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EL-CELL ECC-Opto-Std, User Manual

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EL-CELL ECC-Opto-Std User Manual Download Page 15

 

  Page 15 of 19

 

User Manual ECC-Opto-Std – Release 2.62 

8  Further Kits 

 

Components Sapphire Kit: 

ECC1-00-0156-C

 

1.

 

Sapphire window (22 x 0.3 mm) 

ECC1-00-0149-A  

 

2.

 

Lid Sapphire 

ECC1-00-0127-B

 

 

Components Zinc Selenide Kit: 

ECC1-00-0156-D

 

1.

 

Zinc Selenide window (22 x 0.3 mm) 

ECC1-00-0250-B s

 

2.

 

Lid Zinc Selenide 

ECC1-00-0127-E

 

 

Components Calciumfluoride Kit: 

ECC1-00-0156-E

 

1.

 

Calciumfluorid window (22 x 0.3 mm) 

ECC1-00-0250-C 

 

2.

 

Lid Calciumfluorid 

ECC1-00-0127-E

 

 

 

 

 

 

Summary of Contents for ECC-Opto-Std

Page 1: ...2016 EL CELL GmbH User Manual Release 2 62 Electrochemical Test Cell ECC Opto Std November 2016...

Page 2: ...ies EL CELL GmbH maintains the right to make changes without further notice to products described in this manual to improve reliability function or design EL CELL GmbH does not assume any liability ar...

Page 3: ...Description 4 2 Features 6 3 Safety Precautions 7 4 Unpacking 7 5 Assembly and Connection 9 6 Disassembly and Cleaning 12 7 X Ray Experiments 13 8 Further Kits 15 9 Components ECC Opto Std 16 10 Spar...

Page 4: ...nt collector is placed right below the optical window This WE is sandwiched from below with a glass fiber separator and an appropriate counter electrode CE This way the optical instrument looks from t...

Page 5: ...window Current collector mesh Aluminium or Copper 16 mm Spring loaded piston Working electrode material WE placed on the current collector mesh Glass fiber separator Counter electrode CE Inspection ar...

Page 6: ...pphire Beryllium and Kapton windows are available on request Working electrodes can be single crystals or grains powder samples and free standing electrodes applied onto current collector mesh Maximum...

Page 7: ...ly toxic and can cause cancer Take proper precautions when handling the Beryllium window Avoid direct contact with skin Carefully collect and dispose properly any Beryllium fragments when accidentally...

Page 8: ...eed wire assy ECC1 00 0010 F 4 Current collector mesh copper 5 pieces ECC1 00 0328 A V 5 Current collector mesh aluminium 5 pieces ECC1 00 0328 B V 6 Filling tube with syringe 5 ml for vacuum filling...

Page 9: ...ctrode max 10 mm in diameter max 1 mm thick 4 Put the provided glass fiber separator on top 5 Place the working electrode on top of the separator with the active layer pointing UPWARDS The working ele...

Page 10: ...rds Then release the piston so that the electrolyte is sucked into the cell by the previously applied vacuum NOTE Never pressurize the cell during the filling procedure Repeat the two previous steps t...

Page 11: ...11 of 19 User Manual ECC Opto Std Release 2 62 13 Connect your potentiostat to the 2 mm sockets 1 of the cell cable grey REF red WE blue CE Adapters 2 are provided for connection to 4 mm banana plugs...

Page 12: ...slightly depends on the thickness of the cell stack 6 Disassembly and Cleaning Right after use disassemble the cell in the reverse order of assembly All chemicals used have to be disposed properly Al...

Page 13: ...kit comprises a Beryllium window ECC1 00 0222 A and a modified cell lid ECC1 00 0127 C The lid features a 10 mm inspection hole and a 10 mm wide groove that allows for a viewing angle onto the sample...

Page 14: ...small piece of polyethylene foil 15 mm in diameter 10 m thick in between the holed current collector and the Beryllium window Beryllium is highly toxic and can cause cancer Take proper precautions wh...

Page 15: ...w 22 x 0 3 mm ECC1 00 0149 A 2 Lid Sapphire ECC1 00 0127 B Components Zinc Selenide Kit ECC1 00 0156 D 1 Zinc Selenide window 22 x 0 3 mm ECC1 00 0250 B s 2 Lid Zinc Selenide ECC1 00 0127 E Components...

Page 16: ...328 B Current collector mesh Cu ECC1 00 0328 A Stand ECC Opto Std ECC1 00 0151 A Feed wire ECC1 00 0010 F Compression spring Au FED9015 Touch screw ECC1 00 0128 A WE Glass fiber separator with tongue...

Page 17: ...10 N Au standard 5 pieces FED9015 V Spring forces see page 12 Compression spring 20 N Au 5 pieces FED9020 V Spring forces see page 12 Compression spring 30 N Au 5 pieces FED9021 V Spring forces see pa...

Page 18: ...Kit ECC1 00 0306 A Glass window 5 pieces LAB0018 V Glass fiber separator 5 pieces ECC1 01 0012 J V Current collector mesh copper 5 pieces ECC1 00 0328 A V Current collector mesh aluminium 5 pieces EC...

Page 19: ...ted Warranty does not cover defects damage or nonconformity resulting from abuse misuse neglect lack of reasonable care modification or the attachment of improper devices to the goods This Limited War...

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