Barnstead|Thermolyne D11911 Operation Manual Download

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ARNSTEAD

HERMOLYNE

NANOpure

DIamond

™

ultrapure water system

Operation Manual

Series 1191

Model No.

Voltage

D11911

100V - 240V

LT1191X1 • 6/22/00

Summary of Contents for D11911

Page 1: ...BARNSTEAD THERMOLYNE NANOpure DIamond UV ultrapure water system Operation Manual Series 1191 Model No Voltage D11911 100V 240V LT1191X1 6 22 00 ...

Page 2: ...ting the Sanitization Timer 26 Resetting the UV Timer 26 Setting Volumetric Dispensing 27 Setting Timed Dispensing 28 Performing a System Flush 28 Changing Purity Units 28 Temperature Compensation 29 Installing Float or Pressure Switch 30 N I S T Calibration Module 31 Performing an Electronic Calibration Using the Optional N I S T Calibration Module 31 Remote Dispenser 32 Computer Printer Setup 33...

Page 3: ...Opure DIamond UV di rectly over equipment that requires electrical service Routine maintenance of this unit may involve water spillage and subsequent electrical shock hazard if improperly located 3 Replace fuses with those of the same type and rating 4 Disconnect from the power supply prior to main tenance and servicing To avoid personal injury 1 Do not use in the presence of flammable or combusti...

Page 4: ...ety instructions on labels of chemical containers and material safety data sheets 7 Depressurize system prior to removing the cartridge pack 8 This unit is equipped with an ultraviolet lamp Ultraviolet radiation is harmful to the eyes and skin Do not attempt to observe the lamp directly 9 Refer servicing to qualified personnel 10 A full cartridge pack may weigh about 20 lbs 4 SAFETY INFORMATION ...

Page 5: ...w TOC 3 0 ppb water with a resistivity of up to 18 2 megohm cm Water resistivity is continuously monitored by a resistivity cell and displayed on a digital display The electronics can be verified and calibrated utilizing a N I S T Traceable Calibration module See accessory ordering information Please read the instructions carefully to ensure that you receive maximum benefit from the NANOpure DIamo...

Page 6: ...y feed to 100 psig 7kg cm2 maximum Temperature Range 4 C 40 C 40 104 F TDS CaCO3 70 ppm Silica 1 ppm Silt 5 SDI Product Water Water Quality Resistivity 18 0 mΩ cm TOC Less than 3 0 ppb Flow Rate 1 5 lpm maximum at minimum inlet feed water pressure 10 PSIG with a new final filter Volumetric Dispense Accuracy 5 Repeatability 3 Electrical Requirements The NANOpure DIamond UV is equipped with 2 power ...

Page 7: ... Limits for Harmonic Current Emissions EN 61000 3 3 Limits for Voltage Fluctuations and Flicker EN 61326 1 Electrical Equipment for Measurement Control and Laboratory Use Part I General Requirements Safety EN 61010 1 Safety Requirements for Electrical Equipment for Measurement Control and Laboratory Use Part I General Requirements per the provisions of the Low Voltage Directive 73 23 EEC as amende...

Page 8: ...e discarding Put the NANOpure DIamond UV on a bench UV Lamp LMX13 Sanitization Cartridge CMX25 Wall Bracket Unit Wall Bracket Remote Display BC1190X10 Accessory Parts Bag Includes Feed Water Tube 3 8 O D Drain Tube 1 4 O D 240 V Power Cord w Fuses CRX70 2 FZX54 120 V Power Cord w Fuses CRX72 2 FZX47 Display Cable WHX20 Blank Display Plug Adapter CEX42 Also required for installation Customer Suppli...

Page 9: ...ion as well as fastener type must be considered when mounting this unit The mounting surface and fasteners selected must be capable of supporting a minimum of 150 lbs 68 kg Inadequate support and or fasten ers may result in damage to mounting surface and or equipment If you are unsure of mounting surface composition condition and construc tion or correct fasteners consult your building maintenance...

Page 10: ...ies for this unit include a float switch low pressure switch N I S T Traceable Calibration Module remote dispenser and printer Installation proce dures for these accessories are explained in later sec tions of this manual INSTALLATION 10 ...

Page 11: ...free cloth use isopropyl alcohol as required 4 Remove black cap by sliding off UV housing 5 Insert the lamp halfway into the UV lamp cham ber and plug it in then fully insert the lamp into the chamber 6 Make sure the UV lamp cable is tucked behind the chamber before closing and relatching the door 11 INSTALLATION Caution DO NOT TOUCH THE GLASS POR TION OF THE LAMP It is recom mended that lint free...

Page 12: ...e wall bracket slots 7 Push the locking slides on each side of the wall bracket in as far as they will go 8 Replace the locking screws 12 INSTALLATION Note Please refer to the General Specifications section for clearance requirements Warning Do not locate the NANOpure DIamond UV directly over equipment that requires electrical service Routine maintenance of this unit may involve water spillage and...

Page 13: ...ight of the unit Remove the protective black cover and store it for future use if the control panel is returned to the top cover 6 Locate the 10 ft 3 1 m 25 pin M F cable included with the unit attach the female end to the 25 pin connector on the back top right of the unit and the other end to the connector on the bottom of the control panel 7 Tighten the cable screws on each end to secure the cab...

Page 14: ...e used see the Installing a Float or Pressure Switch section for more information Atmospheric Drain Connection When the NANOpure DIamond UV flushes the water used is sent to drain through this connection To install 1 Locate the drain water tubing This is the 1 4 64 cm O D tubing that is approximately 6 ft 1 9 m long The atmospheric drain fitting is located on the lower left side of the NANOpure DI...

Page 15: ...he system status as follows LED is not illuminated System is OFF or in Idle mode Solid Green LED System is recirculating and operating normally Blinking Green LED System is in Standby mode Red LED System is alerting user to an operational error or maintenance issue The control panel can be removed from the unit and remotely mounted Please refer to Installing the Control Panel in a Remote Location ...

Page 16: ...he User Settings section of this manual for information UP and DOWN arrows allow you to scroll between menu options items and values BACK allows you to return to the previous menu option item Please note that use of the BACK switch from a selection screen will return you to the previous menu option item while maintaining the selection s value upon entry ENTER allows you to activate a selected menu...

Page 17: ...er Cartridge Pack Installation 1 Open front left side door Turn the cartridge pack so the caps are facing you Remove the caps 2 Verify that each of the four posts on the car tridge pack has an o ring 3 Lift unit manifold upwards insert cartridge pack and align the pack so that it mates with the unit manifold 4 Lower unit manifold until it is flush with the top of the cartridge pack 5 Hand tighten ...

Page 18: ...to the I ON position 7 The system greeting will display the type of unit you own This greeting is UV 8 The system electronics will initialize and check its calibration All units have been factory cali brated If calibration is OK the display will show Calibration passed The display will next read Self Test in progress Self Test Passed Finally the display will read 10 0 2 MΩ cm This is a reading of ...

Page 19: ...tem injection port located on the right side of the cartridge pack manifold by turning counterclockwise 8 Remove syringe luer cap and attach syringe to the system luer fitting 9 Slowly inject solution into system and remove syringe Avoid injecting air into the system 10 Replace luer cap on injection port and close door 11 Press the UP or DOWN arrow to select YES and then press ENTER Display will n...

Page 20: ...icron filter and bell assembly from the bag and insert it into the dis penser arm manifold Gently turn it clockwise until it is fully seated 18 Remove the protective cap from the filter bell Turn the dispense knob to the left or right and flush 1 2 liters of water through the 0 2 micron filter The product water is now ready for use INITIAL OPERATION Note For more demanding applications where low T...

Page 21: ...ry set to OFF This feature is accessible only from the normal recirculating mode when the display is showing purity 1 Place a container under the dispenser 2 Press DISPENSE Water will start dispensing immediately Display will read xx MΩ cm xx Liters Remaining or xx MΩ cm xx Seconds Remaining or AUTO DISPENSE OFF depending on which dispensing method was last chosen in the auto dispense menu Normal ...

Page 22: ...s BACK until you return to the Idle mode Setting the Displayed Language 1 From the Idle mode when display reads NANOpure DIamond Idle xx xx xx xx xx xx press the BACK switch until the dis play reads LANGUAGE 2 The currently selected language is displayed on line 2 of the display 3 Press the UP or DOWN arrow to select the lan guage desired 4 Press ENTER Setting the Date and Time 1 From the Idle mod...

Page 23: ...9 When prompted with Set Time press the UP or DOWN arrow to choose Yes then press ENTER This is to set the time of day 10 Press the UP or DOWN arrow until you reach the desired hour value Press ENTER 11 Press the UP or DOWN arrow until you reach the desired minute value Press ENTER 12 Press BACK twice to return to the Idle mode Setting the Cell Constant The actual temperature and cell constants ar...

Page 24: ...d Menu 7 Press ENTER 8 Proceed through the options by pressing ENTER until Set Cell Constant is displayed 9 Press the UP or DOWN arrow to select Yes 10 Press ENTER 11 Note that the digits are entered from left to right 12 Press the UP or DOWN arrow to change the blinking digit Once the digit is correct press ENTER to advance to the next digit 13 After all digits have been entered line 2 of the dis...

Page 25: ...The lamp is on 10 minutes out of every four hours Press START STOP to return to the recirculating mode Selecting the Set Point The NANOpure DIamond UV electronics include a user programmable set point which alerts you when water quality falls below the programmed set point The set point is user selectable from 1 18 MΩ cm factory set at 10 MΩ cm 1 From the Idle mode when display reads NANOpure DIam...

Page 26: ...ill read Reset UV Timer NO 3 Press ENTER 4 Display will read Reset San Timer and show on the right side of the second line when the user will start receiving Sanitize Unit reminders 5 Press the UP or DOWN arrow to select Yes 6 Press ENTER and the timer will be reset This will reset the sanitization timer for approximately six months calendar time Resetting the UV Timer When the NANOpure DIamond UV...

Page 27: ... ENTER Display will read Volume Setting xx Liters 5 Press the UP or DOWN arrow to set the desired volume value Press ENTER UP arrow 0 25 up to 1 L then 5 L then incremental by 5 L DOWN arrow Decrement by 1 L until 1 L then by 0 25 L Maximum 60 L Minimum 0 25 L Note Volumetric dispensing is based upon total fluid volume entering the NANOpure DIamond UV Point of dra woff accuracy will be compromised...

Page 28: ...row 1 up to 5 min then increments by 5 minutes DOWN arrow Decrement by 1 minute Maximum 40 minutes Minimum 1 minute Performing a System Flush 1 From the normal recirculating mode when the dis play is showing purity press the UP or DOWN arrow until the display reads System Flush Press ENTER 2 Press the UP or DOWN arrow to select Short Flush or Extended Flush Press ENTER 3 Display will read System F...

Page 29: ... the display is showing purity press the Up or DOWN arrow until the display reads Temperature Compensation Press ENTER 2 Press the UP or DOWN arrow to select OFF or ON Press ENTER 3 Press BACK to return to the normal recirculating mode USER SETTINGS Note Purity displayed will have an asterisk the the left of the reading xx x MΩ cm or x xx uS cm to inform the user that uncompensated purity is being...

Page 30: ...ion instructions included with the float switch for installation into a tank 3 If using the D2706 low pressure switch install the PVC tee supplied with D2706 in the incoming water line Screw the switch into the top of the tee then connect the inlet tubing of the NANOpure DIamond UV into the remaining opening of the PVC tee 4 Route the cable from the float or low pressure switch to the top left of ...

Page 31: ... N I S T calibration module to the connection point J2 To Outlet Cell on the calibration board PC1190X2 5 Close and latch door 6 Reconnect the power cord and turn the unit on by depressing the main power switch 7 From the Idle mode Press the UP or DOWN arrow until the display reads N I S T Calibrate Press ENTER 8 Display will show Calibration Module Installed Press the UP or DOWN arrow to select Y...

Page 32: ... switch to the OFF O position Unplug the unit 13 Remove the calibration module and reconnect the cell 14 Reattach the cover plate and close and latch the door 15 Reconnect the power cord Calibration is now complete Remote Dispenser Refer to the Operating Instructions for your remote dis penser ...

Page 33: ...the normal Recirculation mode date time purity and temperature readings will be sent to the computer once per minute 7 Run your Microsoft Windows program Open Hyperterminal located in the accessories direc tory give your setting a name and choose a symbol 8 In the Connect Using box select direct to COM2 or COM1 as port depending on your computer and click OK 9 Using the selection boxes in the next...

Page 34: ...the NANOpure DIamond RS 232 port to COM2 port or COM1 port on back of computer 2 From the Idle display press the UP or DOWN arrow until the display reads Advanced Menu 3 Press ENTER 4 From the Printer Attached display Press the Up or DOWN arrow for NO 5 Press ENTER 6 The unit will now during the normal Recirculation mode send a purity and tempera ture reading to the computer once per minute 7 Open...

Page 35: ...e record for future reference During normal Recirculation the printer prints date time purity and temperature readings once every minute Connecting and Starting the Printer 1 Make sure the printer and NANOpure DIamond are turned OFF 2 Connect the NANOpure DIamond to the printer via the RS232 port Use the tan printer cable included with the Epson printer Plug the printer power cord into an electric...

Page 36: ... A The green POWER light will illuminate when the printer is ON Paper Feed Button Press this button once to advance the tape one line or hold the button down to advance paper continuously When the paper roll nears the end the red PAPER OUT light will illuminate If the red ERROR light illuminates the printer is off line This could be a result of the print head being too hot in which case the printe...

Page 37: ...traight 3 Insert the paper roll into the printer See Figure C 4 Insert the paper straight into the paper slot see Figure D The paper will feed automatically 5 Tear off a strip of paper and close the cover The red PAPER OUT light will be OFF if paper roll installation is successful COMPUTER PRINTER SETUP Note A colored stripe along the edge of the paper indicates that you are approach ing the end o...

Page 38: ...mended handling procedure This may be done in an ultrasonic cleaner or with a soft brush 6 Thoroughly rinse the cell in deionized or distilled water following the detergent or acid cleaning 7 After cleaning check the o ring replace if nec essary 8 Reinstall the cell into the cell well and hand tighten 9 Reroute the cable and reconnect to J2 on circuit board 10 Replace pc board cover and close door...

Page 39: ...on port Close door 11 Press the UP or DOWN arrow to select YES and then press ENTER Display will now read Reconnected Water NO 12 Attach feed water supply removed in step 4 13 Press the UP or DOWN arrow to select YES and press ENTER Display will now read Unit Sanitizing 39 MAINTENANCE AND SERVICING Note The sanitization timer will display after six months reminding you to sanitize the unit Complet...

Page 40: ...ld be done prior to removing a cartridge pack The unit needs to be plugged in and operating to correctly perform this depressurization step 1 IMPORTANT Disconnect inlet water from the left back of unit 2 From the Idle display press ENTER 3 From Air Purge press the UP arrow 4 From Depressurize press the UP arrow to select YES 5 Press ENTER Display will show System Flushing and the time remaining as...

Page 41: ...e sanitization 1 Remove the feed water line by depressing the stainless steel thumb pad 2 Depressurize the system by opening the remote dispenser or from an operational unit in the normal recirculating mode push the dispense knob to dispense water until no more water flows 3 Shut power OFF to the unit and disconnect the electrical service to the unit 4 Open the front left side door 5 Loosen the wi...

Page 42: ...g and insert it into the dispense arm mani fold Gently turn it clockwise until it is fully seat ed Remove the protective cap from the filter bell 3 Rinse 1 2 liters of water through the filter to drain prior to using the product water 42 MAINTENANCE AND SERVICING Caution Do not overtighten the 0 2 micron filter or use excessive force in seating it The filter can be damaged by over tightening or ex...

Page 43: ...rtically 3 Remove the black cap by sliding it off the UV chamber Disconnect and remove old UV lamp and dispose of it in the proper manner see Note 4 Remove the UV lamp from its packaging DO NOT TOUCH THE GLASS PORTION OF THE LAMP It is recommended that lint free gloves be worn when handling the lamp The glass por tion must be free of fingerprints perspiration etc Even a light coating of perspirati...

Page 44: ... out the fuse drawer located in the power entry module 3 Remove old fuses and replace with fuses of the same type and rating See Replacement Parts 4 Replace fuse drawer 5 Reattach the power cord 6 Operate normally Shutdown If the NANOpure DIamond UV is to be shut down for an extended period of time the unit should be completely drained and the new cartridge pack removed to prevent the growth of ba...

Page 45: ...not run feed water line pressure switch plug or pressure switch cord to the or jumper plug not connected to receptacle located on the upper left pump interlock hand section of the NANOpure DIamond Insufficient feed water pressure Open feed water line shut off connect or volume to satisfy the NANOpure feed water line to NANOpure DIamond DIamond and ensure sufficient pressure or sufficient water lev...

Page 46: ... described in UV Lamp Replacement Purity display continuously Air in system Dispense more water through the OVERRANGE NANOpure DIamond to purge air from the unit Bad cell connection Check the connection of the cell as it attaches to the meter circuit board mounted on the inside of the right door Incorrect N I S T calibration offset If you have a N I S T module perform a N I S T calibration If you ...

Page 47: ... door Water is leaking between the Wing head screws are not Tighten wing head screws on unit tight enough manifold manifold and the cartridge pack New cartridge pack o ring missing Disconnect inlet water and from post each of the 4 posts depressurize system Next disconnect must contain an o ring the manifold and verify replace missing o ring Reinstall cartridge pack as indicated in Cartridge Pack ...

Page 48: ...heck with your Barnstead Thermolyne representative for additional information on the expendables kit Recommended Description Catalog No Quantity DIamond Kit Organic Free R O Distilled Feed D50280 1 DIamond Kit Organic Free Deionized Feed D50281 1 Final Filter D3750 2 Main Fuse 120 Volt Slow Blow 1 6 Amp 250V FZX47 2 Main Fuse 230 Volt Type T Time Lag 0 63 Amp 250V FZX54 2 Teflon Tape Roll 06078 1 ...

Page 49: ... Cell E896X4 1 Solid State Ballast UV SC1191X1 1 Quartz Sleeve UV Lamp TU733X1 1 Power Supply PC Board TNX116 1 Calibration PC Board PCX48 1 Resistivity Meter PC Board PC896X2 1 Check Valve PMX214 1 Wire Harness UV Bulb WH1191X1 1 Flow Sensor ME1190X1 Flush Solenoid RY1190X3 1 Unit Manifold Dispenser Manifold Dispense Switch SW1190X1 1 Optional Accessory Ordering Information Description Catalog No...

Page 50: ...ermolyne Vx xx Style English Advanced menu Set Time Set Date Optional Printer Date Format Set Cell Constant Adjust Set Point Set Display Brightness Diagnostics menu Air Purge Purity display up or down keys pressed Change Units System flush Auto Dispense Menu Temperature Compensation dispense key pressed enter key pressed C back key pressed force print line Arrow Legend Keypress Options Automatic E...

Page 51: ...SW1190X1 SW1190X1 SW1190X1 TNX116 TNX116 TNX116 PU1190X1 PU1190X1 PU1190X1 PC896X2 PC896X2 PC896X2 PC1190X2 PC1190X2 PC1190X2 PC1190X1 PC1190X1 PC1190X1 LMX13 ME1190X1 ME1190X1 ME1190X1 WH9 CAL METER HARNESS WM896X2 WM1 GROUND WIRE WM1190X2 WH7 DISPLAY HARNESS WHX19 WH6 METER BOARD HARNESS WH1190X6 WH5 PRESSURE SW HARNESS WH1190X5 WH4 CAL BOARD HARNESS WH1190X4 WH3 AC POWER HARNESS WH1190X3 WH2 DC...

Page 52: ...rmolyne dealer from whom you purchased this unit or can be obtained promptly from the factory When service or replacement parts are needed we ask that you check first with your dealer If the dealer cannot handle your request then contact our Customer Service Department at 319 556 2241 or 800 553 0039 Prior to returning any materials to Barnstead Thermolyne Corp please contact our Customer Service ...

Page 53: ...s own discretion Heating elements however because of their susceptibility to overheating and contamination must be returned to our factory and if upon inspection it is concluded that failure is not due to excessive high temperature or contamination warranty replacement will be provided by Barnstead Thermolyne The name of the authorized Barnstead Thermolyne dealer nearest you may be obtained by cal...

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Page 56: ...9001 ISO REGISTERED Barnstead Thermolyne 2555 Kerper Blvd P O Box 797 Dubuque IA 52004 2241 Phone 319 556 2241 800 553 0039 Fax 319 589 0516 E Mail Address mkt barnstead com ...

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