplate PD 8 R PD 12 R Mains connection through CEE plug in conformity with IEC standard 60309 2 plug not pre assembled all pole separable from the mains D O M I N I Q U E D U T S C H E R S A S ...

Page 24: ...e 15 Amp inert for PD 4 R 6 A000091 Contactor 7 0014325 Stand 8 A000127 Main switch 9 0012635 LED pilot lamp red 10 92002019 Dust guard shield 11 0017427 Profiled silicon sealing 12 0016214 Cooling coil for PD 2 R A000110 Cooling coil for PD 4 R A000111 Cooling coil for PD 8 R 0016205 Cooling coil for PD 12 R 0025232 Nut 0017339 Seal 13 0015115 Hose spout for cooling water outlet 0015116 Nut 00173...

Page 25: ...09 2020 Puridest Distillation Apparatus 25 30 5 1 5 2 Please always state model and serial no of the Distillation Apparatus when placing an order for spare parts D O M I N I Q U E D U T S C H E R S A S ...

Page 26: ...lustration Separate Water Supply with solenoid valve Only factory installation into models PD 2 R to PD 12 R is possible When the storage tank is full the solenoid valve switches off pretreated water automatically Part No is depending on the Model of the Distillation Apparatus without illustration Dechlorite Filter eliminates chlorine particles in tap water added by the local waterworks Complete w...

Page 27: ...r one filter and fillings mounted completely Part No A000136 Part No A000135 Hose Set consisting of hoses for water inlet and outlet length 1 5 m including hose clips Hose Set Part No A000138 Level Control Switch Only factory installation into models PD 2 R to PD 12 R is possible When connecting an external storage tank not included in the scope of supply to the Distillation Apparatus it is recom ...

Page 28: ...28 30 Puridest Distillation Apparatus 09 2020 D O M I N I Q U E D U T S C H E R S A S ...

Page 29: ...09 2020 Puridest Distillation Apparatus 29 30 D O M I N I Q U E D U T S C H E R S A S ...

Page 30: ...ellschaft für Labortechnik mbH Schulze Delitzsch Straße 4 5 30938 Burgwedel Deutschland Tel 49 0 5139 9958 0 Fax 49 0 5139 9958 21 E Mail info lauda gfl de Internet www GFL de D O M I N I Q U E D U T S C H E R S A S ...

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