Koehler K41091 Operation And Instruction Manual Download Page 11

K41091 Micro Carbon Residue and Ash Tester 

Operation and Instruction Manual 

 

K41091-Manual

    

 

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The  maximum  time  duration  is  240  minutes  per 
segment.  The  type  of  gas  flow  to  choose  from  is 
listed in section 5.1 of this manual.  
 

NOTE:

  The  Temperature  Rate  must  not  exceed 

15°C per minute in order to maintain the condition 
of the Furnace.  
 

Creation or Modification: 

 

1. 

From  the  main  menu  press  the 

“Go”

  key 

located at the bottom left corner of the screen.  

 

2. 

Next  press  the 

“Program”

  key  at  the  bottom 

right corner of the screen.  

 

3. 

Enter the number of the program to modify or 
create.  This  will  bring  you  to  the  screen 
illustrated in Figure 9 below.  

 

 

 

Figure 9: Program Parameter Screen 

 

4. 

Pressing  the 

“Validate  the  Parameter”

  key 

displays the type of gas and flow available.  

 

5.  Alphanumeric Keyboard Function.

 Pressing 

the 

“A…Z”

  key  displays  a  table  with  column 

headings and lines allowing the user to select 
a letter, figure or symbol for inputting a sample 
ID or naming a newly created program. Please 
see Figure 10 below: 

 

6.  Weight  Input  Function.

  This  function  makes 

it possible to enter the weights of the samples 
so  that  the  apparatus  can  make  a  calculation 
after  the  weights  entered  at  the  end  of  the 
test.  When  entering  a  weight  value,  the 
numbers  will  start  on  the  operators  left  and 
scroll  to  the  right  as  additional  numbers  are 
entered. To  enter  the  desired  value  it  may  be 
required to enter a number of “Zeros” after the 
value has been entered. The standard number 
of significant figures is shown below: 

 

XX.XXXXX G 

 
For  example,  to  enter  2.45  G,  the  user  must 
enter  2,  then  4,  then  5  followed  by  three 
Zeros.  This  places  the  two  (2)  in  the  single 
digit place resulting in the desired value.  
 

7.  Set  Point  Function.

  This  function  allows  the 

user  to  input  the  idle  set  point  temperature  of 
the  furnace  between  tests.  This  value  is 
limited to the range from 20 to 80°C 

 

8.  Standby  Function.

  This  function  allows  the 

user  to  shut  down  the  apparatus  via  the 
control  panel  without  having  to  switch  off  the 
circuit  breaker  or  push  the  emergency  stop 
button.  This  method  of  shut  down  avoids 
restarting the circuit breaker at the time of the 
next  power  up.  Upon  activation  of  this 
function,  the  instrument  automatically  shuts 
down after a few seconds.  

 

5.3.2  Software Configuration Functions 

 

The  following  functions  are  accessible  via  the 

Software Function

.  

 
From  the  main  menu  press  the 

“Configuration 

Key

  located  at  the  bottom  right  corner.  During 

this functions

’ first use a password is not required 

to enter this menu. A password must be created in 
the “New Password” function screen to implement 
this  security  feature.  Once  in  the  Software 
Function  Menu,  press  next  and  enter  the  “New 
Password Function” screen. See step  5 below for 
further detail on this function.  
 

1.  Buzzer  Function. 

This  function  allows  the 

user  to  choose  between  a  continuous  buzzer 
that  sounds  at  the  end  of  the  test  until  the 
operator turns it off or a buzzer that sounds for 
3 minutes. 

 

 
2.  Stop  Ventilation  Function. 

This  function  is 

automatically  set  to  20°C  above  the  Idle  Set 
Point Temperature value.  The minimum value 
for  this  set  point  is  80°C.  The  fan  starts  at 
500°C  and  stops  at  the  Idle  set  point  plus 
20°C. 

 

 
3.  Stop  Safety  Function. 

This  function  allows 

the user to set a safety temperature limit.

 

This 

temperature  is  measured  on  the  Furnace 
temperature  probe.  If  a  malfunction  occurs 
and  the  temperature  of  the  furnace  exceeds 
this value, the microprocessor cuts the heating 

Summary of Contents for K41091

Page 1: ... Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analysis Instrumentation Custom Design Manufacturing K41091 Micro Conradson Carbon Residue and Ash Tester ...

Page 2: ......

Page 3: ...scriptions Back 5 5 Operation 6 5 1 Instrument Start up 6 5 2 Starting a Test 7 5 3 Control Panel Operation 8 5 3 1 Creation of New Programs 8 5 3 2 Software Configuration Functions 9 5 3 3 Hardware Configuration Functions 10 6 Maintenance 11 6 1 Maintenance Checks 11 6 2 Routine Maintenance 11 6 2 1 Cleaning of Furnace Opening and Hot Lid 11 6 2 2 De Carbonizing the Furnace 11 6 2 3 Temperature C...

Page 4: ...ehler for a full range of accurate and reliable instrumentation as well as support for your laboratory testing programs Please do not hesitate to contact us at any time with your inquiries about equipment tests or technical support Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 Email info koehlerinstrument com http www koehlerinstrument com 1 2 Recommended Resources and Pub...

Page 5: ...ions The use of this equipment may involve hazardous materials and operations This manual does not purport to address all of the safety problems associated with the use of this equipment It is the responsibility of any user of this equipment to investigate research and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use Equipment...

Page 6: ...artz sample vial re usable Ash Content Test K41000 5 16 ml Quartz sample vial re usable Ash Content Test K41000 8 4 ml Borosilicate glass sample tube MRC test 3 2 Unpacking Carefully unpack and place the instrument and accessories in a secure location Ensure that all items listed on the packing list are present Inspect the unit and all accessories for damage If any damage is found keep all packing...

Page 7: ...rns off the power to the entire unit 4 Numeric Keypad For entering sample data and parameter values for testing 5 Key Function Buttons For navigation through the instruments sub menus Note The function of these buttons and subsequent display icons will change depending on the menu the user is in 6 Display For user friendly control of the instrument 7 Insulating Cover For enhanced temperature stabi...

Page 8: ... an attempt to further evacuate the exhaust fumes The chimney must remain free to ensure optimal exhaust of the system Any connection on the chimney or its extension pipe would be likely to cause Condensates in the piping of the apparatus A backpressure which would disturb the test by modifying the flows and cause leaks on the hot lid of the furnace 2 Connect the line cord to properly fused and gr...

Page 9: ...cting an External PC to Serial Line 1 and using the Data Acquisition Software provided with the accessories of the instrument NOTE The calculation of residue percentage can also be determined by the apparatus Inputting the initial and final weight of the samples into the software will then calculate the residue percentage automatically 5 2 Starting a Test WARNING For either program selected the In...

Page 10: ...ntage ratio of residue remaining at the end of the test 13 Choose the desired program Micro Carbon Residue or Ash 14 Confirm the launching of the test by pressing Go once again on the display panel 15 The instrument will then sound a series of beeps The display will now indicate the temperature of the furnace the duration of the test the current segment of the test program running and the limiting...

Page 11: ...e two 2 in the single digit place resulting in the desired value 7 Set Point Function This function allows the user to input the idle set point temperature of the furnace between tests This value is limited to the range from 20 to 80 C 8 Standby Function This function allows the user to shut down the apparatus via the control panel without having to switch off the circuit breaker or push the emerg...

Page 12: ...rature of the furnace Either in degrees Celsius or Fahrenheit 3 Calibration Function This function allows the user to calibrate the furnace temperature probe 3 1 Physical Calibration This calibration is done by entering three 3 temperature points via the keyboard Enter these points by first replacing the furnace thermocouple with a temperature simulator To do this open remove the furnace thermocou...

Page 13: ...e each test it is recommended to check the furnace exhaust The exhaust must be free from calamine If the apparatus has calamine deposits in the furnace exhaust it is recommended to remove the deposits using the cleaning cable provided 6 2 Routine Maintenance Depending on the frequency of use and the type of samples being tested it is recommended to perform routine maintenance procedures For exampl...

Page 14: ...its Check the state of the chimney and chimney extension pipe for calamine deposits and clean in the same manner 6 2 3 Temperature Check of the Furnace To check the temperature of the furnace it is necessary for a control thermocouple to be in place In order to make this possible the hot lid has a small thermocouple port located along the outside If the actual temperature of the furnace does not c...

Page 15: ...tension Pipe Gripping Hook Complete Furnace Furnace Thermocouple Safety Thermocouple Thermal Printer Paper for Thermal Printer Insulating Lid Small Vial Borosilicate Large Vial Borosilicate Long Vial Borosilicate Borosilicate Vial 12mm dia 72mm height Support for Porcelain Crucible Control Thermocouple w cable Furnace Thermocouple Calibration Cord Upstream Pressure Gauge Condensate Tank Joint for ...

Page 16: ...K41091 Micro Carbon Residue and Ash Tester Operation and Instruction Manual K41091 Manual 14 7 Diagrams 7 1 Flow Meter Calibration Chart ...

Page 17: ...K41091 Micro Carbon Residue and Ash Tester Operation and Instruction Manual K41091 Manual 15 7 2 Function Flow Chart ...

Page 18: ...the return of the product to the factory The sole responsibility of Koehler Instrument Company and the purchaser s exclusive remedy for any claim arising out of the purchase of any product is the repair or replacement of the product In no event shall the cost of the purchaser s remedy exceed the purchase price nor shall Koehler Instrument Company be liable for any special indirect incidental conse...

Page 19: ...K41091 Micro Carbon Residue and Ash Tester Operation and Instruction Manual K41091 Manual 17 Notes ...

Page 20: ...K41091 Micro Carbon Residue and Ash Tester Operation and Instruction Manual K41091 Manual 18 Notes ...

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