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POLARIMETER

ADP

440

Summary of Contents for ADP440

Page 1: ...POLARIMETER ADP440...

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Page 3: ...es in PDF format may be downloaded from this section of the site by clicking the flag We apologise if the foreign language brochure of your choice is not available Contact Sales at Bellingham and Stan...

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Page 5: ...wing Product Specifications Safety BSEN60950 1992 A1 A2 A3 A4 A11 EMC Emissions EN55022 1998 Radiated Emissions Class A EN55022 1998 Conducted Emissions Class A Immunity EN61000 3 2 Harmonics EN61000...

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Page 7: ...ugh and water jacketed tubes 2 17 Setting up the system 3 Menu flow chart 3 1 Shortcut keys 3 3 Calibration 3 5 Measurement settings 3 8 Methods 3 9 User accessibility 3 13 21 CFR Part 11 3 17 System...

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Page 9: ...256 01 R0 September 2006 Section 1 section1 Installing the instrument Unpacking the instrument 1 1 Contents list 1 1 Part numbers 1 1 Positioning the system 1 2 Mains connection 1 2 Power requirements...

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Page 11: ...55 105 1 Mains lead see below for part number 1 Polarimeter tube 35 47 1 Operating Instructions 37 256 1 Instruction manual CD ROM 55 300 Part numbers ADP440 polarimeter part numbers Model Complete po...

Page 12: ...of several socket types For UK lead replace fuse only with the type indicated on the plug Power requirements Voltage 110 to 230V 10 50 to 60 Hz Maximum load less than 40 mA Power supply adapter 55 105...

Page 13: ...al values 2 8 Display screen information 2 9 Taking a reading 2 10 Blocked light path 2 10 Grey result display 2 10 Zeroing the reading 2 11 Optical density 2 12 Temperature sensor 2 12 Printing the r...

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Page 15: ...trument is housed in a rigid polyurethane foam moulded case which is light in weight whilst being extremely rugged and has a high resistance to chemical attack from the majority of commonly used sampl...

Page 16: ...r for the instrument module Serial number Always specify this number in any communication with B S Ltd Warning symbol See similarly marked warnings in this manual RS232 Serial port 1 For printing or r...

Page 17: ...ck keys for negotiating through menus etc Power key Press to switch ON Press for 2 seconds to switch to STANDBY Soft key functions Alpha numeric keys Telephone style keys for entering letters and numb...

Page 18: ...eading is to be taken only once per day Switching on for the first time When the instrument is switched on for the first time after delivery a Setup Wizard will step you through a number of questions...

Page 19: ...or reading mechanism to reach operating speed the vertical progress bar indicates how much longer this will take which should take less than one minute When reached it will automatically carry out a z...

Page 20: ...list of options to choose from then either select the menu item and then choose the option from the displayed list or press the Forward Back arrow keys to step through the options Menu items that can...

Page 21: ...press the key 3 times c the key 3 times o the key 3 times l the key 1 time a the key 11 times the key 5 times 7 the key 4 times 4 the key 12 times Once a key is pressed the available characters that...

Page 22: ...ponent E symbols that will be required to enter both numerical formats As the user enters the number the instrument responds to the key strokes by changing the soft key function If an error is made wh...

Page 23: ...ent description 37 256 01 R0 Page 2 9 Display screen information Current time Stability Progress bar Reading Result Measurement Settings Softkey titles B B a a s s i i c c o o p p e e r r a a t t i i...

Page 24: ...ss bar will slowly fill also as an indication that the reading has yet to stabilise the reading result is displayed in grey When finally stabilised the progress bar will appear full and the reading wi...

Page 25: ...lace in the chamber Wait for the instrument to stabilise using the reading progress bar as a guide When stable press ZERO The displayed reading will now change to 0 00 Below the instrument is showing...

Page 26: ...ical density of the sample is greater than 3 the background of the reading area will appear grey show below see page 2 10 Temperature sensor The ADP440 has a in built temperature sensor The measured t...

Page 27: ...strument such as when the last span was carried out and measurement settings Each measurement has a number of parameters On the left is the parameter name and on the right is the parameters value The...

Page 28: ...ithin the instrument the user who carries out the change will be also logged The Reading log If the fourth right hand softkey is set to Save or Prt Save then pressing it will save the last displayed r...

Page 29: ...nu The mode menu will be familiar to users of the ADP220 polarimeter and many other Bellingham Stanley instruments The measurement settings are changed from the Mode menu which is accessed from the Me...

Page 30: ...n modes available By default the available temperature compensation modes are TC Name TC ID none nc sugar sc quartz qc Limits The instrument is able to have limits set on a number of parameters If the...

Page 31: ...ation greater than 89 then the correct value can be calculated from 180 Displayed Rotation Alternatively if the 1 to 179 or the 91 to 269 scale is selected then the correct rotation will be displayed...

Page 32: ...8 50 37 601 01 ADP410 No PF05000 Only available when Mode menu is accessible Methods not in use see page 3 8 Set scale to a S 1 83 49 Scale 1 2 Scale a Set scale to z S 2 83 50 Scale 1 2 Scale z Set T...

Page 33: ...ar of the instrument The interconnecting cable socket can be secured with the 2 screws but these must be finger tightened only DO NOT OVER TIGHTEN 9 Pin D type plug connections Pin No Function Data di...

Page 34: ...etween them The rubber washer must be placed between the end cap and the cover glass The end caps should be lightly finger tightened just enough to prevent leaking Over tightening will stress the glas...

Page 35: ...will decrease to approximately 99 5 Z at 30 C a quartz control plate with a rotation of 100 Z at 20 C will increase to approximately 100 14 Z at 30 C Therefore it is necessary to maintain the sample a...

Page 36: ...d 4mm Allen key The slots will allow the circulation hoses to exit the chamber and also ensure that funnel tubes are held in an upright position It is important that any hoses connected to the tube mu...

Page 37: ...condition 3 12 Editing or deleting a limit test condition 3 12 User accessibility 3 13 Security features 3 14 Preset protection level 3 15 Setting the protection level 3 16 Adding a User 3 16 Editing...

Page 38: ...dding a custom designed scale 3 25 Adding a custom designed temp compensation 3 26 Special library scales 3 27 Activating special library scales 3 27 Specific rotation 3 28 Concentration 3 30 Purity 3...

Page 39: ...d new 1 Header 2 Temperature 3 Quality 4 Reading Info 5 Configuration 1 Response 2 Resolution 3 Scales 4 Temp Comps 1 low 2 medium 3 high 1 fast 2 sec 2 medium 15 sec 3 slow 30 sec 1 Date Format 2 Sum...

Page 40: ...Page 3 2 37 256 01 R0 September 2006 Setting up the system...

Page 41: ...functions can be activated when the Measurement Display is shown Press and hold down the key until the next screen is displayed Press and hold to switch to standby Press and hold to adjust the Displa...

Page 42: ...Page 3 4 37 256 01 R0 September 2006 Setting up the system...

Page 43: ...tered in the scale units as selected in the measurement settings If the instrument s measurement settings are being set using Methods then the span method will automatically be selected when a span is...

Page 44: ...was applied or the wrong value was entered it can be cancelled press the Menu softkey select 1 Calibration select 2 Undo press Yes Calibration report Display a report of the last Zero Span calibration...

Page 45: ...o users with Setup and Calibration rights press the Menu softkey select 1 Calibration select 4 Warning Frequency type the number of days enter 0 to disable The warning will be displayed after a result...

Page 46: ...red on the polarimeter requires the same measurement settings then Mode Menu option would be most suitable The mode menu is discussed further on page 2 15 However if a number of products with differin...

Page 47: ...r each of them E g a range of soft drinks could be regularly measured in the a scale and the display should show whether each product reading value is within its set tolerance The profiles can be give...

Page 48: ...e Methods function can be disabled and the second softkey in the Measurement display will be blank Alternatively if a number of profiles are created for a standard range of products e g cola orange le...

Page 49: ...d method by its index number rather than scrolling through the list To change the method selection method press the Menu softkey select 3 Setup select 1 Methods select 4 Settings Note the selection nu...

Page 50: ...ber will change as limits tests are added select the parameter 1 reading 2 temp 3 od enter the Lower Limit enter the Upper Limit Example A method has been configured with the scale set to a and two li...

Page 51: ...level set to low Rights User Name Default PIN Mode Methods Set Zero Set Span Select Tools Select Setup administrator 000 Yes Yes Yes Yes Yes calibrator 355 Yes Yes Yes No No operator 123 Yes No No No...

Page 52: ...emember the last users for If set the instrument will remember the last entered user so the user will not have to re enter it Reset PIN Only no yes If selected the administrator will only be able to R...

Page 53: ...heir PIN This preset does not have features enabled that could increase the administration overheads User Selection user and pin PIN Length 4 Maximum PIN Age off Remember Last User 10 mins Invalid PIN...

Page 54: ...will change as users are added Enter the User name which can be a combination of lower case letters numbers and other characters Then enter the PIN code see Preset protection levels above for PIN leng...

Page 55: ...See page 1 Protection level set to high 3 16 2 Log User set to login 3 24 3 Set the print mode printer 3 19 4 Select use of serial 1 csv 3 19 5 Add necessary users 3 16 6 Reset administrators PIN 3 16...

Page 56: ...lock for summer daylight saving time The instruments clock can easily be adjusted for daylight saving time adding one hour to the clock press the Menu softkey select 3 Setup select 5 System select 2 T...

Page 57: ...Printer select 1 Mode Available print formats This instrument can output data using either the serial port 1 and or parallel port There are 2 formats available Format Description 24 column Optimised...

Page 58: ...gether and a statistical analysis carried out upon the results When Print is pressed and no previous results have been logged the instrument will request the traceability data batch and operator detai...

Page 59: ...instrument averages over effects the measurement response stability and reading time The greater the averaging the better the stability the disadvantage is a slower response to a change in sample and...

Page 60: ...tensity The instrument must be in the measuring condition with the Measurement Display screen showing Press and hold down the Methods or Mode softkey for approximately three seconds The Configure Disp...

Page 61: ...est a batch code number Number from 0 to 32000 text 14 character alpha numeric string dateinc auto increasing number from 0 to 9999 in the format of yymmddnnnnn Example 0603117775 11th March 2006 numb...

Page 62: ...ation If the printer type is set to printer then the measurement will be printed showing the scanned in barcode number User codes When the user code option is selected the user can be recorded in a nu...

Page 63: ...then be available when adding or editing methods Adding a custom designed scale The readings can be converted to custom units using the following formule No Equation 1 reading A Bx Cx2 Dx3 Ex4 Fx5 2 a...

Page 64: ...ion before the reading is converted to z or another scale Therefore the Reading Correction must also be calculated in rotation Corrected reading Uncorrected reading Reading Correction press the Menu s...

Page 65: ...pecific rotation using a known concentration conc g cm3 co Concentration using a known specific rotation purity pu Purity using a known brix value inv sucrose pi Inversion of sucrose solution change p...

Page 66: ...at 20 C and measured using a sodium D light source c is the concentration of in g 100cm3 l is the length of the polarimeter tube in dm The International Commission for Uniform Methods of Sugar Analysi...

Page 67: ...ment allows the concentration to be changed shown below The change whether concentration is fixed or variable press press the Menu softkey select 3 Setup select 4 Reading select 4 Scales select 1 spec...

Page 68: ...cm3 20 D is the specific rotation in angular degrees per dm and per g cm3 at 20 C and measured using a sodium D light source 20 D is the optical rotation in angular degrees at 20 C and measured using...

Page 69: ...rument allows the specific rotation to be changed shown below The change whether concentration is fixed or variable press press the Menu softkey select 3 Setup select 4 Reading select 4 Scales select...

Page 70: ...e ADP440 has a number of settings which allow the instrument to be setup using the appropriate calculation The general equation used to calculate sugar purity is shown below brix density t puritycons...

Page 71: ...ort 2 All these settings are access by press the Menu softkey select 3 Setup select 4 Reading select 4 Scales select 1 purity Note the selection number might be different depending upon other scales a...

Page 72: ...sion o where rsuc is the rotation in A of non inverted 15 Brix sucrose solution in 100mm tube rinv is the rotation in A of fully inverted 15 Brix sucrose solution in 100mm tube A o is the rotation in...

Page 73: ...nstrument allows the concentration to be changed shown below The change whether concentration is fixed or variable press press the Menu softkey select 3 Setup select 4 Reading select 4 Scales select 1...

Page 74: ...tion in A of the product sample rstart is the rotation in A of product sample in start state e g non inverted rend is the rotation in A of product sample in end state e g fully inverted cstart cend cs...

Page 75: ...instrument allows the concentration to be changed shown below The change whether concentration is fixed or variable press press the Menu softkey select 3 Setup select 4 Reading select 4 Scales select...

Page 76: ...ll show Initially the two options will be set to no Select the settings which you want to return to default values by setting them to show yes When set correctly press Quit The instrument will ask the...

Page 77: ...tion 37 256 01 R0 Section 4 section4 Specification Performance 4 1 Polarimeter tube 4 1 Temperature 4 1 Temperature compensation 4 1 Light source 4 1 RS232 configuration 4 1 Physical 4 1 Power require...

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Page 79: ...e 5 to 60 C Temperature compensation None Sugar 5 to 40 C Quartz 5 to 40 C Light source Light emitting diode with interference filter 589 nm Beam diameter maximum 4 mm RS232 configuration Baud rate 96...

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Page 81: ...56 01 R0 Section 5 section5 Spares and accessories Printers 5 1 Barcode readers 5 1 Interconnecting cables 5 1 Quartz control plates 5 1 Instruction manuals 5 1 Spares 5 1 Polarimeter tubes 5 2 Upper...

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Page 83: ...e Quartz Control Plate nominal 100 Z 34 6 Angular 34 20 Quartz Control Plate nominal 15 Z 5 2 Angular 34 21 QCP UKAS certificate of calibration traceable to PTB 90 803 Thermal Block Assembly 34 241 In...

Page 84: ...25 50 37 010 35 74 35 73 35 72 35 71 Low volume continuous flow through tube with water jacket for temperature control 25 50 37 012 35 75 35 76 Low volume continuous flow through tube for highly acid...

Page 85: ...es Code Power supply unsealed 110 230V 55 105 Mains lead for 55 105 with plug suitable for United Kingdom 61 191 Euro Schuko 61 193 United States 61 192 Switzerland 61 181 Denmark 61 182 India South A...

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