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Probe Setup, Operations, Probe Modifiers
User Manual Version 002
BRUKER BIOSPIN
45 (327)
Figure 3.35.
λ
/4 (low range) and
λ
/2 Mode (high range), 400 MHz Probe
At 400 MHz, the wavelength is large, so the
λ
/4 point is below the closed section
(7) of the
λ
-line. At higher frequencies, the
λ
/4 point may fall within the closed sec-
tion 7.
The proton channel (decoupling channel) is usually tuned via a so-called
λ
-line
(“transmission line”). This is just a coaxial cable or a coaxial conductor with an ar-
rangement of an outer conductor (a tube) and an inner conductor (a rod). The rel-
ative diameters and distances and also the dielectric in between (usually air in WB
probes) determine the impedance of the transmission line. Since such a line is as
well an inductance as a capacitance, it is a resonating circuit. If the length of the
transmission line equals
λ
/4 or
λ
/2 of the RF-wave, it is a
λ
/4 or
λ
/2 line. Since the
upper end of the transmission line (inner conductor) is connected to the coil, high
voltage is required there. This means that the
λ
/4 point has low voltage but high
current, whereas the
λ
/2 point is at high voltage and low current. A short between
1.
λ
-line inner conductor
2. Rotating switch at
λ
/4 position
3. Switch closed rotating counterclockwise
(seen from probe lower end). Contact springs
(grounded) touch the
λ
-line at the
λ
/4 position
4. Switch open rotating clockwise.
5. Switch operating rod
6. Tuning capacitor
at the end of the
λ
-line inner conductor: Fine tunes the effective length and there-
fore resonating frequency of the
λ
-line. This tunes the proton channel frequency (“tune”).
Summary of Contents for Solid State NMR
Page 8: ...8 BRUKER BIOSPIN User Manual Version 002 Contents...
Page 14: ...14 327 BRUKER BIOSPIN User Manual Version 002 Test Samples...
Page 118: ...118 327 BRUKER BIOSPIN User Manual Version 002 Basic CP MAS Experiments...
Page 122: ...122 327 BRUKER BIOSPIN User Manual Version 002 FSLG HETCOR Figure 8 3 The ased Display...
Page 154: ...154 327 BRUKER BIOSPIN User Manual Version 002 Proton Driven Spin Diffusion PDSD...
Page 178: ...178 327 BRUKER BIOSPIN User Manual Version 002 SUPER...
Page 192: ...192 327 BRUKER BIOSPIN User Manual Version 002 Symmetry Based Recoupling...
Page 212: ...212 327 BRUKER BIOSPIN User Manual Version 002 Relaxation Measurements...
Page 270: ...270 327 BRUKER BIOSPIN User Manual Version 002 Double CP...
Page 290: ...290 327 BRUKER BIOSPIN User Manual Version 002 Modified W PMLG...
Page 302: ...302 327 BRUKER BIOSPIN User Manual Version 002 CRAMPS 2D...
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Page 318: ...318 327 BRUKER BIOSPIN User Manual Version 002 Tables...
Page 326: ...326 327 BRUKER BIOSPIN User Manual Version 002 Index...
Page 327: ...User Manual Version 002 BRUKER BIOSPIN 327 327 End of Document...