Knick A405B User Manual Download Page 98

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-05- Nitric acid HNO

-08-

Conductivity versus substance concentration and process temperature
for nitric acid (HN0

)

Source: Haase/Sauermann/Dücker; Z. phys. Chem. New Edition, Vol. 47 (1965)

Concentration measurement not possible in this range.

c [% by wt]

Concentration Curves

-05-

-08-

Summary of Contents for A405B

Page 1: ... X II 1G Ex ia IIC T3 T4 T6 SE 706X 2 NMSN 14163 Berlin BVS 10 ATEX E089 X II 1G Ex ia IIC T3 T4 T6 II 1G Ex ia IIC T3 T4 T6 SE 706X 1 NM 14163 Berlin BVS 10 ATEX E II 1G Ex ia IIC SE 706X 2 NM 14163 Berlin BVS 10 ATEX E II 1G Ex ia IIC x ia IIC T3 T4 T6 ATEX E 089 X SE 706X 2 NMS 14163 Berlin BVS 10 ATEX E0 II 1G Ex ia IIC T Stratos MS A405 Conductivity Measurement Latest Product Information www ...

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Page 3: ... Cable 15 Wiring Example SE 670 SE 680 16 Measuring Mode 17 The Keys and Their Functions 18 The Display 19 Display in Measuring Mode 20 Selecting the Mode Entering Values 21 Operating Modes 22 HOLD Mode 23 Operating Modes Functions 24 Connecting a Memosens Sensor 26 Replacing a Sensor 27 Configuration Overview 29 Device Type Cond CondI 32 Sensor Verification TAG GROUP 34 Output Current Range Curre...

Page 4: ...Wiring of Relay Contacts 58 Time and Date Measuring Point TAG GROUP 60 Calibration 63 Calibration with Calibration Solution 64 Product Calibration 66 Temp Probe Adjustment 68 Calibrating Toroidal Sensors 69 Calibration by Input of Cell Factor 70 Zero Calibration 71 Measurement 72 Diagnostics 73 Service 78 Error Messages 81 Sensocheck and Sensoface 83 Operating States 84 Product Range 85 Specificat...

Page 5: ...t Limit 1 hysteresis Limit 1 delay Relay Contacts Function Assignment Limit Values Example device type pH 1 Press menu key 2 Select CONF using keys press enter 3 Select RELAY1 menu using keys press enter Specify relay contact function LIMIT 4 All items of this menu group are indicated by the LM1 code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing ent...

Page 6: ...ocumentation available on our website www knick de Safety Instructions In official EU languages and others Quickstart Guides Installation and first steps Operation Menu structure Calibration Error messages and recommended actions Specific Test Report Electronic Documentation Manuals Software ...

Page 7: ... The sturdy molded enclosure is rated IP 67 NEMA 4X outdoor Material of front unit PBT rear unit PC Dimensions H 148 mm W 148 mm D 117 mm It is provided with knockouts to allow panel mounting 138 mm x 138 mm cutout to DIN 43700 wall mounting with sealing plugs to seal the enclosure post pipe mounting dia 40 60 mm 30 45 mm Protective hood accessory The protective hood provides additional protection...

Page 8: ... 6 5 4 1 2 3 Fig Assembling the enclosure 1 Jumper 3 x 2 Washer 1 x for conduit mounting Place washer between enclosure and nut 3 Cable tie 3 x 4 Hinge pin 1 x insertable from either side 5 Enclosure screw 4 x 6 Sealing insert 1 x 7 Rubber reducer 1 x 8 Cable gland M20x1 5 3 x 9 Filler plug 3 x 10 Hexagon nut 5 x 11 Sealing plug 2 x for sealing in case of wall mounting Overview of the Stratos MS ...

Page 9: ... conduit dia 21 5 mm 2 knockouts Conduit couplings not included 3 Knockout for pipe mounting 4 x 4 Knockout for wall mounting 2 x 6 2 Mounting Accessories Pipe mount kit accessory ZU 0274 Protective hood for wall and pipe mounting accessory ZU 0737 Panel mount kit accessory ZU 0738 All dimensions in mm ...

Page 10: ...ll and pipe mounting accessory ZU 0737 Fig Pipe mount kit accessory ZU 0274 1 Hose clamp with worm gear drive to DIN 3017 2 x 2 Pipe mount plate 1 x 3 For vertical or horizontal posts or pipes 4 Self tapping screw 4 x 1 2 3 4 ø40 ø60 Overview of the Stratos MS ...

Page 11: ...g Panel mount kit accessory ZU 0738 1 Circumferential sealing 1 x 2 Screw 4 x 3 Position of control panel 4 Span piece 4 x 5 Threaded sleeve 4 x Cutout 138 x 138 mm DIN 43700 Overview of the Stratos MS All dimensions in mm ...

Page 12: ... Output 1 HOLD input Output 2 Power RS 485 Memosens Terminal Assignments Rating Plates The terminals are suitable for single or stranded wires up to 2 5 mm2 AWG 14 Application in Hazardous Locations When using the device in a hazardous location observe the specifications of the Control Drawing ...

Page 13: ...nments Memosens connection Brown Green Yellow White Transp Current outputs OUT1 OUT2 Relay contacts REL1 REL2 Power supply Areas for placing the screwdriver to pull out the terminals 1 22 Overview of the Stratos MS Figure Terminals device opened back of front unit Connection of Memosens sensor Brown Green Yellow White Transp ...

Page 14: ...ic and Advanced www knick de Function selection The selected func tion is highlighted Connected sensor sensor type manu facturer order code and serial number measuring point and tag number Last adjustment Conductivity 1 010 mS cm Measured values Conductivity Resistance Temperature 1 010 mS cm 1 00 kΩ 25 C Sensor data Sensor type Manufacturer Order code Serial number Conductivity Knick SE630 MS 110...

Page 15: ...0 m Process temperature 20 C 135 C 4 275 F Ingress protection IP 68 Order Codes Cable type Cable length Order number Memosens Ferrules 3 m 5 m 10 m 20 m M12 plug 8 pin 3 m 5 m Memosens Ex Ferrules 3 m 5 m 10 m 20 m M12 plug 8 pin 3 m 5 m Other cable lengths or cable types are available on request Ex certified ATEX II 1G Ex ia IIC T3 T4 T6 Ga ...

Page 16: ...ensor to the RS 485 interface of the device When SE 670 SE 680K is selected as sensor in the Configuration menu the default values are taken as calibration data They can then be modified by calibration All calibration data of the SE 680M sensor with Memosens protocol are stored in the sensor Cable types M12 ferrules 5 m 10 m 20 m ...

Page 17: ...isplays as standard display for the measuring mode see page 20 Note By pressing the meas key in measuring mode you can view the displays for approx 60 sec Sensoface indicator sensor status Time Mode indicator measuring Hold meas key depressed for calling the measuring mode hitting the key once more switches the display Display indicates OUT1 e g measured value Display indicates OUT2 e g temperatur...

Page 18: ...rarily for approx 60 s info Retrieve information Show error messages menu Measuring mode Call menu Up Down arrows Menu Increase decrease a numeral Menu Selection Left Right arrows Menu Previous next menu group Number entry Move between digits enter Configuration Confirm entries next configuration step Calibration Continue program flow ...

Page 19: ... response time 4 Sensor data 5 Wear 6 Limit message Limit 1 or Limit 2 7 Alarm 8 Service 9 Not used 10 Calibration 11 Memosens sensor 12 Waiting time running 13 Info available 14 HOLD mode active 15 Primary process value 16 Secondary display 17 Proceed using enter 18 Not used 19 Diagnostics 20 Configuration mode 21 Calibration mode 22 Measuring mode 23 Sensoface 24 Unit symbols The Display ...

Page 20: ...play as MAIN DISPLAY displayed permanently in measuring mode The secondary display shows MAIN DISPLAY NO Use the UP DOWN arrows to select MAIN DISPLAY YES and confirm by pressing enter This display is now shown in measuring mode The MAIN DISPLAY is the display which is shown in measuring mode To call the mea suring mode from any other mode hold the meas key depressed for at least 2 sec Display in ...

Page 21: ...ssing enter To select the operating mode 1 Hold meas key depressed 2 s measuring mode 2 Press menu key the selection menu appears 3 Select operating mode using left right arrow key 4 Press enter to confirm the selected mode Selection menu Selected mode blinks 1 4 3 2 5 7 6 Selecting the Mode Entering Values ...

Page 22: ...tion the device can be adjusted In that case the device dis plays the actual value and internally corrects the measurement error of the sensor Calibration must be repeated at regular intervals The time between the calibration cycles depends on the load on the sensor During calibration the device is in HOLD mode During calibration the device remains in the HOLD mode until it is stopped by the opera...

Page 23: ... active 21 4 HOLD active Output current mA Output signal for HOLD FIX setting 21 0 mA Output signal for HOLD LAST setting Output signal during HOLD Output signal response LAST The output current is frozen at its last value Recommended for short configuration procedures The process should not change decisively during configuration Changes are not noticed with this setting FIX The output current is ...

Page 24: ...Current source output 2 Relay test Specifying access codes for operating modes Selecting the device type Reset to factory setting Access via code factory setting 5555 Display of calibration data Display of sensor data Self test RAM ROM EEPROM module 100 events with date and time Display of direct sensor values Display of software version model designation serial no Pressing the menu key down arrow...

Page 25: ...ters Pressing enter opens a menu item Use the arrow keys to edit a value Press enter to confirm save the settings Return to measurement Hold meas key depressed 2 s Select menu group Menu group Code Display Select menu item Sensor settings Menu item 1 Menu item Current output 1 Current output 2 Compensation Alarm mode Relay outputs LIMIT ALARM WASH Setting the clock Tag number Overview of Configura...

Page 26: ...Check sensor data MEMO SENS View sensor information using keys confirm using enter Sensoface is friendly when the sensor data are okay Go to measuring mode Press meas info or enter After 60 sec the device auto matically returns to measuring mode timeout Possible error message Sensor defective Replace sensor When this error message appears the sensor cannot be used Sensoface is sad Connecting a Mem...

Page 27: ...e or set to a fixed value Disconnect and remove old sensor Install and connect new sensor Temporary messages which are activated during the replace ment are indicated but not output to the alarm contact and not entered in the logbook Wait until the sensor data are displayed MEMO SENS Check sensor data MEMO SENS View sensor information using keys confirm using enter You can view the sensor manu fac...

Page 28: ...28 ...

Page 29: ...S cm xxxx μS cm x xxx mS cm xxxx mS cm xx xx mS cm xxx x mS cm x xxx S m xx xx S m xx xx MΩ Conc SOLUTION 01 NaCl 02 HCl 03 NaOH 04 H2 SO4 05 HNO3 06 H2 SO4 07 HCl 08 HNO3 09 H2 SO4 10 NaOH 11 H2 SO4 SO3 oleum TEMP UNIT C F CHECK TAG OFF ON CHECK GROUP OFF ON not for toroidal inductive conductivity sensors only for inductive conductivity measurement ...

Page 30: ...ions for bilinear characteristic Vertex X BEGIN CORNER X END rising BEGIN CORNER X END falling CORNER Y Default 12 mA Vertex Y 0 mA 4 mA CORNER Y 20 mA TMP C BEGIN 0 4 mA 50 250 C 000 0 C END 20 mA 50 250 C 100 0 C TMP F BEGIN 0 4 mA 58 482 F 032 0 F END 20 mA 58 482 F 212 0 F ERROR Output current for error message OFF FAIL FACE Sensoface FILTERTIME Output filter time interval 0 s 120 s 0 s filter...

Page 31: ...selected setting 0 50 full scale Relay 2 Default LIMIT FUNCTION Hi LEVL other settings like Relay 1 Time date CLK FORMAT 24 h 12 h 24 h hh mm 12 h hh mm AM PM 00 12 59 AM 1 11 59 PM DAY MONTH dd mm YEAR 2000 2099 Measuring points TAG GROUP The entries are made in the text line A Z 0 9 The entries are made in the text line 0000 9999 0000 ...

Page 32: ...xt page Confirm and proceed by pressing enter 4 Exit Press meas key until the meas mode indicator is displayed Select measuring mode Select measuring range Concentration determination Temperature unit CHECK TAG CHECK GROUP enter Configuration The device type is automatically selected upon first start up In the SERVICE menu you can change the device type Afterwards you must select the corresponding...

Page 33: ...firm x xxx μS cm xx xx μS cm xxx x μS cm xxxx μS cm x xxx mS cm xx xx mS cm xxx x mS cm x xxx S m xx xx S m xx xx MΩ Concentration determination For conc measurement only Select desired concentration solution using keys Press enter to confirm 01 NaCl 02 HCl 03 NaOH 04 H2 SO4 05 HNO3 06 H2 SO4 07 HCl 08 HNO3 09 H2 SO4 10 NaOH 11 H2 SO4 SO3 oleum Temperature unit Select C or F using keys Press enter...

Page 34: ...f this menu group are indicated by the SNS code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 4 Exit Press meas key until the meas mode indicator is displayed Configuration Select measuring mode Select measuring range Concentration determination Temperature unit CHECK TAG CHECK GROUP ...

Page 35: ...G or group of measuring points GROUP in the sensor TAG and GROUP can be specified by the calibration tool or automatically entered by the transmitter When connecting an MS sensor to the transmitter it can be checked if the sensor con tains the correct TAG or belongs to the correct GROUP If not a message will be generated and Sensoface gets sad The sad Sensoface icon can also be signaled by a 22 mA...

Page 36: ...rrent Range Current Start End Example current output 1 device type Cond 1 Press menu key 2 Select CONF using press enter 3 Select OUT1 menu using keys press enter 4 All items of this menu group are indicated by the OT1 code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed Configurin...

Page 37: ...ss variable range If the adjusted range is exceeded the device automati cally switches to the next higher range Autorange Current end Enter value using keys Press enter to confirm Entered value applies to selected process variable range If the adjusted range is exceeded the device automati cally switches to the next higher range Autorange Assignment of measured values Current start and current end...

Page 38: ...ing HOLD Output current for HOLD FIX Output Current Curve Example Current Output 1 1 Press menu key 2 Select CONF using press enter 3 Select OUT1 menu using keys press enter 4 All items of this menu group are indicated by the OT1 code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed...

Page 39: ...he next higher range Autorange Bilinear curve Vertex X Y Enter value using keys Press enter to confirm Entered value applies to selected vertex of bilinear curve Corner X process variable and Corner Y output current see figure below Vertex of bilinear curve Output current Process variable Example Current range 4 20 mA Current start 0 µS cm Current end 200 µS cm Vertex CORNER X 10 µS cm process var...

Page 40: ...me units either in µS cm or in S m see listing 1 0 µS cm 10 0 µS cm 0 001 S cm 100 0 µS cm 0 01 S cm 1 0 mS cm 0 1 S cm 10 0 mS cm 1 0 S cm 100 0 mS cm 10 0 S cm 1000 mS cm 100 S cm The start value is the next decade value below the lowest measured value The end value is the next decade value above the highest measured value The number of decades results from Number of decades log end value log st...

Page 41: ...ent Select using keys confirm by pressing enter LOG Logarithmic curve biLIN Bilinear curve LIN Linear characteristic Start value Enter value using keys Press enter to confirm Start value of logarithmic out put curve End value Enter value using keys Press enter to confirm End value of logarithmic output curve Possible start and end values for the logarithmic curve Configuring the Current Output ...

Page 42: ... Output Current Time Averaging Filter Example Current Output 1 1 Press menu key 2 Select CONF using press enter 3 Select OUT1 menu using keys press enter 4 All items of this menu group are indicated by the OT1 code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed Configuring the Cur...

Page 43: ...ut 100 the output level is at 63 after the time interval has been reached The time interval can be set from 0 to 120 sec If the time interval is set to 0 sec the current output directly follows the input Note The filter only acts on the current output not on the display or the limit values During HOLD the filter is not applied This prevents a jump at the output Time interval 0 120 s 1st variable c...

Page 44: ...Output Current Error and HOLD Example Current output 1 1 Press menu key 2 Select CONF using press enter 3 Select OUT1 menu using keys press enter 4 All items of this menu group are indicated by the OT1 code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed 4 enter Configuring the Cur...

Page 45: ...ssing enter OFF ON Output current during Sensoface messages The output current can be set to 22 mA in the case of Sensoface messages Select ON or OFF using keys Confirm by pressing enter OFF ON Output current during HOLD LAST During HOLD the last measured value is maintained at the output FIX During HOLD a value to be entered is maintained at the output Select using Press enter to confirm LAST FIX...

Page 46: ...nu using keys press enter 4 All items of this menu group are indicated by the ALA code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed 4 enter Alarm Delay Sensocheck Tempcheck Configuring the Alarm ...

Page 47: ...ion Choices Alarm delay Enter value using keys Press enter to confirm 0 600 SEC 10 SEC Sensocheck Select Sensocheck continuous monitoring of sensor membrane and lines Select ON or OFF using keys Press enter to confirm At the same time Sensoface is activated With OFF Sensoface is also switched off ON OFF Tempcheck To monitor the temperature probe with TC OFF selected Select Tempcheck ON using keys ...

Page 48: ...tion Selecting the compensation method Temperature Compensation 1 Press menu key 2 Select CONF using press enter 3 Select CORRECTION menu using keys press enter 4 All items of this menu group are indicated by the COR code Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed 4 ...

Page 49: ...t and reference temperature nLF Temperature compensation for natural waters to EN 27888 NaCl HCL NH3 NaOH Ultrapure water with traces of impurity 0 120 C 32 248 F Temperature compensa tion of process medium With linear compensation only Step 1 Enter temperature compensation of the process medium Enter reference temperature Step 2 Enter reference temperature Enter value using keys Press enter to co...

Page 50: ...t Values 1 Press menu key 2 Select CONF using press enter 3 Select RELAY1 menu using keys press enter Specify relay contact function LIMIT 4 All items of this menu group are indicated by the LM1 code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed Configuring the Relay Contacts ...

Page 51: ...ss variable using keys Press enter to confirm Limit 1 function Select desired function using arrow keys LoLevel active if value falls below setpoint LoLevel active if value exceeds setpoint Press enter to confirm Limit 1 icon Limit 1 contact response N O normally open contact N C normally closed contact Select using keys Press enter to confirm Limit 1 setpoint Enter setpoint using keys Press enter...

Page 52: ...mple relay 1 1 Press menu key 2 Select CONF using press enter 3 Select RELAY1 menu using keys press enter Specify relay contact function LIMIT 4 All items of this menu group are indicated by the LM1 code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed Configuring the Relay Contacts...

Page 53: ...firm 0 50 full scale Limit 1 delay The contact is activated with delay deactivated without delay Adjust delay using keys Press enter to confirm Limit Lo Hysteresis Setpoint Contact 0 1 Signal Limit Hi Hysteresis Signal Contact 0 1 Application of Hysteresis Configuring the Relay Contacts Setpoint ...

Page 54: ...ect RELAY1 menu using keys press enter Specify relay contact function ALARM 4 All items of this menu group are indicated by the AL1 code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed Configuring the Relay Contacts ...

Page 55: ...s trigger signal using keys Press enter to confirm Contact response N O normally open contact N C normally closed contact Select using keys Press enter to confirm 15 14 Alarm contact A relay contact RELAY1 RELAY2 can be configured as alarm contact Alarm RELAY1 Configuring the Relay Contacts ...

Page 56: ... relay contact function WASH 4 All items of this menu group are indicated by the WS1 code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed Configuring the Relay Contacts Function Cleaning interval Cleaning duration Relax time Contact type 4 enter ...

Page 57: ...ends on the selected setting Cleaning interval Adjust value using keys Press enter to confirm Cleaning duration Adjust value using keys Press enter to confirm Without figure Relax time Relax time Contact type N O normally open contact N C normally closed contact Select using keys Press enter to confirm N O N C Cycle interval Cleaning Relax time adjustable HOLD Configuring the Relay Contacts ...

Page 58: ...s the service life of the contacts will be reduced For suppression of sparks and arcing components such as RC combinations nonlinear resistors series resistors and diodes should be used Typical AC applications with inductive load 1 Load 2 RC combination e g RIFA PMR 209 Typical RC combinations for 230 V AC capacitor 0 1 µF 630 V resistor 100 Ω 1 W 3 Contact 1 2 3 1 2 3 ...

Page 59: ...amps A1 Inductive load A2 Free wheeling diode e g 1N4007 Observe polarity A3 Contact B1 Capacitive load B1 Resistor e g 8 Ω 1 W at 24 V 0 3 A B3 Contact C1 Incandescent lamp max 60 W 230 V 30 W 115 V C3 Contact Typical Protective Wiring Measures WARNING Make sure that the maximum ratings of the relay contacts are not exceeded even during switching ...

Page 60: ...key 2 Select CONF using press enter 3 Select CLOCK or TAG using keys press enter 4 All items of this menu group are indicated by the CLK or TAG code Press enter to select menu edit using arrow keys see next page Confirm and proceed by pressing enter 5 Exit Press meas key until the meas mode indicator is displayed 4 Configuring the Time Date ...

Page 61: ...r it can be checked if the sensor con tains the correct TAG or belongs to the correct GROUP If not a message will be generated and Sensoface gets sad The sad Sensoface icon can also be signaled by a 22 mA error current Sensor verification can be switched on in the Configuration in two steps as TAG and GROUP if required When no measuring point or group of measuring points is saved in the sensor e g...

Page 62: ...62 ...

Page 63: ...ith calibration solution toroidal sensors temperature probe adjustment Calibration adapts the device to the individual sensor characteristics Access to calibration can be protected with a passcode SERVICE menu First you open the calibration menu and select the calibration mode Calibration with calibration solution Calibration by entry of cell constant Product calibration calibration with sampling ...

Page 64: ...se sensor in cali bration solution Enter the temperature corrected value of the calibration solution using the arrow keys see table Press enter to confirm Lower line display of cell constant cell factor and temperature Contacting conductivity measurement Cond The determined cell con stant is displayed The hourglass icon is blinking Proceed by pressing enter Inductive conductivity measurement CONDI...

Page 65: ...play of conductivity and temperature Senso face is active After end of calibration the outputs remain in HOLD mode for a short time After display of GOOD BYE the device automat ically returns to measur ing mode Note Be sure to use known calibration solutions and the respective temperature corrected conductivity values see Calibration Solutions tables Make sure that the temperature does not change ...

Page 66: ...he calibration mode indicator blinks 2 In the second step you enter the measured sample value in the device From the difference between the stored measured value and entered sample value the device calculates the new cell constant the new cell factor for toroidal sensors If the sample is invalid you can take over the value stored during sampling In that case the old calibration values are stored A...

Page 67: ... open the product calibration once more Display 3 sec Now the device is in HOLD mode The stored value is displayed blinking and can be over written with the lab value Press enter to proceed Display of new cell constant cell factor based on 25 C Sensoface is active To exit calibration Select MEAS then enter To repeat calibration Select REPEAT then enter End of calibration After end of calibration t...

Page 68: ...in HOLD mode Enter the measured tem perature value Maximum difference 10 K Press enter to proceed Display of actual temperature uncom pensated in the lower display The corrected temperature value is displayed Sensoface is active To exit calibration Select MEAS then enter To repeat calibration Select REPEAT then enter After end of calibration the outputs remain in HOLD mode for a short time After c...

Page 69: ...less than 30 mm from the wall you should perform the calibration either by means of sampling product cali bration with the sensor installed or in a suitable calibration beaker with dimensions and material corre sponding to the process conditions Calibrating Toroidal Sensors ...

Page 70: ...method Press enter to proceed Ready for calibration Hourglass blinks Display 3 sec Now the device is in HOLD mode Enter cell factor Press enter to proceed The selected process variable and the tem perature are displayed The device shows the cal culated cell factor and zero point at 25 C Sensoface is active Use the arrow keys to select MEAS exit REPEAT Press enter to proceed Exit HOLD is deactivate...

Page 71: ...device is in HOLD mode Calibration in air Edit digits until the lower display indicates Zero Calibration in air AIR SET for SE680 M and Memosens sensors Press enter to start AIR SET When zero point and cell factor are displayed press enter to confirm The device shows the cell factor at 25 C and the zero point Sensoface is active Use the arrow keys to select MEAS exit REPEAT Press enter to proceed ...

Page 72: ...red process variable Cond Conc or temperature The meas mode indicator lights Note After prolonged power outage 5 days the time display is replaced by dashes and cannot be used for processing In that case enter the correct time By pressing the meas key you can step through the different displays When no key has been pressed for 60 sec the device returns to the standard display see Display in Measur...

Page 73: ...ly measured values Displaying device type software version serial number Access to diagnostics can be protected with a passcode SERVICE menu Note HOLD is not active during Diagnostics mode Action Key Remark Activate diagnostics Press menu key to call the selection menu Select DIAG using keys confirm by pressing enter Select diagnos tics option Use keys to select from See next pages for further pro...

Page 74: ...red parameter from the bottom line of the display LAST_CAL CELL ZERO INSTALL The selected parameter is shown in the upper display line Press meas to return to measurement Displaying the sensor data Manufacturer type serial number and last calibration date In each case Sensoface is active Display data using keys return by pressing enter or meas ...

Page 75: ... changing background colors white green red Proceed by pressing enter 2 RAM test Hourglass blinks then display of PASS or FAIL Proceed by pressing enter 3 EEPROM test Hourglass blinks then display of PASS or FAIL Proceed by pressing enter 4 FLASH test Hourglass blinks then display of PASS or FAIL Proceed by pressing enter ...

Page 76: ...s through the logbook entries 00 99 00 being the last entry If the display is set to date time you can search for a particular date using the keys Press to view the corresponding message text If the display is set to the message text you can search for a particular message using the keys Press to display the date and time Press meas to return to measurement ...

Page 77: ... from the bottom line of the display The selected parameter is shown in the upper display line Press meas to return to measurement Display of sensor operating time Version Display of device type software hardware version and serial number for all device components Use the keys to switch between software and hardware version Press enter to proceed to next device component ...

Page 78: ...ce type pH Oxy Cond Resetting the device to factory settings Note HOLD is active during Service mode Action Key Display Remark Activate Service Press menu key to call the selection menu Select SERVICE using keys press enter to confirm Passcode Enter passcode 5555 for service mode using the keys Press enter to confirm Display In service mode the following icons are displayed HOLD triangle Service w...

Page 79: ...tputs 1 and 2 Select OUT1 or OUT2 using the keys press enter to confirm Enter a valid current value for the respective output using keys Confirm by pressing enter For checking purposes the actual output current is shown in the bottom right corner of the display Exit by pressing enter or meas Relay test manual test of contacts Select RELAIS using press enter to confirm Now the status of the relays ...

Page 80: ...cifying the serial number and hardware version of your device To enter the Ambulance TAN call the Service function and enter passcode 7321 After correct input of the ambulance TAN the device signals PASS for 4 sec and resets the Service passcode to 5555 Reset to factory settings In the SERVICE DEFAULT menu you can reset the device to fac tory settings NOTICE After a reset to factory setting the de...

Page 81: ...ration or calibration data defec tive completely reconfigure and recali brate the device ERR 95 SYSTEM ERROR System error Restart required If error still persists send in the device for repair ERR 01 NO SENSOR Sensor error Device type not assigned Defective sensor Sensor not connected Break in sensor cable ERR 02 WRONG SENSOR Wrong sensor ERR 04 SENSOR FAILURE Failure in sensor ERR 05 CAL DATA Err...

Page 82: ...2 0 3 8 mA ERR 64 OUTPUT 2 TOO HIGH Output current 2 20 5 mA Sensoface messages Cell factor monitoring SENSOR CELL FACTOR CALIBRATE OR CHANGE SENSOR Table monitoring TC Conc Sal USP OUT OF INTERNAL TABLE Zero point monitoring SENSOR ZERO CALIBRATE OR CHANGE SENSOR Cell factor zero point monitoring SENSOR ZERO CELL FACTOR CALIBRATE OR CHANGE SENSOR Sensor TAG does not corre spond to device entry WR...

Page 83: ... the Sensoface indicator can only take place after calibration or removal of the sensor defect Sensoface message The Sensocheck message is also output as error message Err 15 The alarm contact is active the display backlighting turns red output current OUT is set to 22 mA when configured correspondingly All other Sensoface message can be output via a contact relay contacts alarm FACE Disabling Sen...

Page 84: ...us OUT 1 OUT 2 REL1 2 Time out Measure DIAG 60 s CAL No CONF 20 min SERVICE 20 min SERVICE OUT 1 20 min SERVICE OUT 2 20 min SERVICE RELAYS 20 min Cleaning function No HOLD No Explanation as configured Last Fix or Last Off active manual ...

Page 85: ...ardous locations Zone 2 A405B Mounting accessories Pipe mount kit ZU 0274 Panel mount kit ZU 0738 Protective hood ZU 0737 M12 socket for sensor connection with Memosens cable M12 connector ZU 0860 Up to date information www knick de Phone 49 30 80191 0 Fax 49 30 80191 200 Email info knick de ...

Page 86: ...pending on Memosens Temp compensation Reference temp 25 C OFF Without LIN Linear characteristic 00 00 19 99 K NLF Natural waters to EN 27888 NACL NaCl from 0 ultrapure water to 26 wt Concentration determination 01 NaCl 0 26 wt 0 C 32 F 0 28 wt 100 C 212 F 02 HCl 0 18 wt 20 C 4 F 0 18 wt 50 C 122 F 03 NaOH 0 13 wt 0 C 32 F 0 24 wt 100 C 212 F 04 H2 SO4 0 26 wt 17 C 1 4 F 0 37 wt 110 C 230 F 05 HNO3...

Page 87: ...lay of cell constant cell factor and temperature Product calibration for conductivity Temperature probe adjustment Zero calibration CondI Sensocheck Polarization detection Delay Approx 30 s Sensoface Provides information on the sensor condition Sensor monitor Direct display of measured values from sensor for validation resistance temperature user defined 1 according to IEC 746 Part 1 at normal ope...

Page 88: ...messages Characteristic Linear bilinear or logarithmic Output filter PT1 filter time constant 0 120 s Measurement error 1 0 25 current value 0 025 mA Output 2 0 4 20 mA max 10 V floating terminals 9 10 galvanically connected to output 1 Overrange 22 mA in the case of error messages Characteristic Linear bilinear or logarithmic Output filter PT1 filter time constant 0 120 s Measurement error 1 0 25...

Page 89: ...ate formats selectable Power reserve 5 days Display LC display 7 segment with icons colored backlighting Primary display Character height approx 22 mm unit symbols approx 14 mm Secondary display Character height approx 10 mm Text line 14 characters 14 segments Sensoface 3 status indicators friendly neutral sad face Mode indicators meas cal conf diag Further icons for configuration and messages Ala...

Page 90: ...HS conformity according to EC directive 2002 95 EC Power supply 80 V 15 230 10 V AC approx 15 VA 45 65 Hz 24 V 15 60 10 V DC 10 W Overvoltage category II protection class II Nominal operating conditions Ambient temperature 20 55 C 4 131 F Transport Storage temperature 30 70 C 22 158 F Relative humidity 10 95 not condensing Enclosure Molded enclosure made of PBT PC glass fiber reinforced Mounting W...

Page 91: ...tions Potassium Chloride Solutions Conductivity in mS cm Temperature 1 Data source K H Hellwege Editor H Landolt R Börnstein Zahlenwerte und Funktionen volume 2 part volume 6 C 0 01 mol l 0 1 mol l 1 mol l Concentration1 ...

Page 92: ...calculated according to DIN IEC 746 3 2 Data source K H Hellwege Editor H Landolt R Börnstein Zahlenwerte und Funktionen volume 2 part volume 6 Temperature C 0 01 mol l 1 0 1 mol l 1 Saturated 2 Concentration Sodium Chloride Solutions Conductivity in mS cm ...

Page 93: ... temperature probe adjustment For measuring processes with rapid temperature changes use a separate tempera ture probe with fast response Substance Concentration ranges NaCl Configuration 0 26 wt 0 C 32 F 0 26 wt 100 C 212 F 01 HCl Configuration 0 18 wt 20 C 4 F 0 18 wt 50 C 122 F 02 22 39 wt 20 C 4 F 22 39 wt 50 C 122 F 07 NaOH Configuration 0 13 wt 0 C 32 F 0 24 wt 100 C 212 F 03 15 50 wt 0 C 32...

Page 94: ...ration Curves Conductivity versus substance concentration and process temperature for sodium chloride solution NaCl 01 Sodium chloride solution NaCl Concentration measurement not possible in this range c by wt 01 ...

Page 95: ...measurement not possible in this range Conductivity versus substance concentration and process temperature for hydrochloric acid HCl Source Haase Sauermann Dücker Z phys Chem New Edition Vol 47 1965 02 Hydrochloric acid HCl 07 c by wt 02 07 ...

Page 96: ...on Curves 03 Sodium hydroxide solution NaOH 10 Conductivity versus substance concentration and process temperature for sodium hydroxide solution NaOH c by wt Concentration measurement not possible in this range 03 10 ...

Page 97: ...4 06 09 Conductivity versus substance concentration and process temperature for sulfuric acid H2SO4 Source Darling Journal of Chemical and Engineering Data Vol 9 No 3 July 1964 c by wt Concentration measurement not possible in this range 04 09 06 ...

Page 98: ...ivity versus substance concentration and process temperature for nitric acid HN03 Source Haase Sauermann Dücker Z phys Chem New Edition Vol 47 1965 Concentration measurement not possible in this range c by wt Concentration Curves 05 08 ...

Page 99: ...99 Concentration Curves 0 50 100 150 200 250 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 10 C 25 C 40 C 55 C 70 C 85 C 100 C 120 C c by wt Conductivity mS cm 11 Oleum H2SO4 SO3 ...

Page 100: ...Calibration data display 74 Calibration mode 63 Calibration product calibration 66 Calibration solutions 91 Calibration with calibration solution 64 Calibration zero point toroidal sensors 71 Capacitive loads protective wiring of relay contacts 58 Characteristic of output current 38 Concentration curves H2SO4 97 Concentration curves HCl 95 Concentration curves HNO3 98 Concentration curves NaCl 94 ...

Page 101: ... averaging filter 42 Connecting a Memosens sensor menu 26 Connecting a Memosens sensor terminal assignments 13 Control Drawings 6 Controlling a rinsing probe via relay contacts 56 Current calibration data display 74 Currently measured values sensor monitor 77 Currently measured values sensor monitor display with HOLD activated 79 Current output configuration 36 Current source 79 Current start end ...

Page 102: ...6 E EEPROM test 75 Enclosure components 8 Enclosure mounting possibilities 7 ERR 81 Error and HOLD output current 44 Error messages 81 EU Declarations of Conformity 6 F Factory setting 80 FLASH test 75 G GROUP of measuring points 61 H Hardware version display 77 HOLD configure output current 44 HOLD exit 23 HOLD external activation 23 HOLD mode 23 HOLD output signal 23 HOLD output signal response ...

Page 103: ...k entries display 76 Loss of passcode 80 M MAIN DISPLAY 20 Measured values display 77 Measuring function device type 78 Measuring mode 72 Measuring point TAG GROUP 60 Measuring ranges concentration 93 Memosens cable specifications order code 15 Memosens sensor connection menu 26 Memosens sensor connection terminal assignments 13 MemoSuite software for calibrating Memosens sensors 14 Menu structure...

Page 104: ...t filter time interval 42 Output signal during HOLD configuration 45 Output signal during HOLD overview 23 Overview of configuration 29 P Package contents complete 8 Package contents documentation 6 Panel mounting 11 Passcode lost 80 Passcodes setting 80 Post pipe mounting 10 Potassium chloride solutions table 91 Power supply connection 13 Power supply specifications 90 Process variable selection ...

Page 105: ...wiring 16 Selecting the device type 78 Sensocheck configuration 47 Sensocheck description 83 Sensoface configure output current 45 Sensoface description 83 Sensoface messages overview 82 Sensor connection SE 670 SE 680 16 Sensor data display 74 Sensor monitor diagnostics 77 Sensor monitor Service 79 Sensor replacement 27 Sensor verification TAG GROUP 34 Serial number display 77 Series resistors 58...

Page 106: ...s function 50 T Tag number display 72 TAG of measuring point 61 Technical data 86 Tempcheck 46 Temperature compensation 48 Temperature probe adjustment 68 Temperature probe monitoring 47 Temperature unit 32 Terminal assignments 13 Terminals 12 Time and date usage 61 Time averaging filter 43 Time display 72 Time format setting 60 Time setting 60 Toroidal sensors calibration 69 U Use of relays 50 V ...

Page 107: ...107 Index Z Zero calibration CondI 71 ZU 0274 pipe mount kit 10 ZU 0737 protective hood 10 ZU 0738 panel mount kit 11 ...

Page 108: ...31 Software version 1 x 090902 Knick Elektronische Messgeräte GmbH Co KG Beuckestraße 22 14163 Berlin Germany Phone 49 30 80191 0 Fax 49 30 80191 200 Web www knick de Email info knick de Stratos MS A405 Conductivity Measurement ...

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