6 Operation
43
KjelFlex K-360
Operation Manual, Version D
6 .8
Carrying out a distillation
To carry out a distillation, proceed as follows:
• Switch on the instrument and wait until the steam generator is ready.
• Insert the sample tube containing the sample.
• If you do not work with the titration set, prepare a conical flask or a similar receptacle with a volume
of about 250 mL as receiving vessel.
For sample analyses there are two different approaches, depending on how you prefer to work:
• Single sample analyses
• Rack oriented analyses
6 .8 .1
Single sample analysis
For single sample analyses, no predefined sample list is needed for identification. To start an analysis,
provide a sample and press the Sample button in the main menu. The following screen opens:
Fig. 6.14: Sample
Enter a sample name and sample weight via keypad. Choose the desired method and press Start to
start the distillation process.
NOTE
• When you re-enter the screen, sample name, weight, unit, type and method are set to the latest
entered settings.
• You can start a determination at any time without a sample name or weight input.
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