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5
Vacuum System
Vacuum seals
Vacuum seals
Several types of Viton elastomer O-ring seals are used to prevent air leaks into the
vacuum manifold. All these O-rings, and the surfaces to which they must seal,
must be kept clean and protected from nicks and scratches. A single hair, piece of
lint, or scratch can produce a serious vacuum leak. Two of the O-rings are
lightly
lubricated with Apiezon-L vacuum grease: the side plate O-ring and the vent valve
O-ring.
Face seals
A face seal is an O-ring that fits in a shallow groove. The sealing surface is usually
a flat plate. The manifold side plate and end plate O-rings fit into grooves around
the large openings in the vacuum manifold. The side plate swings into place
against the side plate O-ring, and must be held in place when the MSD is turned on
for pumpdown in order to assure a good seal.
The front and rear end plates are screwed onto the manifold, and should not need
to be removed. The GC/MSD interface fastens to the manifold with three screws.
The calibration valve assembly is fastened onto the front end plate by two screws.
The vent valve knob threads into the front end plate. Small O-rings in grooves in
the front end plate provide vacuum seals.
The diffusion pump baffle adapter has a groove for its O-ring. The baffle adapter is
clamped to the manifold with 4 claw grips.
KF (NW) seals
Most of the seals for the high vacuum pumps, foreline gauge, and foreline pump
are KF seals. KF seals have an O-ring supported by a centering ring. The centering
ring can be either on the inside or the outside of the O-ring. The clamp presses two
flanges against the O-ring, making a seal. KF clamps must not be overtightened.
Compression seals
A compression fitting consists of a threaded fitting on the vacuum manifold and a
threaded collar with a ferrule and O-ring. A cylindrical part fits inside the collar.
Tightening the collar presses the ferrule, compressing the O-ring around the part.
The triode gauge tube and calibration vial use compression seals.
Summary of Contents for 5973
Page 1: ...H Hardware Manual HP 5973 Mass Selective Detector ...
Page 3: ...HP 5973 Mass Selective Detector Hardware Manual ...
Page 25: ...1 Installing GC Columns To condition a capillary column 25 ...
Page 30: ...30 ...
Page 37: ...2 Operating the MSD To view MSD analyzer temperature and vacuum status 37 ...
Page 39: ...2 Operating the MSD To set monitors for MSD temperature and vacuum status 39 ...
Page 41: ...2 Operating the MSD To set the MSD analyzer temperatures 41 ...
Page 43: ...2 Operating the MSD To set the interface temperature from the ChemStation 43 ...
Page 51: ...2 Operating the MSD To remove the MSD covers 51 Upper cover Lower cover ...
Page 92: ...92 ...
Page 105: ...4 Maintaining the MSD To drain the foreline pump 105 Fill cap Drain plug Pump motor ...
Page 113: ...4 Maintaining the MSD To separate the MSD from the GC 113 ...
Page 121: ...4 Maintaining the MSD To reconnect the MSD to the GC 121 ...
Page 141: ...4 Maintaining the MSD To lubricate the side plate O ring 141 Side plate O ring ...
Page 159: ...4 Maintaining the MSD To remove a filament 159 Filament 2 Filament 1 ...
Page 161: ...4 Maintaining the MSD To reinstall a filament 161 Filament 2 Filament 1 ...
Page 210: ...210 ...
Page 214: ...214 ...
Page 232: ...232 7 Analyzer Analyzer heaters and radiators ...
Page 280: ...280 ...
Page 294: ...294 Index ...
Page 296: ...294 Chapter ...
Page 297: ...H Manual Part Number G1099 90027 Copyright 1998 Hewlett Packard Printed in USA 11 98 ...