Agilent Technologies G4782A User Manual Download Page 152

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152

1260 SFC Binary Pump

Identifying Cables

Agilent 1200 Module to Printer

To connect a USB Flash Drive use a USB OTG cable with Mini-B plug and A
socket.

p/n

Description

5188-8050

USB A M-USB Mini B 3 m (PC-Module)

5188-8049

USB A F-USB Mini B M OTG (Module to Flash Drive)

Summary of Contents for G4782A

Page 1: ...Agilent Technologies Agilent InfinityLab LC Series 1260 Infinity II SFC Binary Pump User Manual...

Page 2: ...are furnished under a license and may be used or copied only in accordance with the terms of such license Restricted Rights Legend If software is for use in the performance of a U S Government prime...

Page 3: ...meters of the Binary Pump 4 Optimizing Performance This chapter gives information on how to optimize the performance of the Binary Pump under special operational conditions 5 Troubleshooting and Diagn...

Page 4: ...s This chapter provides information on cables used with the Agilent InfinityLab LC Series modules 11 Hardware Information This chapter provides detailed technical information about your binary pump 12...

Page 5: ...7 Hints for Successful Use of the Binary Pump 39 Setting up the Pump with the G4208A Instant Pilot 40 Setting up the Pump with the Instrument Control Interface 41 Solvent Information 46 Algae Growth i...

Page 6: ...e Valve 102 Remove the Pump Head Assembly 105 Maintenance of a Pump Head without Seal Wash 107 Maintenance of a Pump Head with Seal Wash 110 Reinstall the Pump Head Assembly 114 Seal Wear in Procedure...

Page 7: ...onnections 157 Interfaces 159 Setting the 6 bit Configuration Switch 166 Early Maintenance Feedback 170 Instrument Layout 171 12 LAN Configuration 173 What You Have to Do First 174 TCP IP parameter co...

Page 8: ...8 1260 SFC Binary Pump Contents...

Page 9: ...ment and Operation 10 Introduction to the Pump 10 Principle of Operation 11 Product Description 12 Features 12 Overview of the Hydraulic Path 13 Leak and Waste Handling 17 Waste Concept 21 This chapte...

Page 10: ...ser is available for applications that require best flow stability especially at low flow rates for maximum detector sensitivity The pump is capable of delivering flow in the range of 0 1 5 mL min aga...

Page 11: ...p to 600 bar Each channel comprises a pump assembly including pump drive pump head and outlet valve The two channels are fed into cross connector which is connected to a damping unit and a mixer A pre...

Page 12: ...tegrated solvent selection 2 channel degasser and built in active seal wash on channel A for increased uptime Figure 2 Overview of the pump Features Fast and precise gradients the pump is the perfect...

Page 13: ...he pump through an active inlet valve Each side of the binary pump comprises two substantially identical pump units Both pump units comprise a ball screw drive and a pump head with two sapphire piston...

Page 14: ...itialization the pump starts operation with the set parameters for the two pump channels The inlet valve is opened and the down moving piston draws solvent into the first pump head At the same time th...

Page 15: ...how compressibility compensation works Piston 1 draws solvent at ambient pressure The movement direction is reversed and piston 1 now compresses the solvent until the operating pressure of the HPLC sy...

Page 16: ...ity compensation for the solvent in use Small stroke volumes generate less pressure pulsation than larger stroke volumes at the same flow rate In addition the frequency of the pressure pulsation will...

Page 17: ...rnet All leak plane outlets are situated in a consistent position so that all Infinity and Infinity II modules can be stacked on top of each other Waste tubes are guided through a channel on the right...

Page 18: ...18 1260 SFC Binary Pump 1 Introduction Leak and Waste Handling Figure 4 Infinity II Leak Waste Concept flexible rack installation...

Page 19: ...1260 SFC Binary Pump 19 Introduction 1 Leak and Waste Handling Figure 5 Infinity II Single Stack Leak Waste Concept bench installation...

Page 20: ...duction Leak and Waste Handling Figure 6 Infinity II Two Stack Leak Waste Concept bench installation The waste tube connected to the leak pan outlet on each of the bottom instruments guides the solven...

Page 21: ...ng Waste Concept 1 Agilent recommends using the 6 L waste can with 1 Stay Safe cap GL45 with 4 ports 5043 1221 for optimal and safe waste disposal If you decide to use your own waste solution make sur...

Page 22: ...22 1260 SFC Binary Pump 1 Introduction Leak and Waste Handling...

Page 23: ...nt Technologies 2 Site Requirements and Specifications Site Requirements 24 Physical Specifications 27 Performance Specifications 28 This chapter provides information about site requirements and speci...

Page 24: ...use automatic electronic fuses are implemented in the power supply WARNING Hazard of electrical shock or damage of your instrumentation can result if the devices are connected to a line voltage higher...

Page 25: ...er connector of the instrument can be easily reached and unplugged Provide sufficient space behind the power socket of the instrument to unplug the cable WARNING Absence of ground connection The absen...

Page 26: ...G Power cords Solvents may damage electrical cables Prevent electrical cables from getting in contact with solvents Exchange electrical cables after contact with solvents NOTE Agilent recommends that...

Page 27: ...10 Wide ranging capability Line frequency 50 or 60 Hz 5 Power consumption 90 VA 74 W Ambient operating temperature 4 55 C 39 131 F Ambient non operating temperature 40 70 C 40 158 F Humidity 95 r h a...

Page 28: ...eater Based on retention time at constant temperature Pressure operating range Up to 60 MPa 600 bar 8702 psi up to 5 mL min Compressibility compensation Pre defined based on mobile phase compressibili...

Page 29: ...ea Network LAN Safety and maintenance Extensive diagnostics error detection and display through Agilent LabAdvisor leak detection safe leak handling leak output signal for shutdown of the pumping syst...

Page 30: ...30 1260 SFC Binary Pump 2 Site Requirements and Specifications Performance Specifications...

Page 31: ...the Pump with the G4208A Instant Pilot 40 Setting up the Pump with the Instrument Control Interface 41 Overview 41 Setup of Basic Pump Parameters 41 Pump Control 42 Auxiliary Pump Parameters 43 Data C...

Page 32: ...32 1260 SFC Binary Pump 3 Using the Pump Magnets Magnets 1 This stack exemplarily shows the magnets positions in the modules...

Page 33: ...1260 SFC Binary Pump 33 Using the Pump 3 Turn on off Turn on off 1 Plug in power cord 2 Power switch 1 On 2 Off 3 Plug off the module...

Page 34: ...e 2 Run mode 3 Not ready Waiting for a specific pre run condition to be reached or completed 4 Error mode interrupts the analysis and requires attention for example a leak or defective internal compon...

Page 35: ...fer applications were used Inspect solvent filters for dirt or blockages Clean or exchange if no flow is coming out of the solvent line when removed from the degasser inlet Power up Shut down the pump...

Page 36: ...volatile additives How to deal with solvents Use clean bottles only Exchange water based solvents daily Select solvent volume to be used up within 1 2 days Use only HPLC grade solvents and water filte...

Page 37: ...ons Always keep the temperature in the sample compartment at least 25 K below the boiling point of the solvent used Do not operate the instrument in an explosive atmosphere Reduce the volume of substa...

Page 38: ...ing Waste Concept 1 Agilent recommends using the 6 L waste can with 1 Stay Safe cap GL45 with 4 ports 5043 1221 for optimal and safe waste disposal If you decide to use your own waste solution make su...

Page 39: ...Check purge valve frit and column frit in regular time intervals A blocked purge valve frit can be identified by black yellow or greenish layers on its surface or by a pressure greater than 10 bar in...

Page 40: ...ith the G4208A Instant Pilot Generic operation of the G4208A Instant Pilot is covered in the Agilent Instant Pilot G4208A User s Guide G4208 90006 Details about setting up module specific parameters c...

Page 41: ...run manually useful for method development Post Time off 99999 min Time between the end of a run and the start of the next Used for column equilibration after a gradient Pressure Limits Max 0 600 bar...

Page 42: ...n will show up in method printouts etc Timetable max number of lines depends on free space in pump memory Use the timetable to build solvent gradients flow gradients or combinations of both Gradients...

Page 43: ...scription Maximum Flow Gradient 0 1 100 mL min default 100 mL min With this parameter flow rate changes can be ramped up and down slowly to avoid pressure shocks to the column The default value is 100...

Page 44: ...sure data curve is generated from the pressure sensor readings while A B and flow are calculated from the method settings of the pump CAUTION The bottle filling feature fails if multiple solvent inlet...

Page 45: ...volume in liter which considers the position of the solvent inlet and size shape of the solvent bottle such that no air is drawn if the actual volume gets close to this limit Turn pump off default unc...

Page 46: ...ions for the pH range given for different materials like flow cells valve materials etc and recommendations in subsequent sections Materials in Flow Path Following materials are used in the flow path...

Page 47: ...f UHPLC systems solvents solvent mixtures and samples Information can also not be generalized due to catalytic effects of impurities like metal ions complexing agents oxygen etc Apart from pure chemic...

Page 48: ...compatibility of PEEK Polyimide Agilent uses semi crystalline polyimide for rotor seals in valves and needle seats in autosamplers One supplier of polyimide is DuPont which brands polyimide as Vespel...

Page 49: ...if your chromatography method allows by phosphoric acid or phosphate buffer which are less corrosive against stainless steel Halogenated solvents or mixtures which form radicals and or acids for exam...

Page 50: ...with ammonia 10 Diamond Like Carbon DLC Diamond Like Carbon is inert to almost all common acids bases and solvents There are no documented incompatibilities for HPLC applications Fused silica and Quar...

Page 51: ...ts like halogenated hydrocarbons TFE PDD copolymer tubings which are used in all Agilent degassers except 1322A are not compatible with fluorinated solvents like Freon Fluorinert or Vertrel They have...

Page 52: ...adient problems or a complete failure of the pump Small pore high pressure solvent filters usually placed before the injector to plug resulting in high system pressure PTFE frits blockage leading to i...

Page 53: ...e solvent Place a layer of argon on top of your solvent Avoid exposure of the solvent bottle to direct sunlight Checking the Solvent Filters The solvent filters are located on the low pressure side of...

Page 54: ...apillary columns can be damaged by nitric acid Replace the filter WARNING When opening capillary or tube fittings solvents may leak out The handling of toxic and hazardous solvents and reagents can ca...

Page 55: ...for valve balls which is a conductive ceramic and replaces non conductive ruby balls The balls do not charge up electrostatically and show good performance in normal phase The valves are marked with N...

Page 56: ...ls have a limited life time when used with normal phase solvents and sapphire pistons Agilent recommends a maximum pressure of 200 bar for this combination which shall also be applied for pressure tes...

Page 57: ...al Hints for the Vacuum Degasser 58 When to Use the Active Seal Wash Option 59 How to Optimize the Compressibility Compensation Setting 60 Optimization of Legacy Compressibility Settings 60 This chapt...

Page 58: ...is used with maximum sensitivity in the low UV wavelength range Your application requires highest injection precision Your application requires highest retention time reproducibility flow rates below...

Page 59: ...ash option comprises a peristaltic pump secondary seals gaskets seal holders and tubing for both pump heads A bottle of premixed water isopropanol 90 10 vol is placed in the solvent cabinet and connec...

Page 60: ...ue for the actual pump pressure Compressibility data for the most common solvents is readily available in the pump firmware The compensation algorithm is so powerful that the damper and mixer can be r...

Page 61: ...table Use degassed solvent only Check the tightness of the system with the pressure test see 3 Your pump must be connected to an Agilent data system or Instant Pilot the pressure and ripple can be mon...

Page 62: ...Binary Pump 4 Optimizing Performance How to Optimize the Compressibility Compensation Setting Methanol 120 1 Propanol 100 Toluene 87 Water 46 Table 8 Solvent Compressibility Solvent pure Compressibili...

Page 63: ...Binary Pump Agilent Technologies 5 Troubleshooting and Diagnostics Overview of the Module s Indicators and Test Functions 64 Agilent Lab Advisor Software 65 Overview of the troubleshooting and diagnos...

Page 64: ...check of the operation of the module Error Messages In the event of an electronic mechanical or hydraulic failure the module generates an error message in the user interface For each message a short...

Page 65: ...finity Series and Agilent InfinityLab LC Series instrument The Lab Advisor Advanced features can be unlocked by purchasing a license key and include real time monitoring of instrument actuals all vari...

Page 66: ...66 1260 SFC Binary Pump 5 Troubleshooting and Diagnostics Agilent Lab Advisor Software...

Page 67: ...nsor Open 74 Compensation Sensor Short 74 Fan Failed 75 Open Cover 76 Module Error Messages 77 Solvent Zero Counter 77 Pressure Above Upper Limit 77 Pressure Below Lower Limit 78 Pressure Signal Missi...

Page 68: ...Pump Head Missing 86 Index Limit 86 Index Adjustment 87 Index Missing 87 Stroke Length 88 Initialization Failed 88 This chapter describes the meaning of error messages and provides information on pro...

Page 69: ...LEDs get red and the run will be stopped Depending on the module type this stop is implemented differently For example for a pump the flow will be stopped for safety reasons For a detector the lamp wi...

Page 70: ...as present during a sequence or multiple injection run for a period longer than the timeout threshold Check the logbook for the occurrence and source of a not ready condition Restart the analysis wher...

Page 71: ...f one or more of the modules is no longer recognized as being connected to the system the error message is generated Probable cause Suggested actions 1 Not ready condition in one of the instruments co...

Page 72: ...k sensor is cooled by the solvent This changes the resistance of the leak sensor which is sensed by the leak sensor circuit on the main board Probable cause Suggested actions 1 Loose fittings Ensure a...

Page 73: ...ent to change within defined limits If the current increases above the upper limit the error message is generated Probable cause Suggested actions 1 Leak sensor not connected to the Power Switch board...

Page 74: ...error message is generated Compensation Sensor Short Error ID 0080 The ambient compensation sensor NTC on the main board in the module has failed open circuit The resistance across the temperature co...

Page 75: ...time the error message is generated This limit is given by 2 revolutions second for longer than 5 seconds Depending on the module assemblies e g the lamp in the detector are turned off to assure that...

Page 76: ...message is generated Probable cause Suggested actions 1 The top foam was removed during operation Please contact your Agilent service representative 2 Foam not activating the sensor Please contact yo...

Page 77: ...matches the actual bottle filling and set the shutoff limit to a reasonable value e g 100 mL for 1 L bottles Probable cause Suggested actions 1 Upper pressure limit set too low Ensure the upper pressu...

Page 78: ...lower pressure limit is set to a value suitable for the analysis 2 Air bubbles in the mobile phase Make sure that the degasser is in flow path and works correctly Purge the module Ensure solvent inle...

Page 79: ...efore and after each switching cycle If the voltages are outside expected limits the error message is generated Probable cause Suggested actions 1 Solvent selection valve disconnected Please contact y...

Page 80: ...mp configuration The binary pump is assigned its configuration at the factory If the active inlet valve and pump encoder of channel B are disconnected and the binary pump is rebooted the error message...

Page 81: ...lectronic fuse to open Probable cause Suggested actions 1 Defective solvent selection valve Restart the pump If the error message appears again exchange the solvent selection valve 2 Defective connect...

Page 82: ...continually monitors the temperature of the drive circuits on the main board If excessive current is being drawn for long periods the temperature of the circuits increases If the temperature exceeds...

Page 83: ...hes the maximum limit the module is switched off and the error message is generated Probable cause Suggested actions 1 Flow path blockage in front of the damper Ensure the capillaries and frits betwee...

Page 84: ...n the module is missing or defective The processor checks the presence of the pump encoder connector every 2 s If the connector is not detected by the processor the error message is generated Probable...

Page 85: ...e to take control of the phase sequencing with the commutator If the rotor is unable to move or if the C position cannot be reached the error message is generated Probable cause Suggested actions 1 Me...

Page 86: ...hort pump During initialization the first piston is moved to the mechanical stop After reaching the mechanical stop the piston reverses direction until the encoder index position is reached If the ind...

Page 87: ...dule was not found during initialization During initialization the first piston is moved to the mechanical stop After reaching the mechanical stop the piston reverses direction until the encoder index...

Page 88: ...rated Initialization Failed Error ID 2207 2217 Initialization Failed Pump channel A B Initialization Failed Pump channel B The module failed to initialize successfully within the maximum time window A...

Page 89: ...89 1260 SFC Binary Pump Agilent Technologies 7 Test Functions and Calibration Pump Leak Rate Test 90 This chapter explains all test functions that are available for the binary pump...

Page 90: ...7 Test Functions and Calibration Pump Leak Rate Test Pump Leak Rate Test Introduction The Pump Leak Rate Test is used for verifying the internal tightness of the pump and helps identifying parts which...

Page 91: ...O Ring on the Purge Valve 102 Remove the Pump Head Assembly 105 Maintenance of a Pump Head without Seal Wash 107 Maintenance of a Pump Head with Seal Wash 110 Reinstall the Pump Head Assembly 114 Seal...

Page 92: ...enance Introduction to Maintenance The pump is designed for easy maintenance The most frequent maintenance procedures such as piston seal replacement and purge valve frit exchange can be done from the...

Page 93: ...p edged parts of the equipment may cause injuries To prevent personal injury be careful when getting in contact with sharp metal areas WARNING Toxic flammable and hazardous solvents samples and reagen...

Page 94: ...e board by the edges and do not touch the electrical components Always use ESD protection for example an ESD wrist strap when handling electronic boards and components CAUTION Safety standards for ext...

Page 95: ...cloth slightly dampened with water or a solution of water and mild detergent WARNING Liquid dripping into the electronic compartment of your module can cause shock hazard and damage the module Do not...

Page 96: ...and can be accessed from the front simple repairs Replacement of valve or filters don t require to remove the pump from the system stack Figure 7 Overview of Maintenance and Simple Repairs 1 2 3 4 5...

Page 97: ...ly on page 105 During yearly maintenance Necessary to get access to pump seals and pistons Maintenance of a Pump Head without Seal Wash on page 107 Yearly or if pump performance indicates seal wear Le...

Page 98: ...ed p n Description 5067 5746 Door Assembly Infinity 180 Right 5067 5745 Door Assembly Infinity 180 Left NOTE The figures shown in this procedure exemplarily show the Infinity II Multisampler module Th...

Page 99: ...Remove and Install Doors 1 Press the release buttons and pull the front door out 2 For the Installation of the front door Insert the hinges into their guides and move the door in until the release bu...

Page 100: ...required p n Description 8710 0510 Wrench open 1 4 5 16 inch 8710 1924 Wrench open 14 mm Pair of tweezers OR Toothpick Parts required p n Description Frits Purge Valve 5067 4728 Seal cap Preparations...

Page 101: ...oothpick remove the frit 4 Place a new frit into the purge valve with the orientation of the frit as shown below slit in frit points to the front Reinstall the seal cap including the gold seal 5 Inser...

Page 102: ...Toothpick Parts required p n Description 1 5067 6595 1260 PV O ring FKM 5 pack 1 01018 22707 PTFE frits pack of 5 OPTIONAL 1 5067 4728 Seal cap OPTIONAL Preparations Switch off pump at the main power...

Page 103: ...e Purge Valve Body 6 Place the mounting ring on the screw and push down the o ring 7 Place a new frit into the purge valve with the orientation of the frit as shown below slit in frit points to the fr...

Page 104: ...lace the O Ring on the Purge Valve 8 Push the screw up and guide the o ring into the gap 9 Install the purge valve to the pump make sure that you do not turn the Purge Valve Body when the screw is fix...

Page 105: ...0240 Hex driver slitted Preparations Switch off the pump at the main power switch CAUTION Damage of the pump drive Starting the pump when the pump head is removed may damage the pump drive Never start...

Page 106: ...nce Remove the Pump Head Assembly 1 Open the doors 2 Disconnect the capillaries Beware of leaking solvents 3 Using a 4 mm hexagonal key stepwise loosen and remove the two pump head screws 4 Remove the...

Page 107: ...l PTFE carbon filled black pack of 2 default OR 1 0905 1420 PE seals pack of 2 1 5067 4695 Sapphire piston Preparations Switch off the pump at the main power switch Open the doors of the module Use an...

Page 108: ...carefully pull the pump housing away from the piston housing 3 Remove the support rings from the piston housing 4 Lift the housing away from the pistons 5 Check the piston surface and remove any depos...

Page 109: ...sert tool insert new seals into the pump head 8 Place the support rings on the piston housing Note the correct position of the pins on the support ring 9 Place the pump housing onto the piston housing...

Page 110: ...1718 Wash seal PTFE 5062 2484 Gasket seal wash pack of 6 5067 4695 Sapphire piston 0905 1719 PE Seal Preparations Switch off the pump at the main power switch Open the doors of the module Use an opti...

Page 111: ...t ring assembly 5 Lift the housing away from the pistons 6 Check the piston surface and remove any deposits or layers clean the piston surface with abrasive paper and rinse with 2 propanol Replace pis...

Page 112: ...w wash seal spring pointing upwards into the recess of the support ring 11 Place a seal wash gasket in the recess of the support ring Use a matching orientation of gasket and support ring Put the seal...

Page 113: ...1260 SFC Binary Pump 113 Maintenance 8 Maintenance of a Pump Head with Seal Wash 15 Tighten the lock screw 16 Install the pump head see...

Page 114: ...d Assembly When When reassembling the pump Tools required 3 mm hexagonal key 4 mm hexagonal key 1 Slide the pump head assembly onto the pump drive 2 Using a 4 mm hexagonal key tighten the pump head sc...

Page 115: ...m for 5 min with isopropanol at a flow rate of 2 mL min 5 Close the purge valve set the flow to a value that gives a pressure of 350 bar Pump 15 min at this pressure to wear the seals in The pressure...

Page 116: ...n Description 5065 4445 Peristaltic pump with Pharmed tubing Preparations Switch off pump at the main power switch Open the doors 1 Remove the wash solvent tubings from the support ring outlet and fr...

Page 117: ...eal Wash Cartridge 3 Put the new peristaltic pump cartridge onto the rod of the pump motor and push the plastic clips into the module housing 4 Connect the peristaltic pump tubes to the support rings...

Page 118: ...ubing assembly i d 6 mm o d 9 mm 1 2 m to waste approximately 85 mm required 1 Open the doors 2 Press the Leak Adapter down and remove it together with the tubing 3 Install the Leak Adapter by pressin...

Page 119: ...ive inlet valve G4302 60066 Inlet Valve SFC Preparations Switch off the pump at the main power switch 1 Disconnect the solvent inlet tube at the inlet valve beware of leaking solvents 2 Using a 14 mm...

Page 120: ...mm Parts required p n Description 1 G1312 60167 Outlet valve Channel A 2 G1312 60067 Outlet valve Channel B Preparations Switch off the pump at the main power switch 1 Using a inch wrench disconnect...

Page 121: ...1260 SFC Binary Pump 121 Maintenance 8 Exchange the Outlet Valve 3 Reinstall the outlet valve and tighten it using a torque wrench approx 12 Nm 4 Reconnect the capillary approx 12 Nm...

Page 122: ...on Valve Upgrade Kit Preparations Switch off the pump at the main power switch 1 Lift solvent bottles out of the solvent cabinet and place them on the table Disconnect the solvent tubes from the solve...

Page 123: ...election valve 6 Tighten the screws of the valve holder 7 Reconnect all tubings to the solvent selection valve NOTE After an exchange of the valve it may be required to pump several mL of solvent befo...

Page 124: ...or this module When The installation of newer firmware might be necessary if a newer version solves problems of older versions or to keep all systems on the same validated revision The installation of...

Page 125: ...Pump Head Assembly Channel B 128 Pump Head Assembly Channel A 130 Outlet Valve 132 Purge Valve Assembly 133 HPLC System Tool Kit 134 Active Seal Wash Option 135 Solvent Cabinet 136 Bottle Head Assembl...

Page 126: ...egasser to Channel B 6 1 G1312 87305 Capillary SSL 0 17 x 150 mm pressure sensor to damper 7 13 1 G1316 87300 Capillary ST 0 17 mm x 90 mm S S 8 1 G1312 87300 Absorber capillary 9 1 G7111 60061 Purge...

Page 127: ...1260 SFC Binary Pump 127 Parts and Materials for Maintenance 9 Hydraulic Path with Solvent Selection Valve Figure 8 Hydraulic Path with Solvent Selection Valve 1 2 3 4 5 6 7 8 9 10 11 12 13...

Page 128: ...20 60015 Support ring including backup ring 5 1 0905 1503 Pump seals PTFE PumpHead B 6 1 G1312 25260 Pump housing 7 1 G1312 60066 Passive inlet valve 8 1 G7111 60061 Purge valve 9 1 0515 2118 Pump hea...

Page 129: ...1260 SFC Binary Pump 129 Parts and Materials for Maintenance 9 Pump Head Assembly Channel B Figure 9 Pump Head Assembly Without Seal Wash 1 2 3 4 5 6 7 8 9 10 11 12 13...

Page 130: ...G4220 60016 Seal holder including backup ring 7 0905 1719 PE Seal 8 G1312 25260 Pump housing 9 G4302 60066 Inlet Valve SFC 10 0515 2118 Pump head screw M5 60 mm 11 G1312 60001 Adapter 12 5042 1303 Lo...

Page 131: ...1260 SFC Binary Pump 131 Parts and Materials for Maintenance 9 Pump Head Assembly Channel A Figure 10 Pump Head Assembly with Seal Wash Option 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15...

Page 132: ...60 SFC Binary Pump 9 Parts and Materials for Maintenance Outlet Valve Outlet Valve Figure 11 Outlet valve p n Description G1312 60067 Outlet valve 1220 1260 G1312 60167 1260 Infinity Outlet Valve Type...

Page 133: ...Parts and Materials for Maintenance 9 Purge Valve Assembly Purge Valve Assembly Item p n Description 1 G7111 60061 Purge valve 2 01018 22707 PTFE frits pack of 5 3 5067 4728 Seal cap 5067 6595 1260 PV...

Page 134: ...24 Wrench open 14 mm 01018 23702 Insert tool 0100 1681 Syringe adapter luer barb 8710 2394 Hex key 9 64 inch 15 cm long T handle 8710 1534 Wrench 4 mm both ends open end 8710 2409 Wrench open end 5 16...

Page 135: ...rt ring seal wash 2 0515 1508 Screws for Seal Wash Pump Motor 1 5065 9978 Tubing 1 mm i d 3 mm o d silicone 5 m 4 0905 1175 Wash seal PTFE 1 5063 6589 Piston seal PTFE carbon filled black pack of 2 de...

Page 136: ...0 SFC Binary Pump 9 Parts and Materials for Maintenance Solvent Cabinet Solvent Cabinet For details refer to Usage Guideline for the Solvent Cabinet 01200 90150 p n Description 5067 5760 Solvent Cabin...

Page 137: ...embly Bottle Head Assembly p n Description G7120 60007 Bottle Head Assembly 5063 6598 Ferrules with lock ring 10 Pk 5063 6599 Tube screw 10 Pk Wire marker 5062 2483 Tube PTFE 1 5 mm x 5 m 3 mm od 5062...

Page 138: ...s Figure 12 Cover Parts Item p n Description 1 5067 5746 Door Assembly Infinity 180 Right 2 5067 5745 Door Assembly Infinity 180 Left 3 5043 1354 Name Plate 1290 Infinity 2 4 G7104 68713 Cabinet Kit 1...

Page 139: ...5181 1519 CAN cable Agilent module to module 1 m 1 5500 1246 Capillary ST 0 17 mm x 500 mm SI SI 1 5500 1217 Capillary ST 0 17 mm x 900 mm SI SX ps ps 3 5063 6527 Tubing assembly i d 6 mm o d 9 mm 1 2...

Page 140: ...140 1260 SFC Binary Pump 9 Parts and Materials for Maintenance Accessory Kit...

Page 141: ...0 Identifying Cables Cable Overview 142 Analog Cables 144 Remote Cables 146 CAN LAN Cables 150 RS 232 Cable Kit 151 Agilent 1200 Module to Printer 152 This chapter provides information on cables used...

Page 142: ...ription 35900 60750 Agilent 35900A A D converter 01046 60105 Analog cable BNC to general purpose spade lugs p n Description 5188 8029 ERI to general purpose 5188 8044 Remote Cable ERI ERI 5188 8045 Re...

Page 143: ...int to point connection p n Description RS232 61601 RS 232 cable 2 5 m Instrument to PC 9 to 9 pin female This cable has special pin out and is not compatible with connecting printers and plotters It...

Page 144: ...these cables provides a BNC connector to be connected to Agilent modules The other end depends on the instrument to which connection is being made Agilent Module to 35900 A D converters p n 35900 6075...

Page 145: ...es Agilent Module to BNC Connector Agilent Module to General Purpose p n 8120 1840 Pin BNC Pin Agilent module Signal Name Shield Shield Analog Center Center Analog p n 01046 60105 Pin Pin Agilent modu...

Page 146: ...Color code Enhanced Remote Classic Remote Active TTL 1 white IO1 START REQUEST Low 2 brown IO2 STOP Low 3 green IO3 READY High 4 yellow IO4 POWER ON High 5 grey IO5 NOT USED 6 pink IO6 SHUT DOWN Low...

Page 147: ...RI Signal Pin ERI Active TTL 10 GND 10 1 Start Request 1 Low 2 Stop 2 Low 3 Ready 3 High 5 Power on 5 High 4 Future 4 6 Shut Down 6 Low 7 Start 7 Low 8 Prepare 8 Low Ground Cable Shielding NC p n 5188...

Page 148: ...chnologies APG Analytical Products Group remote connector to be connected to Agilent modules The other end depends on the instrument to be connected to Table 11 5188 8057 ERI to APG and RJ45 p n 5188...

Page 149: ...are run Low 3 Gray 3 Gray Start Low 4 Blue 4 Blue Shut down Low 5 Pink 5 Pink Not connected 6 Yellow 6 Yellow Power on High 7 Red 7 Red Ready High 8 Green 8 Green Stop Low 9 Black 9 Black Start reques...

Page 150: ...lent modules CAN or LAN connectors CAN Cables LAN Cables p n Description 5181 1516 CAN cable Agilent module to module 0 5 m 5181 1519 CAN cable Agilent module to module 1 m p n Description 5023 0203 C...

Page 151: ...601 RS 232 cable 2 5 m Instrument to PC 9 to 9 pin female This cable has special pin out and is not compatible with connecting printers and plotters It s also called Null Modem Cable with full handsha...

Page 152: ...nt 1200 Module to Printer Agilent 1200 Module to Printer To connect a USB Flash Drive use a USB OTG cable with Mini B plug and A socket p n Description 5188 8050 USB A M USB Mini B 3 m PC Module 5188...

Page 153: ...ormation ALL 158 Rear view of the module 158 Interfaces 159 Overview Interfaces 160 ERI Enhanced Remote Interface 162 USB Universal Serial Bus 165 Setting the 6 bit Configuration Switch 166 Special Se...

Page 154: ...RS 232C memory management ability to update the firmware of the main system Main System Its properties are the complete communication capabilities CAN LAN USB and RS 232C memory management ability to...

Page 155: ...for example 1315B for the G1315B DAD R the firmware revision for example A for G1315B or B for the G1315C DAD VVV is the revision number for example 650 is revision 6 50 XXX is the build number of the...

Page 156: ...revision For example a G1315C DAD SL cannot be downgraded below firmware revision B 01 02 or to a A xx xx Some modules can be re branded e g G1314C to G1314B to allow operation in specific control so...

Page 157: ...used to control the module from a computer through a LAN connection This connector is activated and can be configured with the configuration switch With the appropriate software the USB connector may...

Page 158: ...e module Figure 14 Rear view of the pump electrical connections and label CCXZZ00000 Format CC Country of manufacturing DE Germany JP Japan CN China X Alphabetic character A Z used by manufacturing ZZ...

Page 159: ...Pump 2 Yes Yes No No E G7112B Binary Pump 2 Yes Yes No No E G7120A High Speed Pump 2 No Yes Yes 1 A Samplers G7129A B Vialsampler 2 Yes Yes No No E G7167A B Multisampler 2 Yes Yes No No E Detectors G7...

Page 160: ...369B C LAN Interface or they have an on board LAN interface e g detectors G1315C D DAD and G1365C D MWD This interface allows the control of the module system via a PC with the appropriate control sof...

Page 161: ...r technique To provide maximum safety within a distributed analysis system one line is dedicated to SHUT DOWN the system s critical parts in case any module detects a serious problem To detect whether...

Page 162: ...injection cycle for example by start key on any module Receiver is the autosampler 2 STOP L Request to reach system ready state as soon as possible for example stop run abort or finish and stop injec...

Page 163: ...ns eight individual programmable input output pins In addition it provides 24 V power and 5 V power and a serial data line to detect and recognize further add ons that could be connected to this inter...

Page 164: ...ure Use This serial line can be used to read out an EPROM or write into an EPROM of a connected ERI device The firmware can detect the connected type of device automatically and update information in...

Page 165: ...ware command defined turn on off For devices that need higher power Class 0 0 5 A maximum 12 W Class 1 1 0 A maximum 24 W Class 2 2 0 A maximum 48 W Class depends on hosting module s internal power ov...

Page 166: ...ngs provide configuration parameters for LAN and instrument specific initialization procedures All modules with FUSION electronics Default is ALL switches DOWN best settings Default IP address for LAN...

Page 167: ...en from non volatile memory 0 n a 2 2 not assigned Always keep these switches on position 0 off n a LAN Init Mode n a Use Default IP Address3 3 Default IP Address is 192 168 254 11 0 0 0 0 0 Use Stor...

Page 168: ...to bring the module into a defined mode with default parameter settings Boot Main System Revert to Default Data The instrument will boot to main mode and changes to the module s default parameter May...

Page 169: ...15 Boot Resident Forced Coldstart SW1 SW2 SW3 SW4 SW5 SW6 Init Mode 1 0 0 0 0 0 Boot Main System Keep Data 1 1 0 0 0 0 Boot Resident System Keep Data 1 0 0 0 0 1 Boot Main System Revert to Default Dat...

Page 170: ...the limit is exceeded Some counters can be reset to zero after the required maintenance procedure Using the EMF Counters The user settable EMF limits for the EMF Counters enable the early maintenance...

Page 171: ...ed in a metal inner cabinet which is enclosed by a plastic external cabinet The advantages of this packaging technology are virtual elimination of fixing screws bolts or ties reducing the number of co...

Page 172: ...172 1260 SFC Binary Pump 11 Hardware Information Instrument Layout...

Page 173: ...rameter configuration 175 Configuration Switches 176 Initialization Mode Selection 177 Dynamic Host Configuration Protocol DHCP 179 General Information DHCP 179 Setup DHCP 180 Manual Configuration 182...

Page 174: ...on a label at the rear of the module underneath the configuration switch see Figure 18 on page 174 Figure 17 MAC Label 2 Connect the instrument s LAN interface see Figure 18 on page 174 to the PC net...

Page 175: ...ing the so called Dynamic Host Configuration Protocol This mode requires a LAN onboard Module or a G1369C LAN Interface card see Setup DHCP on page 180 by manually setting the parameters using Telnet...

Page 176: ...he configuration switch can be accessed at the rear of the module Figure 19 Location of Configuration switch example shows a G7114A B VWD The module is shipped with all switches set to OFF as shown ab...

Page 177: ...is selected the parameters are taken from the non volatile memory of the module The TCP IP connection will be established using these parameters The parameters were configured previously by one of th...

Page 178: ...he session select the initialization mode Using Stored power on again and establish the TCP IP connection using the new parameters When the module is wired to the PC directly e g using a cross over ca...

Page 179: ...ome the active parameters immediately They are not stored to the non volatile memory of the card Besides requesting the network parameters the card also submits its hostname to the DHCP Server The hos...

Page 180: ...firmware B 06 40 or above or modules with D firmware All modules should use latest firmware from the same set 1 Note the MAC address of the LAN interface provided with G1369C LAN Interface Card or Ma...

Page 181: ...mStation Edition Lab Advisor Firmware Update Tool and use MAC address as host name e g 0030d3177321 The LC system should become visible in the control software see Note in section General Information...

Page 182: ...mandatory to make the stored parameters become the active parameters given that the initialization mode selection switches are allowing it Figure 24 Manual Configuration Principle With Telnet Whenever...

Page 183: ...e Figure 25 Telnet Starting a session where IP address may be the assigned address from a Bootp cycle a configuration session with the Handheld Controller or the default IP address see Configuration S...

Page 184: ...configuration parameter you are defining and value refers to the definitions you are assigning to that parameter Each parameter entry is followed by a carriage return 5 Use the and press Enter to lis...

Page 185: ...AC address initialization mode Initialization mode is Using Stored active TCP IP settings TCP IP status here ready connected to PC with controller software e g Agilent ChemStation here not connected F...

Page 186: ...ration parameters type exit and press Enter to exit with storing parameters Figure 30 Closing the Telnet Session NOTE If the Initialization Mode Switch is changed now to Using Stored mode the instrume...

Page 187: ...nstrument 189 Do Not Operate in an Explosive Atmosphere 190 Do Not Remove the Instrument Cover 190 Do Not Modify the Instrument 190 In Case of Damage 190 Solvents 191 Safety Symbols 192 Waste Electric...

Page 188: ...y for the customer s failure to comply with these requirements Safety Standards This is a Safety Class I instrument provided with terminal for protective earthing and has been manufactured and tested...

Page 189: ...ty or EMC regulations Make all connections to the unit before applying power NOTE Note the instrument s external markings described under Safety Symbols on page 192 WARNING Missing electrical ground E...

Page 190: ...mable gases or fumes Explosion hazard Do not operate the instrument in the presence of flammable gases or fumes WARNING Instrument covers removed Electrical shock Do Not Remove the Instrument Cover On...

Page 191: ...compartment at least 25 K below the boiling point of the solvent used Do not operate the instrument in an explosive atmosphere Reduce the volume of substances to the minimum required for the analysis...

Page 192: ...pecifications of refrigerant charge capacity carbon dioxide equivalent CDE and global warming potential GWP see instrument label Confirms that a manufactured product complies with all applicable Europ...

Page 193: ...jects that could be damaged by strong magnetic fields Indicates a pinching or crushing hazard Indicates a piercing or cutting hazard Table 21 Symbols WARNING A WARNING alerts you to situations that co...

Page 194: ...arting with 13 August 2005 NOTE This product complies with the WEEE Directive 2002 96 EC marking requirements The affixed label indicates that you must not discard this electrical electronic product i...

Page 195: ...protection against radio interference All cables are in compliance with safety or EMC regulations Test and Measurement If test and measurement equipment is operated with unscreened cables or used for...

Page 196: ...tatement is provided to comply with the requirements of the German Sound Emission Directive of 18 January 1991 This product has a sound pressure emission at the operator position 70 dB Sound Pressure...

Page 197: ...Pump 197 Appendix 13 Agilent Technologies on the Internet Agilent Technologies on the Internet For the latest information on products and services visit our worldwide web site on the Internet at http...

Page 198: ...dimensions 27 doors install 98 remove 98 dual piston in series design 11 E electrical connections descriptions of 157 electronic fuse of SSV open 81 electronic waste 194 electrostatic discharge ESD 9...

Page 199: ...figuration with telnet 182 manual configuration 182 TCP IP parameter configuration 175 using default 178 using stored 177 what you have to do first 174 174 leak sensor open 73 leak sensor short 73 lea...

Page 200: ...16 seal wash wash solvent 59 when to use 59 seals 39 serial number information 158 servo restart failed 85 shutdown 70 sieve 97 120 site requirements 23 power cords 25 solvent cabinet 39 136 solvent f...

Page 201: ...1260 SFC Binary Pump 201 Index W wash solvent 59 waste electrical and electronic equipment 194 WEEE directive 194 weight 27 wrong pump configuration 80...

Page 202: ...In This Book This manual contains The manual describes the following Introduction Site Requirements and Specifications Using the Pump Optimizing Performance Troubleshooting and Diagnostics Error Info...

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