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42
CI setup
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To install the GC column in the EI/CI GC/MSD interface
Materials needed:
Adjustment tool (G1099-20030)
Ferrules
0.27-mm id, for 0.10-mm id columns (5062-3518)
0.37-mm id, for 0.20-mm id columns (5062-3516)
0.40-mm id, for 0.25-mm id columns (5181-3323)
0.47-mm id, for 0.32-mm id columns (5062-3514)
0.74-mm id, for 0.53-mm id columns (5062-3512)
Interface column nut (05988-20066)
Wrench, 1/4-inch open-end (8710-0510)
See the MSD reference Collection CD-ROM for a video of this procedure.
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The column should not extend more than 1 mm past the tip of the adjustment tool.
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Tighten only enough so that the column does not slip in the ferrule if tugged gently.
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Note that the EI/CI interface doesn’t extend quite as far into the GC oven as the EI
interface does.
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Do not overtighten. Tighten only until the ferrule squeaks.
N O T E
The EI/CI interface doesn’t extend quite as far into the GC oven as the EI interface did.
Summary of Contents for 5973 MSD
Page 1: ...H Hardware Manual HP 5973 MSD PCI NCI ...
Page 6: ...6 ...
Page 7: ...1 General Information Specifications 9 Reagent gases and regulators 10 ...
Page 13: ... Hardware Reference 13 ...
Page 25: ... Chemical Ionization Theory 3RVLWLYH WKHRU 25 ...
Page 31: ... Chemical Ionization Theory 1HJDWLYH WKHRU 31 ...
Page 34: ...34 ...
Page 92: ...92 ...
Page 114: ...114 ...
Page 120: ...120 ...
Page 122: ...H Manual Part Number G1999 90001 Copyright 1998 Hewlett Packard Printed in USA 2 98 ...