Argonaut Technologies QUEST GASEOUS REACTION AND CONCENTRATION MANIFOLD User Manual Download Page 1

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Summary of Contents for QUEST GASEOUS REACTION AND CONCENTRATION MANIFOLD

Page 1: ...service in house repair center WE BUY USED EQUIPMENT Sell your excess underutilized and idle used equipment We also offer credit for buy backs and trade ins www artisantg com WeBuyEquipment REMOTE IN...

Page 2: ...QUESTGASEOUS REACTION AND CONCENTRATION MANIFOLD PN 103952 Rev 1 0 28 October 1999 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Page 3: ...e reliability function or design Argonaut does not assume any liability arising out of the application or use of any product described herein neither does it convey any license under its patent rights...

Page 4: ...FACT OR BY OPERATION O F LAW STATUTORY OR OTHERWISE AND SELLER EXPRESSLY EXCLUDES AND DISCLAIMS ANY WARRANTY O F MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE Limitation of Liability Buyer agree...

Page 5: ...ers normal use Exclusions from this limited warranty may include Servicing or modification by anyone other than a qualified Argonaut Technologies Service Representative Non conformance to recommended...

Page 6: ...e and Firmware Compliance Safety User Attention Words Warning Labels System Safety Safety Equipment Operating Environment RV Sealing Capabilities Material Safety Data Sheets MSDS GRCM Installation Lis...

Page 7: ...sing the GRCM Hydrogenation Concentration By Evaporation Cleaning the GRCM Gas Delivery Manifold Using the Quest 210 Using the Quest ASW Female Luers on the Quest Lower Manifold A Service Contact Info...

Page 8: ...additional gas delivery manifold Gas Delivery Manifold The gas delivery manifold attachesto the Quest 210 lower manifold luers and delivers gas to the reaction vessels The delivery manifoldhas a gas i...

Page 9: ...CE 1 1 l 1 I l 1 I 1 I f 1 I 1 1 I I 1 I I 1 I l I I 1 I I I I I 1 I I I I I I I I 1 I I 1 I I I I 1 1 1 I The Gaseous Reaction and Concentration Manifold has no related software or firmware For a det...

Page 10: ...pment on which it is used USER ATTENTION W O R D S 1 1 1 1 I 1 1 1 1 1 l n 1 o 1 1 1 1 1 I I I I I I I I I I I I I I l I I t I t l 1 l 1 1 1 l 1 l 1 1 1 User attention words appear in the text of this...

Page 11: ...lied to the equipment in specific areas where the user must observe safety precautions Following is a list of these labels and their meanings Label This symbolindicatesahot surface Use caution when wo...

Page 12: ...will be adversely affected Quest software and hardware does not control temperature based uponthe boiling point and freezing point of the contents of reaction vessels ACaution The GRCM is designed to...

Page 13: ...peration OPERATING ENVIRONMENT 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 I I 1 1 I 1 I 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 The Questm Gaseous Reaction and Concentration Manifold has been tes...

Page 14: ...psig 1 69 barr Delivery Manifold installed M A T E R I A L SAFETY DATA SHEETS M S D S 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 l 1 1 1 1 The MSDS...

Page 15: ...GRCM User Manual Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Page 16: ...ivery Manifold This manifold attaches to the reaction vessel drain hers to allow the delivery of gas to a bank of reaction vessels Part number 300676 Solvent Trap Manifold This manifold is inserted in...

Page 17: ...USER The user must provide the following items An external gas tank for gaseous reagents with a 0 30 psig 1 01 3 08 barr regulator to control the input pressure Nitrogen gas for sparging A house supp...

Page 18: ...ut which connects to the Quest controller using the supplied T and Teflonmtubing Input 2 is the reagent gas input which connects to a user provided regulator We recommend using a regulator designed fo...

Page 19: ...ilical Line 3 Inert Gas Extension Line Part Number 300796 Figure 2 GRCM Control Box Installation 1 On the front of the Quest controller locatethe ports for the five 118 inch Teflon linesfrom the React...

Page 20: ...Part number 300795 to side C of the T Connectthe other end to input 1 of the GRCM Control box See Figure3 below 6 lnsert the 118 inch PEEK fitting of the reagent gas inlet line Part number 300796 to i...

Page 21: ...e container and set it aside 4 Select the side of the Quest reactor which you will be using 5 Align the female hers of the Gas Delivery Manifold with the male luers of the reaction vessel outlets 6 Ge...

Page 22: ...by evaporation 1 Removethe her plugs from the upper manifold of the reaction bank which you will be using 2 Align the male fittings of the Solvent Trap Manifoldwith the upper manifold ports 3 Gently p...

Page 23: ...arated and fitted A Quest Upper Manifold and Solvent Trap Manifold Separated B Solvent Trap Manifold Fitted to Quest Upper Manifold Pnnnertinn Figure 5 Solvent Trap Manifold and the Quest Upper Manifo...

Page 24: ...Installation Steps Figure 6 The Gas Delivery Manifold Installed Figure 7 Gas Delivery and Solvent Trap ManifolIds Installed GRCM User Manual Artisan Technology Group Quality Instrumentation Guaranteed...

Page 25: ...Delivery Manifold of the Expansion Kit 3 Attach the Gas Delivery Manifold to the Lower Manifold Luers for the appropriate reaction bank Solvent Trap Manifold If you are carrying out concentration ins...

Page 26: ...this chapter you must be familiar with the installation procedures described in Chapter 3 GRCM Installation HYDROGENATION 1 1 1 1 1 1 1 1 1 1 1 1 1 1 l 1 1 1 1 I I I I I I I I I I I I 1 I I I I I I I...

Page 27: ...fold Line Part umber 300794 Inert Gas Extension Line I I Quest 210 Controller Part Number 300797 P o r t 3 4 5 6 UUU 7 ssembl Part Number GRCM Control Box 1 2 Reagent Gas e g hydrogen Reagent as Inlet...

Page 28: ...until it i s completely closed b Turn Quest control valves to Metered Gas and Utility 1 c Slowly turn the metered gas needle valve counterclockwise to purge the reaction vessels with N2 6 Add solvent...

Page 29: ...to CLOSED d Move the membrane switch above the Quest control valves from OPEN to CLOSED e Programthe desired mixing rate on the Quest controller and start the agitation 13 Venting the reaction a Turn...

Page 30: ...etup in schematic form For details of the installation procedures see Chapter 3 GRCM Installation Bank A uest 210 eactor Concentration Setup Line to Solvent Trap Expansion Kit Gas Delivery ManifoldLin...

Page 31: ...Quest Lower Manifold 7 Slowlyturn the Out A needlevalvecounterclockwise to adjust the gas flow To achievefastest evaporation rates maximizethe gas flow without allowing the liquidto bubble over As th...

Page 32: ...Figure 10 Evaporation at 45 C for One Hour C L E A N I N G THE GRCM 1 o 1 1 f 1 1 1 1 o 1 1 l 1 o a I l I a t l a a l I I I I I I I I I I B l 1 l l 1 l l 1 1 l l 1 It is essential to clean the GRCM t...

Page 33: ...rol Valve 1 to CLOSED 8 DetachGas Delivery Manifold Line from the Quest 210 and reattach to outlet on the GRCM control box 9 ReattachUpper Manifold Delivery Line to Quest 210 Using the Quest ASW 1 Det...

Page 34: ...5 minutes to remove all solvent from the Gas Delivery Manifold b Turn Control Valve 1to CLOSED 9 DetachGas Delivery Manifold Line from the Quest 210 and reattach to outlet on the GRCM control box 10...

Page 35: ...GRCM User Manual Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Page 36: ...ted States Argonaut Technologies 887 Industrial Road Suite G San Carlos CA 94070 USA Phone 650 598 1350 or 888 598 1350 USAICanada Fax 650 598 1359 In Europe Argonaut Technologies A G St Jakob Strasse...

Page 37: ...ogies K K MK Kojimachi Bldg 4 2 1 Kojimachi Chiyoda Ku Tokyo 102 0083 Japan Phone 81 3 3234 432 1 Fax 81 3 3234 1359 GRCM User Manual Artisan Technology Group Quality Instrumentation Guaranteed 888 88...

Page 38: ...ch Teflon tubing 118 inch PEEK fittings and associated Tefzel ferrules 300794 Solvent Trap Connection 3 feet of inch I D Tygon tubing for Solvent Trap connection 103954 Inert Gas Extension Line 2 inch...

Page 39: ...n 1 Gas Delivery Manifold 300676 1 Solvent Trap Manifold with inch barb fitting 300677 Gas Delivery Manifold Line 7 feet of 118 inch Teflon tubing 118 inch PEEK fitting and associated Tefzel ferrules...

Page 40: ...Solvent Trap Manifold 3 15 Interference 1 2 M Material Safety Data Sheets 2 7 0 Operating Environment 2 6 Overview 1 1 3 11 R Reaction Vessel RV Sealing 2 7 S Safety 2 3 Safety Equipment 2 5 Service A...

Page 41: ...I N D E X IND E X 2 GRCM User Manual Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com...

Page 42: ...service in house repair center WE BUY USED EQUIPMENT Sell your excess underutilized and idle used equipment We also offer credit for buy backs and trade ins www artisantg com WeBuyEquipment REMOTE IN...

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